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    • 60. 发明授权
    • Toner grafting processes
    • 调色剂接枝工艺
    • US5650252A
    • 1997-07-22
    • US669118
    • 1996-06-24
    • T. Hwee NgArthur HelbrechtRaj D. PatelMichael A. HopperRichard P. N. Veregin
    • T. Hwee NgArthur HelbrechtRaj D. PatelMichael A. HopperRichard P. N. Veregin
    • G03G9/08G03G9/087
    • G03G9/0804G03G9/0806G03G9/0815
    • A process for the preparation of toner comprising:(i) preparing a pigment dispersion, which dispersion is comprised of a pigment, an ionic surfactant, and optionally a charge control agent;(ii) shearing said pigment dispersion with a latex or emulsion blend comprised of resin, a counterionic surfactant with a charge polarity of opposite sign to that of said ionic surfactant and a nonionic surfactant;(iii) heating the above sheared blend below about the glass transition temperature (Tg) of the resin to form electrostatically bound toner size aggregates with a narrow particle size distribution;(iv) heating said bound aggregates above about the Tg of the resin; and(v) thereafter washing the toner obtained, adding initiator, adding monomer, polymerizing by heating, and thereafter cooling, followed by an optional second washing.
    • 一种制备调色剂的方法,包括:(i)制备颜料分散体,该分散体由颜料,离子表面活性剂和任选的电荷控制剂组成; (ii)用由树脂,具有与所述离子表面活性剂的电荷极性相反的电荷极性的抗衡离子表面活性剂和非离子表面活性剂的胶乳或乳液共混物剪切所述颜料分散体; (iii)将上述剪切混合物加热至低于树脂的玻璃化转变温度(Tg),以形成具有窄粒度分布的静电结合的调色剂尺寸聚集体; (iv)将所述结合的聚集体加热到树脂的Tg附近; 和(v)然后洗涤所获得的调色剂,加入引发剂,加入单体,通过加热进行聚合,然后冷却,然后进行任选的第二次洗涤。