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51. 发明授权

US4098749A Anticorrosion primer coating composition 失效
标题翻译：防腐底漆涂料组合物
公开(公告)号：US4098749A
公开(公告)日：1978-07-04
申请号：US780994
申请日：1977-03-24
申请人： Minoru Hoshino , Toshio Shinohara , Yukio Kawahara , Katsuji Takase , Toshimoto Tsuji , Jun-ichi Fukuda
发明人： Minoru Hoshino , Toshio Shinohara , Yukio Kawahara , Katsuji Takase , Toshimoto Tsuji , Jun-ichi Fukuda
IPC分类号： C09D5/12 , C09D129/14 , C08J3/00 , C08K3/18 , C08K5/49 , C09D5/08
CPC分类号： C09D5/12 , C08K3/32 , C08K3/38 , C08K5/54 , C09D129/14
摘要： The present invention relates to an anticorrosion primer coating composition comprising (i) a polyvinyl butyral resin, (ii) an organo functional silane, (iii) at least one member selected from the group consisting of inorganic borate compounds and polyphosphate compounds, and (iv) phosphoric acid.
摘要翻译：本发明涉及一种防腐底漆涂料组合物，其包含（i）聚乙烯醇缩丁醛树脂，（ii）有机官能硅烷，（iii）至少一种选自无机硼酸盐化合物和多磷酸盐化合物的组分，和（iv ）磷酸。

52. 发明授权

US4033991A Method for preparing organosilanes containing silicon-bonded oxime groups 失效
标题翻译：制备含硅键肟基团的有机硅烷的方法
公开(公告)号：US4033991A
公开(公告)日：1977-07-05
申请号：US643812
申请日：1975-12-23
申请人： Toshio Shinohara , Masatoshi Arai
发明人： Toshio Shinohara , Masatoshi Arai
IPC分类号： C07F7/10 , C07F7/08 , C08L83/04
CPC分类号： C07F7/0892 , C08K5/54 , C08G77/06
摘要： Organosilanes containing silicon-bonded oxime groups, i.e., ketoximosilanes, are prepared by reacting an halogenosilane with an alkali metal oxime, using no acid acceptors. This method of preparation is safe from the potentiality of explosive hazards that may exist inadvertently or inherently in the conventional reaction system, and also capable of producing amine chloride-free products.
摘要翻译：含有硅键合肟基的有机硅烷，即酮肟基硅烷，通过卤代硅烷与碱金属肟反应，不使用酸受体来制备。这种制备方法可以避免常规反应体系中无意中或固有地存在的爆炸危险的潜力，并且还能够生产无氯化胺的产物。

53. 发明授权

US06984748B2 Co-catalyst and process for the preparation of organohalosilanes 有权
公开(公告)号：US06984748B2
公开(公告)日：2006-01-10
申请号：US10119146
申请日：2002-04-10
申请人： Mikio Aramata , Hideaki Ozeki , Akio Muraida , Susumu Ueno , Toshio Shinohara , Tetsuya Inukai
发明人： Mikio Aramata , Hideaki Ozeki , Akio Muraida , Susumu Ueno , Toshio Shinohara , Tetsuya Inukai
IPC分类号： C07F7/16
CPC分类号： C07F7/16
摘要： In a Rochow process, organohalosilanes are prepared by reacting metallic silicon particles with an organohalide in the presence of a copper catalyst and a co-catalyst. The invention uses as the co-catalyst a powder of co-catalyst active element-copper alloy containing substantial strain energy because this co-catalyst can reduce the activation time taken until a steady state is reached, which has been an outstanding problem in Rochow reaction, maintain the steady state over time and increase the selectivity of desired diorganodihalosilane for eventually increasing the yield based on the starting silicon.

54. 发明授权

US06395917B1 Preparation of organohalosilanes 有权
标题翻译：有机硅烷的制备
公开(公告)号：US06395917B1
公开(公告)日：2002-05-28
申请号：US09981822
申请日：2001-10-19
申请人： Hajime Ishizaka , Susumu Ueno , Toshio Shinohara , Yoichi Tanifuji , Tetsuya Inukai , Mikio Aramata
发明人： Hajime Ishizaka , Susumu Ueno , Toshio Shinohara , Yoichi Tanifuji , Tetsuya Inukai , Mikio Aramata
IPC分类号： C07F716
CPC分类号： C07F7/16
摘要： When oganohalosilanes are prepared by charging a reactor with a contact mass containing a metallic silicon powder, a copper catalyst and a co-catalyst, and introducing an organohalide-containing gas into the reactor to effect the direct reaction, the catalyst and/or co-catalyst used in the contact mass is obtained by mixing particles of the catalyst and/or co-catalyst with finely divided silica, and applying shear forces to the mixture for mutually rubbing the particles, thereby producing the catalyst and/or co-catalyst having finely divided silica fused to surfaces thereof. The invention is successful in producing organohalosilanes at a significantly improved formation rate without reducing the proportion of diorganodihalosilane.
摘要翻译：当通过向包含金属硅粉末，铜催化剂和助催化剂的接触物质装入反应器并且将含有机卤化物的气体引入反应器以进行直接反应来制备原料卤代硅烷时，催化剂和/ 通过将催化剂和/或助催化剂的颗粒与细碎的二氧化硅混合，并向混合物施加剪切力以相互摩擦颗粒而获得催化剂，从而制备具有细小的催化剂和/或助催化剂的催化剂和/或助催化剂分开的二氧化硅与其表面融合。本发明成功地以显着提高的形成速率生产有机卤代硅烷，而不降低二有机二卤代硅烷的比例。

55. 发明授权

US06365766B1 Metallic copper catalyst and process for the synthesis of organohalosilanes 有权
标题翻译：金属铜催化剂及合成有机卤代硅烷的方法
公开(公告)号：US06365766B1
公开(公告)日：2002-04-02
申请号：US09548427
申请日：2000-04-12
申请人： Mikio Aramata , Masaaki Furuya , Yoshihiro Shirota , Akio Muraida , Susumu Ueno , Toshio Shinohara
发明人： Mikio Aramata , Masaaki Furuya , Yoshihiro Shirota , Akio Muraida , Susumu Ueno , Toshio Shinohara
IPC分类号： C07F716
CPC分类号： C07F7/16 , B01J23/72 , B01J35/023 , B22F1/0011
摘要： Organohalosilanes are prepared by reacting an organic halide with metallic silicon particles in the presence of a metallic copper catalyst which is a metallic copper powder in flake form having a bulk specific gravity of 1-3 g/cm3 and a mean particle size of 10 &mgr;m to 1 mm as measured by laser diffraction particle size distribution analysis.
摘要翻译：有机卤代硅烷通过在金属铜催化剂的存在下使有机卤化物与金属硅颗粒反应来制备，金属铜催化剂是片状比重为1-3g / cm 3，平均粒径为10〜通过激光衍射粒度分布分析测量为1mm。

56. 发明授权

US06353274B1 Mounting structure of rotary shaft of rotary electric machinery 有权
标题翻译：旋转电机旋转轴安装结构
公开(公告)号：US06353274B1
公开(公告)日：2002-03-05
申请号：US09577278
申请日：2000-05-23
申请人： Toshiki Ogawara , Toshio Shinohara , Michihiro Suzuki
发明人： Toshiki Ogawara , Toshio Shinohara , Michihiro Suzuki
IPC分类号： H02K500
CPC分类号： F04D29/059 , F16C25/083 , F16C35/063 , F16C2360/46 , H02K5/1735
摘要： The present invention provides a mounting structure of a rotary shaft of rotary electric machinery in which it is possible to cope with vibration of the rotary shaft in an axial direction with a low parts count. A fitting groove into which a portion of a rear side stopper is fitted is formed at a rear end portion of the rotary shaft. A rear side stopper has three projecting chips fitted into the fitting groove and three leaf spring chips in contact with an inner ring of a rolling bearing forming a bearing structure. The rear side stopper has a structure in which the rear side stopper generates spring force for restoring an original shape thereof when the rear side stopper is compressed in an axial direction of the rotary shaft. The rear side stopper is disposed in a compressed state between a wall face surrounding the fitting groove and the inner ring of the rolling bearing.
摘要翻译：本发明提供一种旋转电机的旋转轴的安装结构，其中可以以低的零件数量在轴向方向上应对旋转轴的振动。在旋转轴的后端部形成有嵌合有后侧止动件的一部分的嵌合槽。后侧止动件具有装配到装配槽中的三个突出的芯片和与形成轴承结构的滚动轴承的内圈接触的三个板簧片。后侧止动件具有后侧止动器在旋转轴的轴向被压缩时产生用于恢复其原始形状的弹簧力的结构。后侧挡块以压缩状态设置在围绕嵌合槽的壁面与滚动轴承的内圈之间。

57. 发明授权

US5473037A Method of producing dimethylpolysiloxanes 失效
标题翻译：生产二甲基聚硅氧烷的方法
公开(公告)号：US5473037A
公开(公告)日：1995-12-05
申请号：US291067
申请日：1994-08-17
申请人： Kunio Itoh , Toshio Shinohara , Hiroaki Kizaki , Shoichi Tanaka , Yukinori Satou , Kazunobu Umemura
发明人： Kunio Itoh , Toshio Shinohara , Hiroaki Kizaki , Shoichi Tanaka , Yukinori Satou , Kazunobu Umemura
IPC分类号： C07F7/08 , C08G77/04 , C08G77/06 , C08G77/08
CPC分类号： C08G77/045 , C07F7/0874 , C08G77/06
摘要： Disclosed is a method of producing dimethylpolysiloxanes through hydrolysis of dimethyldichlorosilane wherein a water solution containing a water-soluble oxygen-containing organic compound is introduced into dimethyldichlorosilane. Therein, linear dimethylpolysiloxanes alone having both ends blocked with chlorine atoms can be selectively produced by properly controlling the water content in the hydrolysis system and further by rendering the hydrolysis system acidic, and cyclic dimethylpolysiloxanes alone can also be selectively produced by properly controlling the water content in the hydrolysis system and optionally rendering the hydrolysis system acidic.
摘要翻译：公开了通过水解二甲基二氯硅烷生产二甲基聚硅氧烷的方法，其中将含有水溶性含氧有机化合物的水溶液引入二甲基二氯硅烷中。其中，通过适当地控制水解体系中的水分含量和进一步使水解体系成为酸性，单独具有两端被氯原子封端的直链二甲基聚硅氧烷可以选择性地制备，单独的环状二甲基聚硅氧烷也可以通过适当地控制水含量在水解系统中并且任选地使水解体系呈酸性。

58. 发明授权

US5130461A 1,3-bis(p-hydroxybenzyl)-1,1,3,3-tetramethyldisiloxane and method for making 失效
标题翻译： 1,3-双（对羟基苄基）-1,1,3,3-四甲基二硅氧烷及其制备方法
公开(公告)号：US5130461A
公开(公告)日：1992-07-14
申请号：US710478
申请日：1991-06-05
申请人： Toshio Shinohara , Makoto Satoh
发明人： Toshio Shinohara , Makoto Satoh
IPC分类号： C07F7/08 , C07F7/18
CPC分类号： C07F7/0852
摘要： There is provided a novel organosilicon compound, 1,3-bis(p-hydroxybenzyl)-1,1,3,3-tetramethyldisiloxane. It is prepared by silylating 1,3-bis(p-methoxybenzyl)-1,1,3,3-tetramethyldisiloxane with trimethylsilyl iodide, followed by desilylation.
摘要翻译：提供了一种新的有机硅化合物，1,3-双（对羟基苄基）-1,1,3,3-四甲基二硅氧烷。通过用三甲基甲硅烷基碘使1,3-双（对甲氧基苄基）-1,1,3,3-四甲基二硅氧烷甲硅烷基化，然后脱甲硅烷化来制备。

59. 发明授权

US5013768A Photopolymerizable coating composition and process for forming a coating having a stereoscopic pattern 失效
标题翻译：可光聚合涂料组合物和用于形成具有立体图案的涂层的方法
公开(公告)号：US5013768A
公开(公告)日：1991-05-07
申请号：US152587
申请日：1989-12-19
申请人： Yoshiyuki Kiriyama , Kazuyuki Moriga , Toshio Shinohara , Mitsuhiro Matsuda , Hiromi Maeda
发明人： Yoshiyuki Kiriyama , Kazuyuki Moriga , Toshio Shinohara , Mitsuhiro Matsuda , Hiromi Maeda
IPC分类号： C08F2/44 , C08F290/06
CPC分类号： C08F290/067
摘要： A photopolymerizable coating composition comprising:(A) 100 parts by weight of a vehicle consisting essentially of a urethaneacrylate oligomer;(B) from 0.1 to 5 parts by weight of an acylphosphine oxide compound as a photoinitiator;(C) from 1 to 100 parts by weight of a color pigment; and(D) from 20 to 300 parts by weight of a transparent glass powder having an average particle size of not larger than 100 .mu.m and an index of refraction which does not differ more than 0.3 from the index of refraction of the composition excluding the color pigment.
摘要翻译：一种可光聚合涂料组合物，其包含：（A）100重量份的基本上由氨基甲酸酯丙烯酸酯低聚物组成的载体; （B）0.1〜5重量份作为光引发剂的酰基氧化膦化合物; （C）1〜100重量份的着色颜料; 和（D）20〜300重量份的平均粒径不大于100μm的透明玻璃粉末，折射率与折射率之差不超过0.3的折射率不超过0.3 彩色颜料。

60. 发明授权

US4957607A Method for the preparation of a cycloalkyl silane compound 失效
标题翻译：环烷基硅烷化合物的制备方法
公开(公告)号：US4957607A
公开(公告)日：1990-09-18
申请号：US380350
申请日：1989-07-17
申请人： Mikio Endo , Minoru Takamizawa , Toshinobu Ishihara , Tohru Kubota , Toshio Shinohara
发明人： Mikio Endo , Minoru Takamizawa , Toshinobu Ishihara , Tohru Kubota , Toshio Shinohara
IPC分类号： C07F7/12 , C07B61/00 , C07F7/08 , C07F7/14 , C07F7/18
CPC分类号： C07F7/0801 , C07F7/14 , C07F7/1876
摘要： Cycloalkyl silane compounds such as cyclohexyl methyl dichlorosilane can be efficiently prepared by the photochemically induced hydrosilylation reaction. For example, an equimolar mixture of cyclohexene and methyl dichlorosilane with admixture of a catalytic amount of a platinum catalyst, which is an alcohol complex of chloroplatinic acid, is irradiated at a temperature of 70.degree. C. with ultraviolet light so that the hydrosilylation reaction takes place and proceeds almost to completeness without deactivation of the platinum catalyst to give the desired product in a yield of 90% or even higher. Unexpectedly, the efficiency of the reaction can be greatly increased when the platinum catalyst is prepared by heating a solution of chloroplatinic acid in 2-ethylhexyl alcohol at 50.degree. to 80.degree. C. for at least 4 hours.

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