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    • 75. 发明授权
    • Process of forming silver halide grains
    • 形成卤化银颗粒的方法
    • US5145768A
    • 1992-09-08
    • US454243
    • 1989-12-21
    • Yasunori IchikawaHiroshi OhnishiShigeharu UrabeAkira KojimaAkira Katoh
    • Yasunori IchikawaHiroshi OhnishiShigeharu UrabeAkira KojimaAkira Katoh
    • C01G5/02G03C1/005G03C1/015
    • G03C1/015G03C1/0051G03C2001/0153
    • A process of producing silver halide grains by disposing a mixer outside of a reaction vessel for causing a nucleus formation and/or a crystal growth of silver halide grains and containing an aqueous protective colloid solution. The process further includes the steps of: supplying an aqueous solution of a water-soluble silver salt, an aqueous solution of a water-soluble halide(s), and an aqueous solution of a protective colloid to the mixer while controlling the flow rates of the solutions; mixing them while controlling the rotational speed of a stirring blade of the mixer to form fine, silver halide grains; and immediately supplying the fine grains into the reaction vessel to perform the nucleus formation and/or the crystal growth of the silver halide grains in the reaction vessel. The silver halide fine grains thus formed in the mixer are quickly diluted with a liquid withdrawn from the reaction vessel and then the diluted mixture is supplied to the reaction vessel.
    • 通过在反应容器的外部设置混合器以产生卤化银颗粒的核形成和/或晶体生长并含有水性保护胶体溶液来生产卤化银颗粒的方法。 该方法还包括以下步骤:将水溶性银盐的水溶液,水溶性卤化物的水溶液和保护胶体的水溶液加入到混合器中,同时控制流动速率 解决方案; 混合它们同时控制混合器的搅拌叶片的旋转速度以形成细小的卤化银颗粒; 并立即将细粒供给到反应容器中,以进行反应容器内的卤化银颗粒的核形成和/或结晶生长。 在混合器中形成的卤化银细颗粒用从反应容器中取出的液体迅速稀释,然后将稀释的混合物供入反应容器。