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61. 发明授权

US07951882B2 Catalyst composition comprising shuttling agent for higher olefin multi-block copolymer formation 有权
标题翻译：催化剂组合物包含用于高级烯烃多嵌段共聚物形成的穿梭剂
公开(公告)号：US07951882B2
公开(公告)日：2011-05-31
申请号：US10589379
申请日：2005-03-17
申请人： Daniel J. Arriola , Edmund M. Carnahan , David D. Devore , Phillip D. Hustad , Roger L. Kuhlman , Timothy T. Wenzel
发明人： Daniel J. Arriola , Edmund M. Carnahan , David D. Devore , Phillip D. Hustad , Roger L. Kuhlman , Timothy T. Wenzel
IPC分类号： C08F4/76 , C08F4/42
CPC分类号： C08F10/00 , C08F4/65908 , C08F4/65912 , C08F4/65925 , C08F4/65927 , C08F110/02 , C08F210/16 , C08F297/08 , C08F2410/04 , C08F2420/02 , C08L23/06 , C08L23/0815 , C08L23/0853 , Y10T428/24942 , Y10T428/24992 , Y10T428/2826 , Y10T428/31573 , Y10T428/31587 , Y10T442/60 , C08F4/65904 , C08F2/38 , C08L2666/06 , C08F2500/09 , C08F2500/03 , C08F210/14 , C08F2500/08 , C08F4/64193 , C08F4/64048 , C08F4/7006 , C08F4/6411 , C08F4/64113 , C08F4/64144
摘要： Copolymers, especially multi-block copolymer containing therein two or more segments or blocks differing in chemical or physical properties, are prepared by polymerizing propylene, 4-methyl-1-pentene, or other C4-8α-olefin and one or more copolymerizable comonomers, especially ethylene in the presence of a composition comprising the admixture or reaction product resulting from combining: (A) a first metal complex olefin polymerization catalyst, (B) a second metal complex olefin polymerization catalyst capable of preparing polymers differing in chemical or physical properties from the polymer prepared by catalyst (A) under equivalent polymerization conditions, and (C) a chain shuttling agent.
摘要翻译：通过聚合丙烯，4-甲基-1-戊烯或其它C 4-8α-烯烃和一种或多种可共聚共聚单体制备共聚物，特别是其中含有两个或更多个化学或物理性质不同的链段或嵌段的多嵌段共聚物，特别是乙烯在组合物存在下，该组合物包含通过混合得到的混合物或反应产物：（A）第一金属络合物烯烃聚合催化剂，（B）能够制备化学或物理性质不同的聚合物的第二金属络合物烯烃聚合催化剂在等同的聚合条件下由催化剂（A）制备的聚合物，和（C）链穿梭剂。

62. 发明申请

US20100016527A1 TETHERED SUPPORTED TRANSITION METAL COMPLEX 有权
标题翻译：全面支持的过渡金属复合材料
公开(公告)号：US20100016527A1
公开(公告)日：2010-01-21
申请号：US12529966
申请日：2008-03-05
申请人： Edmund M. Carnahan
发明人： Edmund M. Carnahan
IPC分类号： C08F4/52 , C08F2/00
CPC分类号： C08F10/00 , C08F4/659 , C08F4/025 , C08F4/64144
摘要： A supported metal complex comprising the reaction product of a transition metal complex of a polyvalent heteroaryl donor ligand containing at least one ortho-metallated aromatic ligand group and an ethylenically or poly(ethylenically) functionalized particulated organic or inorganic solid, a method for preparing the same and the use thereof as an addition polymerization catalyst.
摘要翻译：一种负载金属络合物，其包含含有至少一个邻金属化的芳族配体基团的多价杂芳基供体配体和烯属或聚（烯属）官能化的有机或无机固体的多价杂芳基供体配体的过渡金属络合物的反应产物，其制备方法及其作为加成聚合催化剂的用途。

63. 发明申请

US20090111944A1 PSEUDO-BLOCK COPOLYMERS AND PROCESS EMPLOYING CHAIN SHUTTLING AGENT 有权
公开(公告)号：US20090111944A1
公开(公告)日：2009-04-30
申请号：US11817344
申请日：2006-01-30
申请人： Roger L. Kuhlman , Timothy T. Wenzel , Daniel J. Arriola , Marilyn Bokota , Edmund M. Carnahan , Phillip D. Hustad , Pamela J. Stirn
发明人： Roger L. Kuhlman , Timothy T. Wenzel , Daniel J. Arriola , Marilyn Bokota , Edmund M. Carnahan , Phillip D. Hustad , Pamela J. Stirn
IPC分类号： C08F4/76
CPC分类号： C08F10/00 , C08F4/659 , C08F4/65908 , C08F4/6592 , C08F4/65927 , C08F210/06 , C08F210/16 , C08F297/06 , C08F297/08 , C08F297/083 , C08F2410/01 , C08L23/10 , C08L23/16 , C08L2308/00 , C08F4/65912 , C08F4/6465 , C08F2/38 , C08L2666/06 , C08F2500/17 , C08F2500/08 , C08F2500/20 , C08F2500/03 , C08F4/64048 , C08F4/64193 , C08F4/64144
摘要： A process for the polymerization of one or more addition polymerizable monomers to form a copolymer comprising multiple regions or segments of differentiated polymer composition or properties comprising contacting an addition polymerizable monomer or mixture of monomers under addition polymerization conditions with a composition comprising at least one olefin polymerization catalyst, a cocatalyst and a chain shuttling agent, said process being characterized by formation of at least some of the growing polymer chains under differentiated process conditions such that two or more blocks or segments formed within at least some of the resulting polymer are chemically or physically distinguishable.
摘要翻译：一种用于聚合一种或多种可加聚的单体以形成共聚物的方法，所述共聚物包含分化聚合物组合物或性质的多个区域或链段，包括在加成聚合条件下使加成聚合单体或单体混合物与包含至少一种烯烃聚合催化剂，助催化剂和链穿梭剂，所述方法的特征在于在不同的工艺条件下形成至少一些生长的聚合物链，使得在至少一些所得聚合物内形成的两个或多个嵌段或链段是化学或物理的可区分

64. 发明授权

US07491672B2 Chemically-modified supports and supported catalyst systems prepared therefrom 失效
标题翻译：由其制备的化学改性的载体和负载的催化剂体系
公开(公告)号：US07491672B2
公开(公告)日：2009-02-17
申请号：US11526242
申请日：2006-09-25
申请人： Edmund M. Carnahan , David R. Neithamer
发明人： Edmund M. Carnahan , David R. Neithamer
IPC分类号： B01J21/00
CPC分类号： B01J31/14 , B01J31/0239 , B01J31/0254 , B01J31/0268 , B01J31/0274 , C08F4/65908 , C08F4/65912 , C08F4/6592 , C08F10/00 , C08F210/16 , C08F4/65916 , C08F210/14
摘要： The present invention provides a chemically-modified support comprising an inorganic oxide containing optionally functionalized hydroxyl groups, having chemically linked thereto the cation of a cation/anion pair. The present invention further provides a supported catalyst system comprising the chemically-modified support as described above, and a transition metal compound of Groups 3-10 (preferably a Group 4 metal compound) containing at least one π-bonded anionic ligand group, said transition metal compound being capable of reacting with the chemically-modified support through the cation of the cation/anion pair to thereby render the transition metal compound catalytically active. The present invention further provides a process for preparing the chemically-modified support of the invention. The present invention further provides an addition polymerization process comprising contacting one or more addition polymerizable monomers with the supported catalyst system of the invention under addition polymerization conditions.
摘要翻译：本发明提供一种化学修饰的载体，其包含含有任选官能化羟基的无机氧化物，其与阳离子/阴离子对的阳离子化学连接。本发明进一步提供了一种载体催化剂体系，其包括如上所述的化学改性的载体和含有至少一个π键合的阴离子配体基团的3-10族（优选第4族金属化合物）的过渡金属化合物，所述转变金属化合物能够通过阳离子/阴离子对的阳离子与化学改性的载体反应，从而使过渡金属化合物具有催化活性。本发明还提供了制备本发明的化学改性载体的方法。本发明进一步提供加成聚合方法，其包括在加成聚合条件下使一种或多种可加聚的单体与本发明的负载型催化剂体系接触。

65. 发明申请

US20080269412A1 Catalytic Olefin Block Copolymers with Controlled Block Sequence Distribution 有权
标题翻译：具有受控块序列分布的催化烯烃嵌段共聚物
公开(公告)号：US20080269412A1
公开(公告)日：2008-10-30
申请号：US12066879
申请日：2006-09-14
申请人： Edmund M. Carnahan , Phillip D. Hustad , Roger L. Kuhiman , Timothy T. Wenzel
发明人： Edmund M. Carnahan , Phillip D. Hustad , Roger L. Kuhiman , Timothy T. Wenzel
IPC分类号： C08F297/00 , C08F2/01
CPC分类号： C08F297/08 , C08F4/659 , C08F4/65908 , C08F4/6592 , C08F4/65927 , C08F10/00 , C08F210/06 , C08F210/16 , C08F2410/01 , C08F4/65912 , C08F2/38 , C08F210/14 , C08F2500/03 , C08F2500/20 , C08F2500/12 , C08F2500/08 , C08F4/64048 , C08F4/64193 , C08F4/64148 , C08F4/64144 , C08F2/001
摘要： A process for the polymerization of one or more addition polymerizable monomers and the resulting polymer products, said process comprising: 1) contacting an addition polymerizable monomer or mixture of monomers under addition polymerization conditions in a reactor or reactor zone with a composition comprising at least one olefin polymerization catalyst and a cocatalyst and characterized by the formation of polymer chains from said monomer or monomers; 2) transferring the reaction mixture to a second reactor or reactor zone and optionally adding one or more additional reactants, catalysts, monomers or other compounds prior to, commensurate with, or after said transfer; and 3) causing polymerization to occur in said second reactor or reactor zone to form polymer chains that are differentiated from the polymer chains formed in step 1); said process being characterized by addition of a chain shuttling agent to the reaction mixture prior to, during, or subsequent to step 1) such that at least some of the resulting polymer molecules from step 3) comprise two or more chemically or physically distinguishable blocks or segments.
摘要翻译：一种用于聚合一种或多种可加聚单体和所得聚合物产物的方法，所述方法包括：1）在反应器或反应器区中的加成聚合条件下将加成聚合单体或单体混合物与包含至少一种烯烃聚合催化剂和助催化剂，其特征在于由所述单体或单体形成聚合物链; 2）将反应混合物转移到第二反应器或反应器区，并任选地在所述转移之前，之后或之后加入一种或多种另外的反应物，催化剂，单体或其它化合物; 和3）在所述第二反应器或反应器区域中引起聚合以形成与步骤1）中形成的聚合物链不同的聚合物链; 所述方法的特征在于在步骤1）之前，期间或之后向反应混合物中加入链穿梭剂，使得来自步骤3）的所得聚合物分子中的至少一些包含两个或多个化学或物理上可区分的嵌段或细分。

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