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61. 发明申请

US20160376499A1 MOISTURE-RESISTANT PHOSPHOR COMPOSITIONS AND ASSOCIATE METHODS 审中-公开
标题翻译：防潮磷酸盐组合物及相关方法
公开(公告)号：US20160376499A1
公开(公告)日：2016-12-29
申请号：US15109267
申请日：2014-12-16
申请人： GENERAL ELECTRIC COMPANY
发明人： Anant Achyut Setlur , Robert Joseph Lyons , Prasanth Kumar Nammalwar , James Edward Murphy , Florencio Garcia , Ravikumar Hanumantha
IPC分类号： C09K11/02 , H01L33/50 , H01L33/52 , C09K11/61
CPC分类号： C09K11/025 , C09K11/616 , C09K11/617 , H01L33/502 , H01L33/505 , H01L33/507 , H01L33/52 , H01L2224/48091 , H01L2224/48247 , H01L2224/48257 , H01L2924/181 , H01L2924/00014 , H01L2924/00012
摘要： A phosphor composition is derived from combining K2SiF6:Mn4+ in solid form with a saturated solution of a manganese-free complex fluoride including a composition of formula I:A3[MF6], where A is selected from Na, K, Rb, and combinations thereof and M is selected from Al, Ga, In, Sc, Y, Gd, and combinations thereof. The composition of formula I:A3[MF6] has a water solubility lower than a water solubility of K2SiF6. A lighting apparatus including the phosphor composition is also provided.
摘要翻译：衍生自固体形式的K2SiF6：Mn4 +与包含式I：A3 [MF6]组成的无锰络合氟化物的饱和溶液的荧光体组合物，其中A选自Na，K，Rb及其组合 M选自Al，Ga，In，Sc，Y，Gd及其组合。式I的组合物：A3 [MF6]的水溶解度低于K2SiF6的水溶性。还提供了包括荧光体组合物的照明装置。

62. 发明授权

US09512357B2 Red-emitting phosphors, associated processes and devices 有权
标题翻译：红色发光荧光体，相关工艺和器件
公开(公告)号：US09512357B2
公开(公告)日：2016-12-06
申请号：US14337984
申请日：2014-07-22
申请人： General Electric Company
发明人： James Edward Murphy
IPC分类号： C09K11/61 , C09K11/02 , H01L33/50
CPC分类号： C09K11/617 , C09K11/616 , F21K9/64 , H01L33/502 , H01L2224/48091 , H01L2224/48247 , H01L2224/48257 , H01L2924/181 , H01L2924/00014 , H01L2924/00012
摘要： A process for synthesizing a Mn4+ doped phosphor is presented. The process includes contacting a source of Mn4+ ions to a suspension comprising aqueous hydrofluoric acid and a complex fluoride compound of formula (II) in solid form, and then contacting a source of A+ ions to the suspension to form the Mn4+ doped phosphor, Ax[MFy] (II) Wherein, A is Li, Na, K, Rb, Cs, or a combination thereof; M is Si, Ge, Sn, Ti, Zr, Al, Ga, In, Sc, Hf, Y, La, Nb, Ta, Bi, Gd, or a combination thereof; x is the absolute value of the charge of the [MFy] ion; y is 5, 6 or 7.
摘要翻译：提出了一种合成Mn4 +掺杂磷光体的方法。该方法包括使Mn4 +离子源与固体形式的含氢氟酸和式（II）的络合氟化合物的悬浮液接触，然后将A +离子源与悬浮液接触以形成Mn 4+掺杂的荧光体。（II）其中A为Li，Na，K，Rb，Cs或其组合; M是Si，Ge，Sn，Ti，Zr，Al，Ga，In，Sc，Hf，Y，La，Nb，Ta，Bi，Gd或它们的组合; x是[MFy]离子的电荷的绝对值; y是5,6或7。

63. 发明申请

US20160329471A1 MN-ACTIVATED HEXAFLUOROSILICATES FOR LED APPLICATIONS 审中-公开
标题翻译：用于LED应用的MN-活化的十六烷基磺酸盐
公开(公告)号：US20160329471A1
公开(公告)日：2016-11-10
申请号：US15213241
申请日：2016-07-18
申请人： KONINKLIJKE PHILIPS N.V.
发明人： Volker Weiler , Wolfgang Schnick , Peter Josef Schmidt , Markus Armin Seibald
IPC分类号： H01L33/50 , G02F1/1335 , C09K11/61
CPC分类号： H01L33/504 , C09K11/616 , C09K11/617 , G02F1/1336 , H01L33/502 , H01L2933/0041
摘要： The invention provides a lighting unit comprising a light source, configured to generate light source light and a luminescent material, configured to convert at least part of the light source light into luminescent material light, wherein the light source comprises a light emitting diode (LED) and wherein the luminescent material comprises a phosphor comprising M2AX6 doped with tetravalent manganese, wherein M comprises monovalent cations, at least comprising potassium and rubidium, wherein A comprises a tetravalent cation, at least comprising silicon, wherein X comprises a monovalent anion, at least comprising fluorine, and wherein M2AX6 has the hexagonal phase.
摘要翻译：本发明提供了一种照明单元，其包括被配置为产生光源光和发光材料的光源，其被配置为将至少部分光源光转换成发光材料光，其中光源包括发光二极管（LED）并且其中所述发光材料包括掺杂有四价锰的M2AX6的磷光体，其中M包含至少包含钾和铷的一价阳离子，其中A包含至少包含硅的四价阳离子，其中X包含一价阴离子，至少包含氟，并且其中M2AX6具有六方相。

64. 发明授权

US09388336B2 Processes for preparing color stable manganese-doped complex fluoride phosphors 有权
标题翻译：制备颜色稳定的锰掺杂复合氟化物荧光体的方法
公开(公告)号：US09388336B2
公开(公告)日：2016-07-12
申请号：US14568396
申请日：2014-12-12
申请人： GENERAL ELECTRIC COMPANY
发明人： James Edward Murphy , William Winder Beers , Robert Joseph Lyons , Fangming Du
IPC分类号： H01L33/50 , C09K11/61
CPC分类号： C09K11/616 , H01L33/502 , H01L33/507 , H01L2224/48247 , H01L2224/48257 , H01L2924/181 , H01L2924/00012
摘要： A process for preparing a color stable Mn4+ doped complex fluoride phosphor of formula I includes Ax(M(1−m), Mnm)Fy (I) contacting a first aqueous HF solution comprising (1−m) parts of a compound of formula HxMFy, and a second aqueous HF solution comprising m*n parts of a compound of formula Ax[MnFy], with a third aqueous HF solution comprising (1−n) parts of the compound of formula Ax[MnFy] and a compound of formula AaX, to yield a precipitate comprising the color stable Mn4+ doped complex fluoride phosphor; wherein A is Li, Na, K, Rb, Cs, NR4 or a combination thereof; M is Si, Ge, Sn, Ti, Zr, Al, Ga, In, Sc, Hf, Y, La, Nb, Ta, Bi, Gd, or a combination thereof; R is H, lower alkyl, or a combination thereof; X is an anion; a is the absolute value of the charge of the X anion; x is the absolute value of the charge of the [MFy] ion; y is 5, 6 or 7; 0
摘要翻译：制备式I的颜色稳定的Mn4 +掺杂复合氟化物荧光体的方法包括与包含（1-m）份式H x M F y的化合物的第一HF水溶液接触的M 1（M（1-m），Mnm）和包含m * n个分子式Ax [MnFy]化合物的第二HF水溶液与包含（1-n）份式Ax [MnF y]化合物和式AaX化合物的第一HF水溶液以产生包含颜色稳定的Mn4 +掺杂的复合氟化物荧光体的沉淀物; 其中A为Li，Na，K，Rb，Cs，NR4或其组合; M是Si，Ge，Sn，Ti，Zr，Al，Ga，In，Sc，Hf，Y，La，Nb，Ta，Bi，Gd或它们的组合; R是H，低级烷基或它们的组合; X是阴离子; a是X阴离子电荷的绝对值; x是[MFy]离子的电荷的绝对值; y为5,6或7; 0

65. 发明授权

US09371481B2 Color stable red-emitting phosphors 有权
标题翻译：颜色稳定的红色发光荧光粉
公开(公告)号：US09371481B2
公开(公告)日：2016-06-21
申请号：US14302907
申请日：2014-06-12
申请人： GENERAL ELECTRIC COMPANY
发明人： Florencio Garcia , Anant Achyut Setlur , James Edward Murphy , Srinivas Prasad Sista
IPC分类号： C09K11/61 , H05B33/12
CPC分类号： C09K11/617 , C09K11/616 , H01L2224/48247 , H01L2224/48257 , H01L2924/181 , H05B33/12 , H01L2924/00012
摘要： A process for synthesizing a Mn4+ doped phosphor includes contacting a precursor of formula I, Ax[MFy]:Mn4+ I at any temperature in a range from about 200° C. to about 700° C. with a fluorine-containing oxidizing agent in gaseous form; maintaining the temperature during a contact period of at least one hour; and, after the contact period, reducing the temperature at a rate of ≦5° C. per minute; wherein A is Li, Na, K, Rb, Cs, or a combination thereof; M is Si, Ge, Sn, Ti, Zr, Al, Ga, In, Sc, Hf, Y, La, Nb, Ta, Bi, Gd, or a combination thereof; x is the absolute value of the charge of the [MFy] ion; y is 5, 6 or 7.
摘要翻译：用于合成Mn4 +掺杂荧光体的方法包括在约200℃至约700℃的任何温度下将含有式I的前体Ax [MFy]：Mn4 + I与气态的含氟氧化剂形成; 在接触期间保持至少1小时的温度; 并且在接触期后以每分钟5℃的速度降低温度; 其中A为Li，Na，K，Rb，Cs或其组合; M是Si，Ge，Sn，Ti，Zr，Al，Ga，In，Sc，Hf，Y，La，Nb，Ta，Bi，Gd或它们的组合; x是[MFy]离子的电荷的绝对值; y是5,6或7。

66. 发明申请

US20160024378A1 RED-EMITTING PHOSPHORS, ASSOCIATED PROCESSES AND DEVICES 有权
标题翻译：红色荧光，相关工艺和器件
公开(公告)号：US20160024378A1
公开(公告)日：2016-01-28
申请号：US14337984
申请日：2014-07-22
申请人： General Electric Company
发明人： James Edward Murphy
IPC分类号： C09K11/61 , F21K99/00
CPC分类号： C09K11/617 , C09K11/616 , F21K9/64 , H01L33/502 , H01L2224/48091 , H01L2224/48247 , H01L2224/48257 , H01L2924/181 , H01L2924/00014 , H01L2924/00012
摘要： A process for synthesizing a Mn4+ doped phosphor is presented. The process includes contacting a source of Mn4+ ions to a suspension comprising aqueous hydrofluoric acid and a complex fluoride compound of formula (II) in solid form, and then contacting a source of A+ ions to the suspension to form the Mn4+ doped phosphor, Ax[MFy] (II) Wherein, A is Li, Na, K, Rb, Cs, or a combination thereof; M is Si, Ge, Sn, Ti, Zr, Al, Ga, In, Sc, Hf, Y, La, Nb, Ta, Bi, Gd, or a combination thereof; x is the absolute value of the charge of the [MFy] ion; y is 5, 6 or 7.
摘要翻译：提出了一种合成Mn4 +掺杂磷光体的方法。该方法包括使Mn4 +离子源与固体形式的含氢氟酸和式（II）的络合氟化合物的悬浮液接触，然后将A +离子源与悬浮液接触以形成Mn 4+掺杂的荧光体。（II）其中A为Li，Na，K，Rb，Cs或其组合; M是Si，Ge，Sn，Ti，Zr，Al，Ga，In，Sc，Hf，Y，La，Nb，Ta，Bi，Gd或它们的组合; x是[MFy]离子的电荷的绝对值; y是5,6或7。

67. 发明申请

US20150361336A1 COLOR STABLE RED-EMITTING PHOSPHORS 有权
标题翻译：颜色稳定的红色发光磷光体
公开(公告)号：US20150361336A1
公开(公告)日：2015-12-17
申请号：US14302907
申请日：2014-06-12
申请人： GENERAL ELECTRIC COMPANY
发明人： Florencio Garcia , Anant Achyut Setlur , James Edward Murphy , Srinivas Prasad Sista
IPC分类号： C09K11/61 , H05B33/12
CPC分类号： C09K11/617 , C09K11/616 , H01L2224/48247 , H01L2224/48257 , H01L2924/181 , H05B33/12 , H01L2924/00012
摘要： A process for synthesizing a Mn4+ doped phosphor includes contacting a precursor of formula I, Ax[MFy]:Mn4+ I at any temperature in a range from about 200° C. to about 700° C. with a fluorine-containing oxidizing agent in gaseous form; maintaining the temperature during a contact period of at least one hour; and, after the contact period, reducing the temperature at a rate of ≦5° C. per minute; wherein A is Li, Na, K, Rb, Cs, or a combination thereof; M is Si, Ge, Sn, Ti, Zr, Al, Ga, In, Sc, Hf, Y, La, Nb, Ta, Bi, Gd, or a combination thereof; x is the absolute value of the charge of the [MFy] ion; y is 5, 6 or 7.
摘要翻译：用于合成Mn4 +掺杂荧光体的方法包括在约200℃至约700℃的任何温度下将含有式I的前体Ax [MFy]：Mn4 + I与气态的含氟氧化剂形成; 在接触期间保持至少1小时的温度; 并且在接触期后以每分钟5℃的速度降低温度; 其中A为Li，Na，K，Rb，Cs或其组合; M是Si，Ge，Sn，Ti，Zr，Al，Ga，In，Sc，Hf，Y，La，Nb，Ta，Bi，Gd或它们的组合; x是[MFy]离子的电荷的绝对值; y是5,6或7。

68. 发明授权

US09091768B2 Scintillator material and radiation detector using same 有权
标题翻译：闪烁体材料和辐射探测器使用相同
公开(公告)号：US09091768B2
公开(公告)日：2015-07-28
申请号：US14118512
申请日：2012-06-06
申请人： Tamaki Kobayashi , Ryoko Ueyama , Toru Den
发明人： Tamaki Kobayashi , Ryoko Ueyama , Toru Den
IPC分类号： G01T1/202 , C09K11/62 , C04B35/515 , C04B35/653 , C09K11/61 , G01T1/20
CPC分类号： G01T1/2023 , C04B35/5152 , C04B35/653 , C04B2235/32 , C04B2235/3201 , C04B2235/3281 , C04B2235/3286 , C09K11/616 , C09K11/625 , G01T1/2006
摘要： Improvement in luminescence intensity is demanded from a scintillator material. The present invention provides a new scintillator material by adding a specific element selected from thallium and indium to a material having a basic composition represented by an alkali element:copper:a halogen element=3:2:5.
摘要翻译：闪烁体材料需要改善发光强度。本发明通过将选自铊和铟的特定元素添加到具有由碱元素：铜：卤素元素= 3:2:5表示的碱性组成的材料中提供新的闪烁体材料。

69. 发明授权

US08906724B2 Color stable red-emitting phosphors 有权
标题翻译：颜色稳定的红色发光荧光粉
公开(公告)号：US08906724B2
公开(公告)日：2014-12-09
申请号：US14311624
申请日：2014-06-23
申请人： General Electric Company
发明人： James Edward Murphy , Anant Achyut Setlur , Florencio Garcia , Robert Joseph Lyons , Ashfaqul Islam Chowdhury , Nagaveni Karkada , Prasanth Kumar Nammalwar
IPC分类号： H01L21/00 , H01L33/50 , H01L33/52 , C09K11/61
CPC分类号： H01L33/502 , C09K11/616 , C09K2211/181 , C09K2211/188 , H01L33/52 , H01L2224/48091 , H01L2224/48247 , H01L2924/181 , H01L2924/00014 , H01L2924/00012
摘要： A process for synthesizing a color stable Mn4+ doped phosphor includes contacting a precursor of formula I, in gaseous form at an elevated temperature with a fluorine-containing oxidizing agent to form the color stable Mn4+ doped phosphor Ax[MFy]:Mn4+ I wherein A is Li, Na, K, Rb, Cs, or a combination thereof; M is Si, Ge, Sn, Ti, Zr, Al, Ga, In, Sc, Hf, Y, La, Nb, Ta, Bi, Gd, or a combination thereof; x is the absolute value of the charge of the [MFy] ion; and y is 5, 6 or 7.
摘要翻译：用于合成颜色稳定的Mn4 +掺杂荧光体的方法包括在高温下以气态形式将式I的前体与含氟氧化剂接触以形成颜色稳定的Mn4 +掺杂荧光体Ax [MFy]：Mn4 + I，其中A为 Li，Na，K，Rb，Cs或其组合; M是Si，Ge，Sn，Ti，Zr，Al，Ga，In，Sc，Hf，Y，La，Nb，Ta，Bi，Gd或它们的组合; x是[MFy]离子的电荷的绝对值; y为5,6或7。

70. 发明申请

US20140320788A1 MN-ACTIVATED HEXAFLUOROSILICATES FOR LED APPLICATIONS 有权
标题翻译：用于LED应用的MN-活化的十六烷基磺酸盐
公开(公告)号：US20140320788A1
公开(公告)日：2014-10-30
申请号：US14007982
申请日：2012-12-06
申请人： Volker Weiler , Wolfgang Schnick , Peter Josef Schmidt , Markus Armin Seibald
发明人： Volker Weiler , Wolfgang Schnick , Peter Josef Schmidt , Markus Armin Seibald
IPC分类号： C09K11/61 , H01L33/50 , G02F1/1335
CPC分类号： H01L33/504 , C09K11/616 , C09K11/617 , G02F1/1336 , H01L33/502 , H01L2933/0041
摘要： The invention provides a lighting unit comprising a light source, configured to generate light source light and a luminescent material, configured to convert at least part of the light source light into luminescent material light, wherein the light source comprises a light emitting diode (LED) and wherein the luminescent material comprises a phosphor comprising M2AX6 doped with tetravalent manganese, wherein M comprises monovalent cations, at least comprising potassium and rubidium, wherein A comprises a tetravalent cation, at least comprising silicon, wherein X comprises a monovalent anion, at least comprising fluorine, and wherein M2AX6 has the hexagonal phase.
摘要翻译：本发明提供了一种照明单元，其包括被配置为产生光源光和发光材料的光源，其被配置为将至少部分光源光转换成发光材料光，其中光源包括发光二极管（LED）并且其中所述发光材料包括掺杂有四价锰的M2AX6的磷光体，其中M包含至少包含钾和铷的一价阳离子，其中A包含至少包含硅的四价阳离子，其中X包含一价阴离子，至少包含氟，并且其中M2AX6具有六方相。

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