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61. 发明授权

US08071531B2 Flavor and fragrance composition 有权
标题翻译：香精和香精组成
公开(公告)号：US08071531B2
公开(公告)日：2011-12-06
申请号：US11922208
申请日：2006-06-20
申请人： Takashi Aida , Kenya Ishida
发明人： Takashi Aida , Kenya Ishida
IPC分类号： A61Q13/00 , A61K8/18 , A61K31/12 , C07C49/00
CPC分类号： A61Q19/00 , A23L2/56 , A23L27/203 , A61K8/35 , A61K2800/244 , A61Q5/02 , A61Q11/00 , A61Q19/10
摘要： A flavor and fragrance composition with a cooling sensation effect comprising 1-(2-hydroxy-4-methylcyclohexyl)ethanone represented by the formula (1). The flavor and fragrance composition is added to a beverage or food product, a fragrance or cosmetic product, a daily utensil product, an oral composition, or a pharmaceutical product in the range of 0.0001 to 20% by weight to the total weight of the flavor and fragrance composition added.
摘要翻译：具有由式（1）表示的1-（2-羟基-4-甲基环己基）乙酮的具有冷却感觉效果的风味和香料组合物。将香料和香料组合物加入饮料或食品，香料或化妆品，日用器具产品，口腔组合物或药物产品中，相对于风味剂的总重量为0.0001至20重量％并加入香料成分。

62. 发明授权

US07964637B2 Process for producing optically active theaspirane 失效
标题翻译：光学活性硅烷的制备方法
公开(公告)号：US07964637B2
公开(公告)日：2011-06-21
申请号：US11992067
申请日：2006-09-08
申请人： Makoto Harada , Hiroyuki Matsuda , Kenya Ishida , Yuichiro Yamazaki
发明人： Makoto Harada , Hiroyuki Matsuda , Kenya Ishida , Yuichiro Yamazaki
IPC分类号： A61K31/335 , C07D307/94
CPC分类号： C12P17/04 , A23L2/56 , A23L27/2052 , A61K8/4973 , A61Q19/00 , C07B53/00 , C07D307/94 , C11B9/0076 , C12P41/005
摘要： A simplified production method of stereoisomer of theaspiran having high optical purity has been desired. An alcohol compound having a specific skeleton is enantioselectively esterified with an enzyme, or an ester compound having a specific skeleton is enantioselectively hydrolyzed with an enzyme. The resultant optically active ester or optically active alcohol is used. Thus, optically active theaspiran having a desired configuration and having a high optical purity is obtained in a satisfactory yield.
摘要翻译：期望具有高光学纯度的阿司匹兰的立体异构体的简化制备方法。具有特定骨架的醇化合物用酶对映体选择性酯化，或者具有特定骨架的酯化合物用酶对映体选择性水解。使用所得光学活性酯或光学活性醇。因此，以令人满意的产率获得光学活性的具有所需构型并具有高光学纯度的阿司匹林。

63. 发明申请

US20110117147A1 COOLING SENSATION AGENT COMPOSITION AND SENSORY STIMULATION AGENT COMPOSITION 失效
标题翻译：冷却感觉剂组合物和感觉刺激剂组合物
公开(公告)号：US20110117147A1
公开(公告)日：2011-05-19
申请号：US12936160
申请日：2009-04-01
申请人： Kenya Ishida , Takashi Aida , Tetsuya Yamamoto
发明人： Kenya Ishida , Takashi Aida , Tetsuya Yamamoto
IPC分类号： A61K8/49 , A61K8/55 , A61Q11/00 , C07C69/96 , C07D317/22 , A61Q17/00 , A61K31/357
CPC分类号： C07D317/36 , A23L27/203 , A23L27/2052 , A61K8/0208 , A61K8/37 , A61K8/4973 , A61K2800/244 , A61Q5/02 , A61Q11/00 , A61Q13/00 , A61Q15/00 , A61Q19/00 , A61Q19/10 , C07C69/24 , C07C69/96 , C07C2601/14
摘要： The invention relates to a cooling sensation agent composition with a prolonged cool sensation effect comprising at least one compound selected from Formula (1) wherein each of A and B is a hydrogen atom or a hydrocarbon group which may have one or more substituents, in which A and B are not hydrogen atoms simultaneously, and the total number of carbon atoms in A and B is in the range of 6 to 18; and Formulae (2) to (4) wherein R1, R2, and R3 each represent a residue of an alcohol selected from 1-menthol, 1-isopulegol, 3-(1-menthoxy)propan-1,2-diol, 2-(1-menthoxy)ethan-1-ol, 3-(1-menthoxy)propan-1-ol, 2-methyl-3-(1-menthoxy)propan-1,2-diol and para-menthan-3,8-diol), and R4 represents a residue of a branched or straight-chain, cyclic or linear, or saturated or unsaturated alcohol having 6 to 18 carbon atoms that may have one or more aromatic rings that may have a condensed ring and substituent groups such as hydroxyl and ether groups; and R6 represents a hydrocarbon group having 11 to 19 carbon atoms that may be branched and contain one or more unsaturated bonds. The invention also relates to a sensory stimulation agent composition comprising the cooling sensation agent composition; a flavor or fragrance composition, a beverage or food product, a perfume or cosmetic product, a toiletry product, a daily utensil product or grocery, a fiber, a fiber product, a cloth or a medicine comprising the cooling sensation agent composition or the sensory stimulation agent composition; a production method thereof; a cooling processing method of a fiber, fiber product or a cloth, comprising compounding the cooling sensation agent composition or the sensory stimulation agent composition; and new compounds.
摘要翻译：本发明涉及具有延长的凉爽感觉效果的冷却感觉剂组合物，其包含至少一种选自式（1）的化合物，其中A和B各自为氢原子或可具有一个或多个取代基的烃基，其中 A和B不同时为氢原子，A和B中碳原子总数为6〜18; 和式（2）至（4）其中R 1，R 2和R 3各自表示选自1-薄荷醇，1-异胡耳醇，3-（1-薄荷氧基）丙-1,2-二醇，2- （1-薄荷氧基）乙-1-醇，3-（1-薄荷氧基）丙-1-醇，2-甲基-3-（1-薄荷氧基）丙-1,2-二醇和对 - 薄荷烷-3,8 - 二醇），R4代表具有6-18个碳原子的支链或直链，环状或直链或饱和或不饱和醇的残基，其可具有一个或多个可具有稠环的芳环和取代基如作为羟基和醚基团; R6表示可以具有支链并含有一个以上的不饱和键的碳原子数为11〜19的烃基。本发明还涉及包含冷却感觉剂组合物的感觉刺激剂组合物; 香料或香料组合物，饮料或食品，香水或化妆品，化妆品，日常用品或杂货，纤维，纤维制品，布或包含该冷却感觉组合物或感官的药物刺激剂组成; 其制造方法; 纤维，纤维制品或布的冷却处理方法，其包括将冷却感觉剂组合物或感觉刺激剂组合物混合; 和新化合物。

64. 发明申请

US20110105773A1 PRODUCTION METHOD OF (2E,6Z,8E)-N-ISOBUTYL-2,6,8-DECATRIENAMIDE (SPILANTHOL), AND FOOD OR DRINK, FRAGRANCE OR COSMETIC, OR PHARMACEUTICAL COMPRISING THE SAME 有权
标题翻译：（2E，6Z，8E）-N-ISOBUTYL-2,6,8-癸胺（SPILANTHOL）的生产方法，以及食品或饮料，香料或化妆品，或包含它们的药物
公开(公告)号：US20110105773A1
公开(公告)日：2011-05-05
申请号：US12673633
申请日：2009-01-16
申请人： Shigeru Tanaka , Kenji Yagi , Hideo Ujihara , Kenya Ishida
发明人： Shigeru Tanaka , Kenji Yagi , Hideo Ujihara , Kenya Ishida
IPC分类号： C07C235/28 , C07C231/02 , C07C231/12 , C07C57/66 , C07C43/303
CPC分类号： A61K8/42 , A23G1/32 , A23G3/36 , A23G4/06 , A23L27/202 , A61Q5/00 , A61Q11/00 , A61Q15/00 , C07C43/303 , C07C45/41 , C07C57/66 , C07C231/12 , C07C233/09 , C07C235/28 , C07C309/66 , C12P13/02 , C07C47/21
摘要： A problem as an object of the invention is to provide a production method of spilanthol in a large scale without using expensive reagents. The present invention provides a production method of N-isobutyl-2,6,8-decatrienamide, wherein a column chromatography purification step is not required in all processes.
摘要翻译：作为本发明的目的的一个问题是在不使用昂贵的试剂的情况下大规模地提供大量的生产方法。本发明提供N-异丁基-2,6,8-癸三酰胺的制备方法，其中在所有方法中不需要柱色谱纯化步骤。

65. 发明申请

US20110077309A1 HUMECTANT COMPOSITION 审中-公开
标题翻译：成分组成
公开(公告)号：US20110077309A1
公开(公告)日：2011-03-31
申请号：US12959670
申请日：2010-12-03
申请人： Tetsuya Yamamoto , Kenya Ishida
发明人： Tetsuya Yamamoto , Kenya Ishida
IPC分类号： A61K47/42 , A61K47/10 , A61K47/14 , A61K47/22 , A61K47/36 , A61K47/46 , A61Q5/12 , A61Q19/00 , A61P17/00 , A61K8/33 , A61Q13/00
CPC分类号： A61K8/345 , A61Q5/00 , A61Q5/02 , A61Q5/12 , A61Q13/00 , A61Q19/00 , A61Q19/10
摘要： The present invention relates to a humectant composition containing, as component (A), at least one member selected from a menthol derivative represented by the following formula (1) and p-menthane-3,8-diol: in which R is an alkylene group having 2 to 5 carbon atoms which may be substituted with at least one member selected from the group consisting of a methyl group and a hydroxyl group, and n is an integer of 1 to 3. The humectant composition of the present invention provides an excellent moisture-retention effect.
摘要翻译：本发明涉及作为组分（A）的至少一种选自由下式（1）表示的薄荷醇衍生物和对 - 薄荷烷-3,8-二醇中的至少一种的组合物：其中R是亚烷基具有2至5个碳原子的基团，其可以被选自甲基和羟基中的至少一种取代，n是1至3的整数。本发明的保湿组合物提供优异的保湿效果。

66. 发明申请

US20100280110A1 (3R)-L-MENTHYL 3-HYDROXYBUTYRATE, PROCESS FOR PRODUCING THE SAME, AND SENSATE COMPOSITION COMPRISING THE SAME 失效
标题翻译：（3R）-L-戊烯3-羟基丁酸酯，其制备方法以及含有它们的感官组合物
公开(公告)号：US20100280110A1
公开(公告)日：2010-11-04
申请号：US12766162
申请日：2010-04-23
申请人： Kazuma HOJO , Takashi AIDA , Kenya ISHIDA
发明人： Kazuma HOJO , Takashi AIDA , Kenya ISHIDA
IPC分类号： A61K8/37 , C07C69/675 , A61K31/22 , A61P43/00 , A61Q90/00 , A23L1/226 , A61K8/365 , A61Q19/10 , A61Q13/00 , A61Q5/02
CPC分类号： C11B9/0034 , A23L2/56 , A23L27/203 , A61K8/37 , A61K31/22 , A61K2800/244 , A61Q5/02 , A61Q13/00 , A61Q19/00 , A61Q19/10 , C07B2200/07 , C07C67/31 , C07C69/675 , C07C2601/14
摘要： The present invention provides a cooling component or sensate component which has further strong cooling intensity and is excellent in the persistency or refresh-feeling and cool-feeling, a sensate composition comprising the same, and various products comprising the sensate composition. The present invention relates to, as a cooling component or sensate component, (3R)-1-menthyl 3-hydroxybutyrate represented by the following formula (I):
摘要翻译：本发明提供一种冷却组分或感觉组分，其具有更强的冷却强度，并且具有优异的持久性，刷新感和凉爽感，含有该组合物的感觉组合物和包含感觉组合物的各种产品。本发明涉及作为冷却成分或感官成分的由下式（I）表示的（3R）-1-薄荷基3-羟基丁酸酯：

67. 发明申请

US20090216039A1 Method for Producing Optically Active Alpha-Ionone 有权
标题翻译：生产光学活性α-紫罗兰酮的方法
公开(公告)号：US20090216039A1
公开(公告)日：2009-08-27
申请号：US11991966
申请日：2006-09-13
申请人： Tetsuya Yamamoto , Kenji Yagi , Kenya Ishida
发明人： Tetsuya Yamamoto , Kenji Yagi , Kenya Ishida
IPC分类号： C12P7/26 , C07C69/75 , C07C45/42
CPC分类号： C12P7/26 , A23L2/56 , A23L27/204 , A61K8/37 , A61Q11/00 , A61Q13/00 , C07B53/00 , C07B2200/07 , C07C403/08 , C07C403/12 , C07C403/14 , C07C2601/16 , C12G3/06 , C12P41/004
摘要： Provided that a method for inexpensively producing optically active α-ionone with a high yield and a high asymmetric yield and with good workability in a short process, and a perfume composition comprising the optically active α-ionone obtained by the aforementioned method. A method for producing optically active α-ionone, comprising allowing α-ionone as a mixture of optical isomers to react with an esterification agent, and hydrolyzing the obtained α-ionone enol ester; a method for producing optically active α-ionone comprising subjecting α-ionone as a mixture of optical isomers to an asymmetric reduction, allowing the obtained optically active α-ionol to react with an esterification agent to give an optically active α-ionol ester, hydrolyzing the obtained optically active α-ionol ester after purification as necessary, and then oxidizing the obtained optically active α-ionol; and a perfume composition comprising thus obtained optically active α-ionone.
摘要翻译：本发明提供了一种低成本地生产光学活性α-紫罗兰酮的方法，其具有高产率和高不对称产率，并且在短时间内具有良好的可加工性，以及包含通过上述方法获得的光学活性α-紫罗兰酮的香料组合物。一种光学活性α-紫罗兰酮的制造方法，其特征在于，使作为光学异构体的混合物的α-紫罗兰酮与酯化剂反应，水解得到的α-紫罗兰酮烯醇酯; 制备光学活性α-紫罗兰酮的方法，包括将α-紫罗烯酮作为光学异构体的混合物进行不对称还原，使得到的光学活性α-离子酚与酯化反应得到光学活性α-离子醇酯，水解根据需要纯化后得到的光学活性α-离子醇酯，然后氧化得到的光学活性α-离子醇; 和包含由此获得的光学活性α-紫罗兰酮的香料组合物。

68. 发明申请

US20090198070A1 Condensation Reaction by Metal Catalyst 有权
标题翻译：金属催化剂的缩合反应
公开(公告)号：US20090198070A1
公开(公告)日：2009-08-06
申请号：US12085988
申请日：2006-12-04
申请人： Kazushi Mashima , Takashi Ohshima , Takanori Iwasaki , Hironori Maeda , Kenya Ishida
发明人： Kazushi Mashima , Takashi Ohshima , Takanori Iwasaki , Hironori Maeda , Kenya Ishida
IPC分类号： C07F15/00 , C07D263/08 , C07D263/52
CPC分类号： C07D263/12 , B01J31/2226 , B01J2531/26 , C07C53/18 , C07C231/02 , C07C253/30 , C07D263/10 , C07D263/14 , C07D263/52 , C07D413/06 , C07F3/003 , C07F7/1892 , C07F9/5022 , C07K1/088 , C07K1/10
摘要： The invention relates to a method for producing an azoline compound represented by the general formula (3): wherein R1 represents an optionally substituted hydrocarbon group, an optionally substituted alkoxy group, an optionally substituted alkoxycarbonyl group, a halogen atom, a substituted amino group, a substituted carbamoyl group or an optionally substituted heterocyclic group; R3, R4, R5 and R6 may be the same or different and each represents a hydrogen atom, an optionally substituted hydrocarbon group, an optionally substituted alkoxy group, an optionally substituted alkoxycarbonyl group, a halogen atom, a substituted amino group, a substituted carbamoyl group or an optionally substituted heterocyclic group; two arbitrary groups selected from R3, R4, R5 and R6 may bond to each other to form a ring; and Z1 represents an oxygen atom, a sulfur atom or a selenium atom; comprising reacting a carboxylic acid or a carboxylic acid derivative represented by the general formula (1): R1CO2R2 (1) wherein R1 is as defined above; R2 represents a hydrogen atom, an optionally substituted alkyl group or an optionally substituted aryl group; and R1 and R2 may bond to each other to form a ring; with an aminochalcogenide represented by the general formula (2): wherein R3, R4, R5, R6 and Z1 are as defined above; in the presence of a compound containing a group 12 metal element in the periodic table.
摘要翻译：本发明涉及一种制备由通式（3）表示的唑啉化合物的方法：其中R1表示任选取代的烃基，任选取代的烷氧基，任选取代的烷氧基羰基，卤素原子，取代的氨基，取代的氨基甲酰基或任选取代的杂环基; R3，R4，R5和R6可以相同或不同，各自表示氢原子，任选取代的烃基，任选取代的烷氧基，任选取代的烷氧基羰基，卤素原子，取代的氨基，取代的氨基甲酰基基团或任选取代的杂环基团; 选自R3，R4，R5和R6中的两个任意基团可以彼此键合形成环; Z1表示氧原子，硫原子或硒原子; 包括使由通式（1）表示的羧酸或羧酸衍生物反应：<？in-line-formula description =“In-line formula”end =“lead”？> R1CO2R2（1）<？ -formulae description =“In-line Formulas”end =“tail”？>其中R1如上定义; R2表示氢原子，任选取代的烷基或任选取代的芳基; 并且R 1和R 2可以彼此键合形成环; 与通式（2）表示的氨基硫族化物：其中R3，R4，R5，R6和Z1如上定义; 在含有元素周期表中第12族金属元素的化合物存在下进行。

69. 发明申请

US20070225378A1 Menthol Dearivative and Cooling Agent Composition Comprising the Same 有权
标题翻译：薄荷醇衍生物和冷却剂组合物组成
公开(公告)号：US20070225378A1
公开(公告)日：2007-09-27
申请号：US11628086
申请日：2004-05-31
申请人： Kenya Ishida , Takashi Aida , Hiroyuki Matsuda , Fumihiro Yanaka
发明人： Kenya Ishida , Takashi Aida , Hiroyuki Matsuda , Fumihiro Yanaka
IPC分类号： C07C43/196 , C07C43/184
CPC分类号： A61K8/39 , A61K2800/244 , A61Q5/02 , A61Q11/00 , A61Q13/00 , A61Q19/00 , A61Q19/10 , C07C43/196 , C07C2601/14
摘要： The invention relates to innovative menthol derivatives which are represented by the general formula (I) below and are excellent in a cooling effect and cool retaining effect, cooling agent compositions comprising the menthol derivatives, and sensory stimulation agent compositions containing the cooling agent compositions, as well as fragrance compositions, beverage or food products, cosmetic products, toiletry products, bathing agents, and pharmaceutical products containing the cooling agent compositions or sensory stimulation agent compositions. (general formula (I)) wherein R represents a hydrogen atom, an alkyl group having 1 to 4 carbon atoms, or an acyl group having 1 to 5 carbon atoms; R and R independently represent an alkylene group having 2 to 5 carbon atoms and optionally having a substituent; double dotted line represents a single bond or a double bond; and n is an integer of 1 to 3.
摘要翻译：本发明涉及由以下通式（I）表示并具有优异的冷却效果和冷保持效果的创新薄荷醇衍生物，包含薄荷醇衍生物的冷却剂组合物和含有冷却剂组合物的感觉刺激剂组合物，如以及香料组合物，饮料或食品，化妆品，化妆品，洗浴剂和含有冷却剂组合物或感觉刺激剂组合物的药物制品。（通式（I））其中R 1表示氢原子，具有1至4个碳原子的烷基或具有1至5个碳原子的酰基; R 2和R 3独立地表示具有2至5个碳原子并且任选具有取代基的亚烷基; 双点划线表示单键或双键; n为1〜3的整数。

70. 发明授权

US07196052B2 Fragrance composition 有权
标题翻译：香料组成
公开(公告)号：US07196052B2
公开(公告)日：2007-03-27
申请号：US10369520
申请日：2003-02-21
申请人： Kenya Ishida , Kenji Arata , Kenji Maruyama
发明人： Kenya Ishida , Kenji Arata , Kenji Maruyama
IPC分类号： A61K8/18
CPC分类号： A61Q13/00 , A61K8/345 , C11B9/0015
摘要： A fragrance composition having high fragrance properties such as fragrance diffusivity and long-lasting property obtained without changing the fragrance note of the fragrance composition which is useful in various fragrance providing products such as cosmetics, toiletry products, bath compositions and pharmaceuticals having satisfactory fragrance properties such as fragrance diffusivity and long-lasting property. The fragrance composition contains 0.1 to 90% by weight of a glyceryl ether derivative represented by the following general formula (I), such as 2-ethylhexyloxypropanediol as a fixative or fragrance note-improving agent. The fragrance-providing product contains 0.01 to 50% by weight of the fragrance composition in the final product composition. General formula (I) is: wherein R1 represents an aliphatic hydrocarbon group having 4 to 12 carbon atoms which may have a branched chain or an aromatic hydrocarbon group, which may have a substituent.
摘要翻译：具有高芳香性的香料组合物，其香味扩散性和持久性优异，而不改变香料组合物的香味，可用于各种香料提供产品如化妆品，化妆品，浴组合物和具有令人满意的香料性能的药物如作为香味的扩散性和持久性。芳香剂组合物含有0.1〜90重量％的由以下通式（I）表示的甘油醚衍生物，例如作为固定剂或香味促进剂的2-乙基己基氧基丙二醇。提供香料的产品在最终产品组合物中含有0.01至50重量％的香料组合物。通式（I）是：

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