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61. 发明授权

US07060750B2 Moisture-curable, polyether urethanes and their use in sealant, adhesive and coating compositions 失效
标题翻译：水溶性聚醚聚氨酯及其在密封剂，粘合剂和涂料组合物中的用途
公开(公告)号：US07060750B2
公开(公告)日：2006-06-13
申请号：US10834143
申请日：2004-04-28
申请人： Craig E. Jansen , Kurt C. Frisch , Richard R. Roesler , Dinesh Pethiyagoda , Kevan E. Hudson
发明人： Craig E. Jansen , Kurt C. Frisch , Richard R. Roesler , Dinesh Pethiyagoda , Kevan E. Hudson
IPC分类号： C08G18/48
CPC分类号： C08G18/3893 , C08G18/10 , C08G18/283 , C08G18/4866 , C08G2190/00
摘要： An adhesive, sealant or coating composition that includes: a) 20 to 80% by weight, based on the weight of a), b), and c) of a polyether urethane containing two or more reactive silane groups and one or more polyether segments, b) 20 to 80% by weight, based on the weight of a), b), and c) of a polyether urethane containing one reactive silane group and one or more polyether segments, and c) 1 to 60% by weight, based on the weight of a), b), and c) of a pigment having a BET surface area of from 15 to 100 m2/g and an oil absorption of from 40 to 110 cc/100 g; where the sum of a), b), and c) does not exceed 100% by weight. The composition can be used to bond and/or coat substrates.
摘要翻译：一种粘合剂，密封剂或涂料组合物，其包括：a）基于a），b）和c）的重量为20至80重量％的含有两个或更多个反应性硅烷基团和一个或多个聚醚部分的聚醚型聚氨酯，b）基于a），b）和c）的重量为20至80重量％的含有一个反应性硅烷基团和一个或多个聚醚链段的聚醚型氨基甲酸酯，以及c）1至60重量％基于a），b）和c）的重量，并且c）具有15-100m 2 / g的BET表面积和40至110cc / 100的吸油量的颜料 G; a），b）和c）的总和不超过100重量％。该组合物可用于粘合和/或涂覆底物。

62. 发明申请

US20050240063A1 Process for preparing reactive polyether polyols having an ethylene oxide end block 失效
标题翻译：制备具有环氧乙烷端嵌段的活性聚醚多元醇的方法
公开(公告)号：US20050240063A1
公开(公告)日：2005-10-27
申请号：US10828967
申请日：2004-04-21
申请人： Thomas Ostrowski , Raimund Ruppel , Gerd Hoppner , Sascha Bergmann , Koenraad Vandewalle , Eva Baum
发明人： Thomas Ostrowski , Raimund Ruppel , Gerd Hoppner , Sascha Bergmann , Koenraad Vandewalle , Eva Baum
IPC分类号： C08G18/48 , C08G65/26 , C07C43/18
CPC分类号： C08G65/2696 , C08G18/4841 , C08G18/4866 , C08G65/2663
摘要： Process for preparing polyether polyols having an end block of ethylene oxide by addition of alkylene oxides onto H-functional starter substances, in which A) a polyether polyol precursor is prepared by means of double metal cyanide (DMC) catalysis in a semicontinuous mode of operation in which previously prepared polyether polyol together with the DMC catalyst are placed in a reactor and H-functional starter substance and propylene oxide are added continuously, B) the polyether polyol precursor from stage A) is reacted with propylene oxide or an ethylene oxide/propylene oxide mixture in the presence of the DMC catalyst in a continuously operating reactor to give a polyether polyol intermediate, C) the intermediate from stage B) is mixed with an alkali metal hydroxide as catalyst and D) reacted with ethylene oxide in a continuously operating reactor to give the final product, E) the catalyst is separated off from the final product obtained in stage D).
摘要翻译：制备具有环氧乙烷端嵌段的聚醚多元醇的方法，其通过在H-功能起始物质上加入环氧烷烃，其中A）聚醚多元醇前体是通过半连续运行模式中的双金属氰化物（DMC）催化制备的其中将预先制备的聚醚多元醇与DMC催化剂一起放入反应器中，并连续加入H官能引发剂物质和环氧丙烷，B）将来自阶段A）的聚醚多元醇前体与环氧丙烷或环氧乙烷/丙烯氧化物混合物在DMC催化剂存在下在连续操作的反应器中得到聚醚多元醇中间体，C）将来自阶段B）的中间体与作为催化剂的碱金属氢氧化物混合，并且D）在连续操作的反应器中与环氧乙烷反应得到最终产物，E）将催化剂从阶段D）中得到的最终产物中分离出来。

63. 发明申请

US20050159629A1 Process for production of polyols with hydroxide containing double metal cyanide (DMC) Catalysts 有权
公开(公告)号：US20050159629A1
公开(公告)日：2005-07-21
申请号：US11029591
申请日：2005-01-05
申请人： George Combs
发明人： George Combs
IPC分类号： C08G65/10 , B01J23/16 , B01J23/54 , B01J23/70 , B01J27/26 , C08G18/48 , C08G65/26 , C07C41/03
CPC分类号： C08G65/10 , B01J27/26 , C08G18/4866 , C08G65/2663
摘要： The present invention provides process for producing polyols using a crystalline, hydroxide containing double metal cyanide (DMC) catalyst of the formulae (I) or (II), M1x[M2(CN)6]yOH•L (I) M1x[M2(CN)6]y.zM1(OH)q•L (II) wherein M1 represents a metal selected from Zn+2, Fe+2, Ni+2, Mn+2, Co+2, Sn+2, Pb+2, Fe+3, Mo+4, Mo+6, Al+3, V+4, V+5, Sr+2, W+4, W+6, Cu+2 and Cr+3, M2 represents a metal selected from Fe+2, Fe+3, Co+2, Co+3, Cr+2, Cr+3, Mn+2, Mn+3, Ir+3, Ni+2, Rh+3, Ru+2, V+4 and V+5, L represents an organic ligand and x, y and q are chosen to maintain electroneutrality. The polyols of the present invention may find use in the preparation of polyurethanes.

64. 发明授权

US06919486B2 Polyetherols produced using aluminium phosphonate catalysts 失效
标题翻译：使用磷酸铝催化剂生产的聚醚砜
公开(公告)号：US06919486B2
公开(公告)日：2005-07-19
申请号：US10036679
申请日：2001-12-21
申请人： Edward M. Dexheimer
发明人： Edward M. Dexheimer
IPC分类号： B01J31/12 , B01J31/14 , C08G65/26 , C07C43/11
CPC分类号： C08G65/2654 , B01J31/0212 , B01J31/0214 , B01J31/0259 , B01J31/143 , B01J2231/14 , C07F9/02 , C08G18/4866 , C08G65/12 , C08G2101/0008 , C08G2101/0083
摘要： A method for the production of polyetherols using aluminum phosphonate catalysts is disclosed. Reaction products of the process include various polyetherols including very low unsaturation polyether polyols. The aluminum phosphonate catalyst preferably has a general structure of RPO-(OAlR′R″)2, wherein O represents oxygen, P represents pentavalent phosphorous, Al represents aluminum, R comprises a hydrogen, an alkyl group, or an aryl group, and R′ and R″ independently comprise a halide, an alkyl group, an alkoxy group, an aryl group, or an aryloxy group. Polyols produced according to the disclosed procedure have properties very similar to or more beneficial than those produced utilizing the typical base catalysts.
摘要翻译：公开了一种使用磷酸铝催化剂生产聚醚的方法。该方法的反应产物包括各种聚醚类，包括非常低不饱和度的聚醚多元醇。膦酸铝催化剂优选具有RPO-（OAlR'R“）2 N的一般结构，其中O表示氧，P表示五价磷，Al表示铝，R包括氢，烷基或芳基，R'和R“独立地包括卤素，烷基，烷氧基，芳基或芳氧基。根据所公开的方法制备的多元醇具有与使用典型的碱催化剂制备的那些非常相似或更有益的性质。

65. 发明申请

US20050119438A1 TMXDI-based oligomer and formulations containing it 有权
标题翻译：基于TMXDI的低聚物和含有它的制剂
公开(公告)号：US20050119438A1
公开(公告)日：2005-06-02
申请号：US10995622
申请日：2004-11-23
申请人： Joseph Leon , Kenneth Swiderski , Joseph DeSousa , Richard Finch
发明人： Joseph Leon , Kenneth Swiderski , Joseph DeSousa , Richard Finch
IPC分类号： C08G18/00 , C08G18/67 , C08G18/76 , C09J175/16
CPC分类号： C08G18/4845 , C08G18/10 , C08G18/282 , C08G18/2825 , C08G18/4825 , C08G18/4866 , C08G18/672 , C08G18/765 , C09D175/16 , C09J175/16 , C08G18/48
摘要： The meta tetramethylxylenediisocyanate-based polyether urethane acrylate oligomer reduces the viscosities of polymerizable formulations, as compared to other isocyanate-based oligomers, significantly enhances adhesion to certain substrates, and imparts increased elongation-to-break valves to cured products produced therefrom.
摘要翻译：与其它异氰酸酯基低聚物相比，间甲基亚甲基二异氰酸酯基聚醚聚氨酯丙烯酸酯低聚物降低了可聚合配方的粘度，显着提高了对某些基材的粘合性，并赋予了由其生产的固化产品增加的断裂 - 断裂阀。

66. 发明申请

US20050090572A1 Process for the preparation of a polyether polyol 审中-公开
标题翻译：制备聚醚多元醇的方法
公开(公告)号：US20050090572A1
公开(公告)日：2005-04-28
申请号：US10961271
申请日：2004-10-08
申请人： Johannes Beckers , Michiel Eleveld , Gerardus Ingenbleek
发明人： Johannes Beckers , Michiel Eleveld , Gerardus Ingenbleek
IPC分类号： C08G18/00 , C08G18/48 , C08G65/10 , C08G65/12 , C08G65/26
CPC分类号： C08G65/2663 , C08G18/4829 , C08G18/4866 , C08G2101/0008
摘要： The invention relates to a process for the preparation of a polyalkoxylene polyether polyol, which process involves contacting an initiator compound having from 2 to 6 active hydrogen atoms in the presence of a catalyst comprising a dimetal cyanide complex with a crude alkylene oxide to obtain the polyoxyalkylene polyether polyol.
摘要翻译：本发明涉及一种制备聚亚烷氧基聚醚多元醇的方法，该方法包括在含有二氰基氰化物络合物的催化剂与粗环氧烷烃的存在下使具有2-6个活性氢原子的引发剂化合物接触，得到聚氧化烯聚醚多元醇。

67. 发明授权

US06855658B1 Hydroxide containing double metal cyanide (DMC) catalysts 有权
标题翻译：含有双金属氰化物（DMC）催化剂的氢氧化物
公开(公告)号：US06855658B1
公开(公告)日：2005-02-15
申请号：US10649520
申请日：2003-08-26
申请人： George G. Combs
发明人： George G. Combs
IPC分类号： C08G65/10 , B01J23/16 , B01J23/54 , B01J23/70 , B01J27/26 , C08G18/48 , C08G65/26
CPC分类号： C08G65/10 , B01J27/26 , C08G18/4866 , C08G65/2663
摘要： The present invention provides a crystalline, hydroxide containing double metal cyanide (DMC) catalyst of the formulae (I) or (II), M1x[M2(CN)6]yOH.L (I) M1x[M2(CN)6]y.zM1(OH)q.L (II) wherein M1 represents a metal selected from Zn+2, Fe+2, Ni+2, Mn+2, Co+2, Sn+2, Pb+2, Fe+3, Mo+4, Mo+6, Al+3, V+4, V+5, Sr+2, W+4, W+6, Cu+2 and Cr+3, M+2 represents a metal selected from Fe+2, Fe+3, Co+2, Co+3, Cr+2, Cr+3, Mn+2, Mn+3, Ir+3, Ni+2, Rh+3, Ru+2, V+4 and V+5, L represents an organic ligand and x, y and q are chosen to maintain electroneutrality. Further provided are processes for the production of the inventive DMC catalysts. The crystalline, hydroxide containing DMC catalysts of the present invention may find use in the preparation of polyols, such as polyether polyols.
摘要翻译：本发明提供一种结晶的含氢氧化物的式（I）或（II）双金属氰化物（DMC）催化剂，其中M 1表示选自Zn 2+，Fe 2+，Ni Mn +2，Co +2，Sn +2，Pb +2，Fe +3，Mo +4，Mo +6，Al + 3+，V +4，V +5，Sr +，W +4，W +6，Cu +和Cr +3，M +2，表示选自Fe +2，Fe +3，Co +2，Co +3，Cr +2，Cr3 +，Mn2 +，Mn + 3+，Ir <+3>，Ni +，Rh +3，Ru +2，V +4和V +5，L表示有机配体，x，y和q 被选为维持电中性。还提供了制备本发明的DMC催化剂的方法。本发明的含结晶氢氧化物的DMC催化剂可用于制备多元醇，例如聚醚多元醇。

68. 发明授权

US06844413B2 Moisture-curable, polyether urethanes with reactive silane groups and their use as sealants, adhesives and coatings 有权
标题翻译：具有反应性硅烷基团的水分固化型聚醚聚氨酯及其作为密封剂，粘合剂和涂料的用途
公开(公告)号：US06844413B2
公开(公告)日：2005-01-18
申请号：US10690956
申请日：2003-10-22
申请人： Richard R. Roesler , Derek L. Crawford , Kurt C. Frisch , Dinesh Pethiyagoda , Karsten Danielmeier
发明人： Richard R. Roesler , Derek L. Crawford , Kurt C. Frisch , Dinesh Pethiyagoda , Karsten Danielmeier
IPC分类号： C08G18/08 , C08G18/10 , C08G18/28 , C08G18/38 , C08G18/48 , C09D175/04 , C09J175/04 , C08G77/26
CPC分类号： C08G18/3893 , C08G18/0885 , C08G18/10 , C08G18/283 , C08G18/289 , C08G18/3821 , C08G18/4866 , C08G2190/00 , C09J175/04
摘要： A moisture-curable, alkoxysilane-functional polyether urethanes containing a) 20 to 90% by weight, of a polyether urethane containing two or more reactive silane groups and one or more polyether segments, where the polyether segments have a number average molecular weight (Mn) of at least 3000 and a degree of unsaturation of less than 0.04 milliequivalents/g, and the sum of Mn of all of the polyether segments per molecule averages 6000 to 20,000, and the reactive silane groups are incorporated by the reaction of an isocyanate group with a compound of formula H2N—Y—Si—(X)3 (I) b) 10 to 80% by weight, of a polyether urethane containing one reactive silane group and one or more polyether segments having Mn of 1000 to 15,000, where the reactive silane groups are incorporated by the reaction of an isocyanate group with a compound of formula
摘要翻译：含有20〜90重量％的含有两个以上反应性硅烷基团和一个以上聚醚链段的聚醚型聚氨酯的水分固化性烷氧基硅烷官能团聚氨酯，其中聚醚链段的数均分子量（Mn）至少3000，不饱和度小于0.04毫当量/ g，每个分子中所有聚醚链段的Mn的总和平均为6000至20,000，反应性硅烷基团通过异氰酸酯基团与一种化合物）10-80重量％的含有一个反应性硅烷基团的聚醚聚氨酯和一个或多个Mn为1000-15,000的聚醚链段，其中反应性硅烷基团通过异氰酸酯基团与式的化合物

69. 发明申请

US20050004304A1 Elastic meth(acrylic) adhesive compositions 审中-公开
标题翻译：弹性（丙烯酸）粘合剂组合物
公开(公告)号：US20050004304A1
公开(公告)日：2005-01-06
申请号：US10468299
申请日：2002-03-04
申请人： Ria De Cooman , Werner Meyer , Rene Flury
发明人： Ria De Cooman , Werner Meyer , Rene Flury
IPC分类号： C08F290/04 , C08F290/06 , C08G18/48 , C08G18/67 , C09J4/06 , C09J175/16 , C08J3/00
CPC分类号： C09J175/16 , C08F290/048 , C08F290/067 , C08G18/4866 , C08G18/672 , C09J4/06 , C08G18/48
摘要： Described is an adhesive composition with a high elasticity, measured in terms of elongation at break, and an elastic behavior approaching the ideal Hook law in the stress-strain diagram. Said adhesive composition comprises (a) at least one mono-functional meth(acrylic) monomer A whose homo-polymer or co-polymer exhibit a glass transition temperature (Tg) between 40° C. and 140° C., (b) at least one monofunctional meth(acrylic) monomer B of the following structure (B): wherein R is H or CH3, R′ is H or (CH2)nCH3 with n=0 to 2, in particular CH2CH3 or H, and R″ is C3-C20-alkyl or phenoxy or O—(CH2)n—H3 or O—[(CH2)2—O]s; 0 to 2, in particular (CH2)nCH3 wherein n is 3 or 10 to 13, and c) at least one liquid elastomer C in the molecular weight range of 1000 to 9000 with (meth)acrylic derivative groups, preferably (meth)acrylic ester groups, whereby the components A, B, and C are present in the following amounts: B based on the total weight of A+B+C=5 to 20% by weight, C based on the total weight of A+C=30 to 70% by weight.
摘要翻译：描述了一种具有高弹性的粘合剂组合物，以断裂伸长率测量，以及在应力 - 应变图中接近理想的Hook定律的弹性性能。所述粘合剂组合物包含（a）至少一种单官能甲基（丙烯酸）单体A，其均聚物或共聚物表现出40℃至140℃之间的玻璃化转变温度（Tg），（b）至少一种具有以下结构（B）的单官能甲基（丙烯酸）单体B：其中R是H或CH 3，R'是H或（CH 2）n CH 3，n = 0至2，特别是CH 2 CH 3或H，R“ 是C 3 -C 20 - 烷基或苯氧基或O-（CH 2）n-H3或O - [（CH 2）2 -O]定制字符文件=“US20050004304A1-20050106-P00900.TIF”wi =“20” “20”id =“custom-character-00001”/> s; 0至2，特别是（CH 2）n CH 3，其中n为3或10至13，以及c）至少一种分子量范围为1000至9000的液体弹性体C（甲基）丙烯酸衍生物基团，优选（甲基）丙烯酸酯基，其中组分A，B和C以以下量存在：基于A + B + C的总重量= 5至20重量％的B，基于A + C = 30〜70重量％。

70. 发明授权

US06835801B2 Activated starter mixtures and the processes related thereto 有权
标题翻译：活化起动混合物及其相关工艺
公开(公告)号：US06835801B2
公开(公告)日：2004-12-28
申请号：US10199916
申请日：2002-07-19
申请人： John E. Hayes
发明人： John E. Hayes
IPC分类号： C08G6510
CPC分类号： C08G65/2696 , C08G18/4866 , C08G65/2609 , C08G65/2663
摘要： The present invention is directed to an activated starter mixture which can be used to prepare polyoxyalkylene polyols. The present invention is also directed to a process for preparing an activated starter mixture, particularly, to a process for preparing an activated starter mixture which is composed of a low molecular weight starter compound. The present invention is also directed to a batch or semi-batch process for the polyaddition of an alkylene oxide on to an activated starter mixture, particularly, on to an activated starter mixture which is composed of a low molecular weight starter compound. The present invention provides an activated starter mixture, particularly, an activated starter mixture which is composed of a low molecular weight starter compound, which rapidly initiates polymerization. The present invention can eliminate the need to synthesize costly high molecular weight starter compounds by KOH catalysis in a separate, dedicated reactor.
摘要翻译：本发明涉及可用于制备聚氧化烯多元醇的活化起始混合物。本发明还涉及一种制备活化起始混合物的方法，特别是制备由低分子量起始化合物组成的活化起始混合物的方法。本发明还涉及用于将烯化氧加成到活化起始混合物上的批次或半间歇方法，特别是涉及由低分子量起始化合物组成的活化起始混合物。本发明提供活化的起始混合物，特别是由低分子量起始化合物组成的活化起始混合物，其迅速引发聚合。本发明可以消除在单独的专用反应器中通过KOH催化合成昂贵的高分子量起始物化合物的需要。

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