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61. 发明授权

US07902406B2 Lubricating oil 失效
标题翻译：润滑油
公开(公告)号：US07902406B2
公开(公告)日：2011-03-08
申请号：US12066300
申请日：2006-09-13
申请人： Suguru Ohara , Satoshi Hiyoshi , Yukihiro Isogai , Makoto Goto
发明人： Suguru Ohara , Satoshi Hiyoshi , Yukihiro Isogai , Makoto Goto
IPC分类号： C10M105/38 , C07C31/27 , C07C47/347 , C07C69/757 , C10M169/02 , C10M177/00
CPC分类号： C07C69/75 , C07C29/141 , C07C31/27 , C07C45/50 , C07C45/69 , C07C67/08 , C07C2601/14 , C07C2602/42 , C10M105/38 , C10M2207/2835 , C10N2230/02 , C10N2230/06 , C10N2230/08 , C10N2230/10 , C07C47/445 , C07C31/278
摘要： The present invention provides a lubricating oil comprising an alicyclic compound represented by a general formula (I): wherein n is an integer of 0 or 1; one of R1 and R2 represents —CH2OR4 (wherein R4 represents a carboxylic acid residue) while the other one represents alkyl, lower alkyl-substituted or unsubstituted cycloalkyl, aryl, or aralkyl; and R3 represents —CH2OR5 (wherein R5 represents a carboxylic residue) and the like. The lubricating oil of the present invention has an excellent traction coefficient, excellent heat resistance, or the like. For the lubricating oil of the present invention, the alicyclic compound represented by the general formula (I) can be directly used as it is, and other base oils such as ester oil, poly-α-olefin, mineral oil, or silicone oil may be included therein, if necessary.
摘要翻译：本发明提供一种润滑油，其含有通式（I）表示的脂环族化合物：其中n为0或1的整数; R 1和R 2之一表示-CH 2 OR 4（其中R 4表示羧酸残基），而另一个表示烷基，低级烷基取代或未取代的环烷基，芳基或芳烷基; 和R 3表示-CH 2 OR 5（其中R 5表示羧基残基）等。本发明的润滑油具有优异的牵引系数，优异的耐热性等。对于本发明的润滑油，可以直接使用由通式（I）表示的脂环族化合物，其它基油如酯油，聚-α-烯烃，矿物油或硅油可以如果有必要的话。

62. 发明授权

US07842844B2 Process for the conversion of hydrocarbons to C2-oxygenates 有权
标题翻译：将烃转化为C2-含氧化合物的方法
公开(公告)号：US07842844B2
公开(公告)日：2010-11-30
申请号：US11988204
申请日：2006-06-29
申请人： Martin Philip Atkins
发明人： Martin Philip Atkins
IPC分类号： C07C29/14 , C07C27/06
CPC分类号： C07C29/149 , C07C29/141 , C07C29/1518 , C07C31/08
摘要： Process for the conversion of hydrocarbons to ethanol and optionally acetic acid by converting hydrocarbon in a syngas reactor into a stream A comprising a mixture of carbon oxide(s) and hydrogen preferably having a H2/CO molar ratio between 1.5 and 2.5, converting at least part of stream A in the presence of a particulate catalyst in a reactor under a temperature between 150 and 400° C. and a pressure of 5 to 200 bar, into a C2-oxygenates stream B, where stream B includes water, alkanes, ethanol, acetaldehyde, ethyl acetate and acetic acid, which together represent least 80% by weight of the products obtained from the C2-oxygenates conversion reactor. The C2-oxygenates stream B is separated into a stream C comprising H2, CO, CO2 and alkanes, and a stream D including 15 to 40 wt % of acetic acid, 10 to 40 wt % of acetaldehyde and 15 to 40 wt % of ethanol. At least part of stream D is hydrogenated in a hydrogenation reactor into an ethanol stream E, and stream E is subjected to a separating step, followed by recovery of ethanol.
摘要翻译：通过将合成气反应器中的烃转化为包含碳氧化物和氢气的混合物的流A优选具有1.5至2.5的H 2 / CO摩尔比的方法将烃转化为乙醇和任选的乙酸的方法，至少转化在反应器中，在150-400℃的温度和5-200巴的压力下，在颗粒催化剂存在下，将一部分流A转化成C2-含氧化合物流B，其中流B包括水，烷烃，乙醇，乙醛，乙酸乙酯和乙酸，它们一起占由C2-含氧化合物转化反应器获得的产物的至少80重量％。将C2-含氧物流B分离成包含H 2，CO，CO 2和烷烃的流C，以及包含15至40重量％的乙酸，10至40重量％的乙醛和15至40重量％的乙醇的流D 。将流D的至少一部分在氢化反应器中氢化成乙醇流E，并使流E进行分离步骤，然后回收乙醇。

63. 发明授权

US07816107B2 Method for producing an optically active 2-methyl-alkane-1-ol from the corresponding 2-methylalk-2-en-1-al, comprising carbonyl-selective reduction, enantioselective hydration and lipase-catalyzed, stereoselective acylation in order to enrich the desired 有权
标题翻译：从相应的2-甲基-2-烯-1-烯制备光学活性2-甲基 - 烷-1-醇的方法，包括羰基选择性还原，对映选择性水合和脂肪酶催化的立体选择性酰化，以富集想要的
公开(公告)号：US07816107B2
公开(公告)日：2010-10-19
申请号：US11576317
申请日：2005-09-22
申请人： Christoph Jäkel , Gunnar Heydrich , Rainer Stürmer , Rocco Paciello
发明人： Christoph Jäkel , Gunnar Heydrich , Rainer Stürmer , Rocco Paciello
IPC分类号： C12P7/04
CPC分类号： C12P7/04 , C07B2200/07 , C07C29/14 , C07C29/141 , C07C29/172 , C12C11/02 , C07C33/025 , C07C31/125
摘要： A process for preparing optically active 2-methylalkan-1-ol of the general formula (III) comprising the following steps: (i) carbonyl-selective reduction of 2-methylalk-2-en-1-al of the general formula (I) to 2-methylalk-2-en-1-ol of the general formula (II), (ii) enantioselective hydrogenation of 2-methylalk-2-en-1-ol to the general formula (iii), (iii) increasing the optical yield of the optically active 2-methylalkan-1-ol (III) obtained in step (ii) by a lipase-catalyzed acylation reaction, where the radical R means C1-C10-alkyl.
摘要翻译：一种制备通式（III）的光学活性2-甲基烷-1-醇的方法，包括以下步骤：（i）通式（I）的2-甲基-α-烯-1-醇的羰基选择性还原）到通式（II）的2-甲基-2-烯-1-醇，（ii）2-甲基烯-2-烯-1-醇与通式（iii）的对映选择性氢化，（iii）增加通过脂肪酶催化的酰化反应在步骤（ii）中获得的光学活性2-甲基
链烷-1-醇（III）的光学收率，其中基团R是指C 1 -C 10 - 烷基。

64. 发明申请

US20100210880A1 MULTISTAGE CONTINUOUS PROCESS FOR THE HYDROFORMYLATION OF HIGHER OLEFINS OR OLEFIN MIXTURES 有权
标题翻译：用于高烯烃或烯烃混合物加氢的多级连续方法
公开(公告)号：US20100210880A1
公开(公告)日：2010-08-19
申请号：US12682500
申请日：2008-10-28
申请人： Hans-Gerd Lueken , Alfred Kaizik , Stefan Drees , Wilfried Bueschken
发明人： Hans-Gerd Lueken , Alfred Kaizik , Stefan Drees , Wilfried Bueschken
IPC分类号： C07C45/00 , C07C29/00
CPC分类号： C07C29/141 , B01J31/20 , B01J2531/845 , C07C29/16 , C07C45/50 , C07C31/125 , C07C47/02
摘要： The invention relates to a process for the continuous preparation of aldehydes and/or alcohols having at least 6 carbon atoms by multistage hydroformylation of olefins or olefin mixtures having at least 5 carbon atoms in the presence of unmodified cobalt complexes, in which at least two reactors are operated at different temperatures in the temperature range from 100 to 220° C. and pressures of from 100 to 400 bar, which is characterized in that a) one reactor is operated at temperatures above 160° C. by the one-pot process with simultaneous catalyst formation, catalyst extraction and hydroformylation and the amount of water fed into the reactor with the aqueous cobalt salt solution is greater than that discharged from the reactor with the liquid reaction mixture and the gas phase together, with part of the aqueous bottom phase being discharged from the reactor to keep the level of the aqueous bottom phase constant, b) and the cobalt carbonyls in the aqueous phase taken off or part thereof are introduced into the reactor which is operated at a lower temperature.
摘要翻译：本发明涉及通过在未改性的钴配合物存在下，通过使具有至少5个碳原子的烯烃或烯烃混合物进行多级加氢甲酰化，连续制备具有至少6个碳原子的醛和/或醇的方法，其中至少两个反应器在不同的温度下在100至220℃的温度范围和100-400巴的压力下操作，其特征在于：a）一个反应器在160℃以上的温度下通过一锅法操作，同时催化剂形成，催化剂萃取和加氢甲酰化反应，并且用钴盐水溶液进料到反应器中的水量大于从反应器排出的水，液体反应混合物和气相在一起，部分水相底部为从反应器排出以保持水相底部相的水平恒定，b）和水相中的羰基钴脱离或部分t 将其引入在较低温度下操作的反应器中。

65. 发明授权

US07663006B2 Process for production of purified alcohols 有权
标题翻译：纯化醇的生产方法
公开(公告)号：US07663006B2
公开(公告)日：2010-02-16
申请号：US10592699
申请日：2005-03-14
申请人： Hirofumi Oota , Hiroki Kawasaki
发明人： Hirofumi Oota , Hiroki Kawasaki
IPC分类号： C07C29/141
CPC分类号： C07C29/141 , C07C45/74 , C07C47/21 , C07C31/125
摘要： A process for producing a purified alcohol giving satisfactory results in a sulfuric acid coloring test is provided.A process for producing a purified alcohol which includes the following steps: a condensation step in which an aldehyde is subjected to aldol condensation and dehydration to obtain the corresponding condensate, a hydrogenation step in which the condensate is hydrogenated to obtain a crude alcohol, and a purification step in which the crude alcohol is distilled to obtain a purified alcohol, characterized in that the crude alcohol in which the concentration of one or more compounds having an oxygen-containing heterocycle having a carbon-carbon double bond in the ring is 200 weight ppm or lower is fed to the purification step. Specifically, the aldehyde is normal butyraldehyde, the condensate is 2-ethylhexenal, and the alcohol is 2-ethylhexanol.
摘要翻译：提供了在硫酸着色试验中得到令人满意的结果的纯化醇的制造方法。一种精制醇的制造方法，其特征在于，包括以下步骤：将醛进行醛醇缩合脱水得到相应的缩合物的缩合工序，将氢化氢化得到粗醇的氢化工序，蒸馏粗醇以获得纯化醇的纯化步骤，其特征在于，其中环中具有碳 - 碳双键的含氧杂环的一种或多种化合物的浓度的粗醇为200重量ppm 或更低的量进料至纯化步骤。具体来说，醛为正丁醛，缩合物为2-乙基己烯醛，醇为2-乙基己醇。

66. 发明申请

US20090306437A1 METHANOL SYNTHESIS 失效
标题翻译：甲醇合成
公开(公告)号：US20090306437A1
公开(公告)日：2009-12-10
申请号：US12136142
申请日：2008-06-10
申请人： John E. Stauffer
发明人： John E. Stauffer
IPC分类号： C07C29/00
CPC分类号： C07C17/154 , C07C17/23 , C07C29/141 , C07C45/43 , C07C19/03 , C07C47/04 , C07C31/04
摘要： A process is disclosed for the synthesis of methanol from methane comprising three reaction steps operated in tandem. In the first step methylene chloride is produced by the reaction of methane with oxygen and hydrogen chloride. In the second step, methylene chloride is hydrolyzed to formaldehyde, which is hydrogenated in the third step to provide the product methanol.
摘要翻译：公开了从甲烷合成甲醇的方法，其包括串联操作的三个反应步骤。在第一步中，通过甲烷与氧气和氯化氢的反应产生二氯甲烷。在第二步中，将二氯甲烷水解成甲醛，在第三步中氢化，得到产物甲醇。

67. 发明申请

US20090293348A1 EFFICIENT AND SELECTIVE CHEMICAL RECYCLING OF CARBON DIOXIDE TO METHANOL, DIMETHYL ETHER AND DERIVED PRODUCTS 有权
标题翻译：二氧化碳对甲醇，二甲醚和衍生产物的有效和选择性化学回收
公开(公告)号：US20090293348A1
公开(公告)日：2009-12-03
申请号：US12537647
申请日：2009-08-07
申请人： George A. Olah , G.K. Surya Prakash
发明人： George A. Olah , G.K. Surya Prakash
IPC分类号： C10L1/185 , C10L1/182
CPC分类号： C07C29/136 , C07C1/20 , C07C29/04 , C07C29/14 , C07C29/141 , C07C29/149 , C07C41/09 , C07C51/15 , C07C67/08 , C07C67/38 , C07C68/005 , C07C68/02 , C25B3/04 , C07C31/08 , C07C31/04 , C07C31/10 , C07C11/02 , C07C53/02 , C07C69/06 , C07C69/96 , C07C43/043
摘要： An efficient and environmentally beneficial method of recycling and producing methanol from varied sources of carbon dioxide including flue gases of fossil fuel burning powerplants, industrial exhaust gases or the atmosphere itself. Converting carbon dioxide by chemical or electrochemical reduction seconardy treatment to produce essentially methanol, dimethyl ether and derived products.
摘要翻译：一种从不同来源的二氧化碳回收和生产甲醇的有效和环保的方法，包括化石燃料燃烧发电厂，工业废气或大气本身的烟道气。通过化学或电化学还原仲胺处理来转化二氧化碳，主要生产甲醇，二甲醚和衍生产物。

68. 发明授权

US07608743B2 Efficient and selective chemical recycling of carbon dioxide to methanol, dimethyl ether and derived products 有权
标题翻译：二氧化碳对甲醇，二甲醚和衍生产物的高效选择性化学回收
公开(公告)号：US07608743B2
公开(公告)日：2009-10-27
申请号：US11766408
申请日：2007-06-21
申请人： George A. Olah , G. K. Surya Prakash
发明人： George A. Olah , G. K. Surya Prakash
IPC分类号： C07C29/51 , C07C29/15 , C07C29/132
CPC分类号： C07C29/136 , C07C1/20 , C07C29/04 , C07C29/14 , C07C29/141 , C07C29/149 , C07C41/09 , C07C51/15 , C07C67/08 , C07C67/38 , C07C68/005 , C07C68/02 , C25B3/04 , C07C31/08 , C07C31/04 , C07C31/10 , C07C11/02 , C07C53/02 , C07C69/06 , C07C69/96 , C07C43/043
摘要： An efficient and environmentally beneficial method of recycling and producing methanol from varied sources of carbon dioxide including flue gases of fossil fuel burning powerplants, industrial exhaust gases or the atmosphere itself. Converting carbon dioxide by chemical or electrochemical reduction secondary treatment to produce essentially methanol, dimethyl ether and derived products.
摘要翻译：一种从不同来源的二氧化碳回收和生产甲醇的有效和环保的方法，包括化石燃料燃烧发电厂，工业废气或大气本身的烟道气。通过化学或电化学还原二次处理将二氧化碳转化为基本上产生甲醇，二甲醚和衍生产物。

69. 发明授权

US07569513B2 Nickel and cobalt plated sponge catalysts 失效
标题翻译：镍和钴电镀海绵催化剂
公开(公告)号：US07569513B2
公开(公告)日：2009-08-04
申请号：US12148622
申请日：2008-04-21
申请人： Stephen Raymond Schmidt
发明人： Stephen Raymond Schmidt
IPC分类号： B01J23/00 , B01J21/00
CPC分类号： C10G2/332 , B01J23/883 , B01J23/8993 , B01J25/00 , B01J25/02 , B01J35/002 , B01J35/1014 , B01J37/0009 , B01J37/0225 , B01J37/0228 , B01J37/16 , B01J37/348 , C07C29/141 , C10G47/12 , C07C31/26
摘要： Novel nickel and/or cobalt plated sponge based catalysts are disclosed. The catalyst have an activity and/or selectivity comparable to conventional nickel and/or cobalt sponge catalysts, e.g., Raney® nickel or Raney® cobalt catalysts, but require a reduced content of nickel and/or cobalt. Catalysts in accordance with the invention comprise nickel and/or cobalt coated on at least a portion of the surface of a sponge support. Preferably, the sponge support comprises at least one metal other than or different from the metal(s) contained in the coating. The method of preparing the plated catalysts, and the method of using the catalysts in the preparation of organic compounds are also disclosed.
摘要翻译：公开了新型的镍和/或钴电镀的海绵基催化剂。该催化剂具有与常规的镍和/或钴海绵催化剂（例如，阮内镍催化剂）相当的活性和/或选择性，但要求镍和/或钴的含量降低。根据本发明的催化剂包括涂覆在海绵支撑体表面的至少一部分上的镍和/或钴。优选地，海绵支撑体包括除了包含在涂层中的金属以外的至少一种金属或不同于其的金属。还公开了制备电镀催化剂的方法，以及在制备有机化合物中使用催化剂的方法。

70. 发明授权

US07511178B2 Process of preparing ethylene glycol 失效
标题翻译：制备乙二醇的方法
公开(公告)号：US07511178B2
公开(公告)日：2009-03-31
申请号：US12208149
申请日：2008-09-10
申请人： Karina Quetzaly Almeida Leñero , Eit Drent , Roelof Van Ginkel , Robert Ian Pugh
发明人： Karina Quetzaly Almeida Leñero , Eit Drent , Roelof Van Ginkel , Robert Ian Pugh
IPC分类号： C07C31/18 , C07C29/14
CPC分类号： B01J31/2485 , B01J31/20 , B01J31/2234 , B01J2231/641 , B01J2231/648 , B01J2531/822 , C07C29/141 , C07C45/49 , C07C45/68 , C07F9/6571 , Y02P20/52 , C07C47/19 , C07C31/202
摘要： The invention provides a process of preparing glycolaldehyde by reacting formaldehyde with hydrogen and carbon monoxide in the presence of a catalyst composition which is based on, a) a source of rhodium, and b) a ligand of general formula R1P—R2(I), wherein R1 is a bivalent radical that together with the phosphorous atom to which it is attached is an optionally substituted 2-phospha-tricyclo[3.3.1.1{3,7}]-decyl group, wherein from 1 to 5 of the carbon atoms has been replaced by a heteroatom, and wherein R2 is a monovalent radical which is an optionally substituted hydrocarbyl group having from 1 to 40 carbon atoms; a catalyst composition of use in said process; and a process of preparing ethylene glycol from the glycolaldehyde thus prepared.
摘要翻译：本发明提供了一种通过甲醛与氢气和一氧化碳在催化剂组合物存在下制备乙二醇的方法，所述催化剂组合物基于a）铑源，和b）通式R 1 -P-R 2（I）的配体，其中R1是与其连接的磷原子一起是任选取代的2-磷杂三环[3.3.1.1 {3,7}] - 癸基的二价基团，其中1至5个碳原子具有被杂原子取代，并且其中R 2是一价基团，其是具有1至40个碳原子的任选取代的烃基; 在所述方法中使用的催化剂组合物; 以及由如此制备的乙二醇制备乙二醇的方法。

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