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    • 52. 发明授权
    • Process for the production of a lubricating oil additive concentrate
    • 用于生产润滑油添加剂浓缩物的方法
    • US5437803A
    • 1995-08-01
    • US96061
    • 1993-07-22
    • Charles CaneJohn CrawfordPatrick S. O'Connor
    • Charles CaneJohn CrawfordPatrick S. O'Connor
    • C10M125/10C10M125/14C10M125/18C10M129/08C10M129/10C10M129/16C10M129/38C10M129/54C10M129/70C10M135/10C10M159/12C10M159/20C10M159/22C10M159/24C10M177/00C10N10/04C10N20/02C10N40/25C10N70/00
    • C10M159/24C10M159/12C10M159/20C10M159/22
    • A process for the production of a lubricating oil additive concentrate which process comprises reacting at elevated temperaturecomponent (A) a defined acid or derivative thereof,component (B) a calcium base added either in a single addition or in a plurality of additions at intermediate points during the reaction,component (C) at least one compound which is (i) water, (ii) a polyhydric alcohol having 2 to 4 carbon atoms, (iii) a di- (C.sub.3 or C.sub.4) glycol, (iv) a tri (C.sub.2 -C.sub.4) glycol, (v) a mono- or poly-alkylene glycol alkyl ether of the formula (I)R(OR.sup.1).sub.x OR.sup.2 (I) wherein R is a C.sub.1 to C.sub.6 alkyl group, R.sup.1 is an alkylene group, R.sup.2 is hydrogen or a C.sub.1 to C.sub.6 alkyl group and x is an integer from 1 to 6, (vi) a C.sub.1 to C.sub.20 monohydric alcohol, (vii) a C.sub.1 to C.sub.20 ketone, (viii) a C.sub.1 to C.sub.10 carboxylic acid ester, or (ix) a C.sub.1 to C.sub.20 ether,component (D) a lubricating oil,component (E) a defined carboxylic acid or derivative in an amount up to 60% by weight of the total weight of component (A) and component (E), said total weight of component (A) and component (E) being that required to satisfy an equivalent ratio of component (B) to component (A) plus component (E) of not greater than one.
    • 一种用于生产润滑油添加剂浓缩物的方法,该方法包括在升高的温度下使组分(A)与所定义的酸或其衍生物,组分(B)在中间加入或加入多个添加物中的钙碱 (C)至少一种化合物,其为(i)水,(ii)具有2至4个碳原子的多元醇,(iii)二(C 3或C 4)二醇,(iv) 三(C 2 -C 4)二醇,(v)式(I)R(OR 1)x OR 2(I)的单 - 或多 - 亚烷基二醇烷基醚,其中R是C1至C6烷基,R1是亚烷基 ,R2为氢或C1〜C6烷基,x为1〜6的整数,(vi)C1〜C20一元醇,(vii)C1〜C20酮,(viii)C1〜C10羧酸酯 ,或(ix)C1至C20醚,组分(D)润滑油,组分(E)定量的羧酸或衍生物,其量高达组分(A)和化合物(A)的总重量的60重量% 组分(A)和组分(E)的总重量是组分(B)与组分(A)的加入量与组分(E)的当量比不大于1所需的总重量。
    • 54. 发明授权
    • Lubricant compositions
    • 润滑剂组合物
    • US4434063A
    • 1984-02-28
    • US291059
    • 1981-08-07
    • Hachiro KageyamaTsutomu MoriuchiYoshiaki Oikawa
    • Hachiro KageyamaTsutomu MoriuchiYoshiaki Oikawa
    • C10M103/06C10M125/10
    • C10M125/10C10M103/06C10M2201/062
    • A novel lubricant composition is disclosed, which contains not less than 0.1% by weight of at least one calcium ferrite having the following general formula:Ca.sub.x Fe.sub.y O.sub.x+(3/2)ywherein x is 1 or 2 and y is 2 or 4, provided that y is 2 or 4 when x is 1, and y is 2 when x is 2. The calcium ferrites may be monocalcium ferrite, dicalcium ferrite or hemicalcium ferrite, produced by mixing iron oxide and a calcium compound in a molar ratio of 1:0.5 to 1:2 and fusing them by heating at a temperature of 1200.degree.-1400.degree. C. The resultant material contains not more than 5% by weight of the whole, of ferric oxide, silica and alumina as impurities. The calcium ferrites have a maximum particle size of 100.mu., preferably 0.15.mu.. They can be used as such for lubricant purposes, or can be incorporated in a lubricating oil or grease, such as a mineral oil, in an amount more than 0.1% by weight and preferably more than 1% by weight.
    • 公开了一种新颖的润滑剂组合物,其含有不少于0.1重量%的至少一种具有以下通式的钙铁氧体:CaxFeyOx +(3/2)y,其中x为1或2,y为2或4,条件是 当x为1时,y为2或4,x为2时y为2。铁酸钙可以是摩尔比为1:0.5,通过混合氧化铁和钙化合物而制备的铁素体铁素体,铁素体铁素体或铁素体铁素体 至1:2,并在1200-140℃的温度下加热熔融。所得材料含有不超过5重量%的氧化铁,二氧化硅和氧化铝作为杂质。 钙铁氧体的最大粒径为100微米,优选为0.15微米。 它们可以原样用于润滑剂目的,或者可以以超过0.1重量%,优选大于1重量%的量掺入润滑油或润滑脂如矿物油中。