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51. 发明授权

US07973087B2 Process of synthesis gas conversion to liquid fuels using mixture of synthesis gas conversion catalyst and dual functionality catalyst 有权
标题翻译：使用合成气转化催化剂和双官能催化剂的混合物将合成气转化为液体燃料的方法
公开(公告)号：US07973087B2
公开(公告)日：2011-07-05
申请号：US12902915
申请日：2010-10-12
申请人： Charles L. Kibby , Kandaswamy Jothimurugesan , Tapan K. Das , Robert J. Saxton , Allen W. Burton, Jr.
发明人： Charles L. Kibby , Kandaswamy Jothimurugesan , Tapan K. Das , Robert J. Saxton , Allen W. Burton, Jr.
IPC分类号： C07C27/00
CPC分类号： C10G2/333 , B01J23/75 , B01J23/894 , B01J29/068 , B01J29/44 , B01J29/74 , B01J35/0006
摘要： A process is disclosed for converting a feed comprising synthesis gas to liquid hydrocarbons within a single reactor at essentially common reaction conditions. The synthesis gas contacts a catalyst bed comprising a mixture of a synthesis gas conversion catalyst on a support containing an acidic component and a dual functionality catalyst including a hydrogenation component and a solid acid component. The hydrocarbons produced are liquid at about 0° C., contain at least 25% by volume C10+ and are substantially free of solid wax.
摘要翻译：公开了用于在基本上常见的反应条件下将包含合成气的进料转化为单个反应器内的液体烃的方法。合成气在包含酸性组分的载体和包含氢化组分和固体酸组分的双官能催化剂的催化剂床上接触合成气转化催化剂的混合物。生产的烃在约0℃是液体的，含有至少25体积％的C 10+，并且基本上不含固体蜡。

52. 发明申请

US20110160315A1 PROCESS OF SYNTHESIS GAS CONVERSION TO LIQUID HYDROCARBON MIXTURES USING SYNTHESIS GAS CONVERSION CATALYST AND HYDROISOMERIZATION CATALYST 审中-公开
标题翻译：使用合成气转化催化剂和氢化催化剂合成气体混合物的合成方法
公开(公告)号：US20110160315A1
公开(公告)日：2011-06-30
申请号：US12780672
申请日：2010-05-14
申请人： Charles L. Kibby , Robert J. Saxton , Kandaswamy Jothimurugesan , Tapan K. Das
发明人： Charles L. Kibby , Robert J. Saxton , Kandaswamy Jothimurugesan , Tapan K. Das
IPC分类号： C07C1/04
CPC分类号： C07C9/22 , C07C1/0435 , C07C5/222 , C07C9/16 , C07C2529/72
摘要： A process is disclosed for converting synthesis gas to a liquid hydrocarbon mixture useful as distillate fuel and/or lube base oil which is substantially free of solid wax. A synthesis gas feed is contacted with a synthesis gas conversion catalyst in an upstream bed and a hydroisomerization catalyst containing a metal promoter and an acidic component in a downstream bed within a single reactor at essentially common reaction conditions. A Fischer-Tropsch wax is formed over the synthesis gas conversion catalyst and said wax is subsequently hydroisomerized over the hydroisomerization catalyst, thereby resulting in a liquid hydrocarbon mixture having a desirable product distribution.
摘要翻译：公开了一种将合成气转化为可用作基本上不含固体蜡的馏出物燃料和/或润滑油基础油的液体烃混合物的方法。合成气进料在上游床中与合成气转化催化剂和含有金属助催化剂和酸性组分的加氢异构化催化剂在基本上常见的反应条件下在单个反应器内的下游床中接触。在合成气转化催化剂上形成费托蜡，然后所述蜡在加氢异构化催化剂上加氢异构化，从而得到具有所需产物分布的液态烃混合物。

53. 发明申请

US20110124750A1 ZEOLITE SUPPORTED COBALT HYBRID FISCHER-TROPSCH CATALYST 有权
标题翻译： ZEOLITE支持的钴混合纤维螯合催化剂
公开(公告)号：US20110124750A1
公开(公告)日：2011-05-26
申请号：US12622972
申请日：2009-11-20
申请人： Charles L. Kibby , Kandaswamy Jothimurugesan , Tapan K. Das , Robert J. Saxton , Allen W. Burton, JR.
发明人： Charles L. Kibby , Kandaswamy Jothimurugesan , Tapan K. Das , Robert J. Saxton , Allen W. Burton, JR.
IPC分类号： C07C27/06
CPC分类号： B01J29/7469 , B01J29/7669 , B01J2229/42 , C07C1/0435 , C07C2529/46 , C10G2/332 , C10G2/334 , C10G2300/1022 , C10G2300/4006 , C10G2300/4012 , C10G2300/703 , C07C9/00
摘要： A method for performing synthesis gas conversion is disclosed which comprises contacting synthesis gas with a hybrid Fischer-Tropsch catalyst formed by impregnating a ZSM-12 zeolite extrudate using a solution, for example, a substantially non-aqueous solution, comprising a cobalt salt and activating the impregnated zeolite extrudate by a reduction-oxidation-reduction cycle. The method results in reduced methane yield and increased yield of liquid hydrocarbons substantially free of solid wax.
摘要翻译：公开了一种用于进行合成气转化的方法，其包括使合成气与通过使用包含钴盐和活化的溶液例如基本上非水溶液浸渍ZSM-12沸石挤出物而形成的混合费 - 托催化剂接触浸渍的沸石通过还原 - 氧化 - 还原循环挤出物。该方法导致甲烷产率降低并且基本上不含固体蜡的液体烃的产率提高。

54. 发明授权

US07670589B2 Synthesis of chabazite-containing molecular sieves and their use in the conversion of oxygenates to olefins 有权
标题翻译：含有菱沸石的分子筛的合成及其在含氧化合物转化为烯烃的用途
公开(公告)号：US07670589B2
公开(公告)日：2010-03-02
申请号：US11521155
申请日：2006-09-14
申请人： Guang Cao , Machteld Maria Mertens , Matu J. Shah , Marc H. Anthonis , Hailian Li , Anil S. Guram , Robert J. Saxton , Mark T. Muraoka , Jeffrey C. Yoder , Anthony F. Volpe, Jr.
发明人： Guang Cao , Machteld Maria Mertens , Matu J. Shah , Marc H. Anthonis , Hailian Li , Anil S. Guram , Robert J. Saxton , Mark T. Muraoka , Jeffrey C. Yoder , Anthony F. Volpe, Jr.
IPC分类号： C01B39/04
CPC分类号： C01B39/48 , B01J29/70 , B01J29/7015 , B01J29/80 , C01B37/02 , C01B39/023 , C07C1/20 , C10G3/49 , C10G3/62 , C10G2300/1011 , C10G2400/20 , Y02P30/20 , C07C11/02
摘要： The synthesis of a crystalline material, in particular, a high silica zeolite, comprising a chabazite-type framework molecular sieve is conducted in the presence of an organic directing agent having the formula: [R1R2R3N—R4]+Q− wherein R1 and R2 are independently selected from hydrocarbyl groups and hydroxy-substituted hydrocarbyl groups having from 1 to 3 carbon atoms, provided that R1 and R2 may be joined to form a nitrogen-containing heterocyclic structure, R3 is an alkyl group having 2 to 4 carbon atoms and R4 is selected from a 4- to 8-membered cycloalkyl group, optionally, substituted by 1 to 3 alkyl groups each having from 1 to 3 carbon atoms; and a 4- to 8-membered heterocyclic group having from 1 to 3 heteroatoms, said heterocyclic group being, optionally, substituted by 1 to 3 alkyl groups each having from 1 to 3 carbon atoms and the or each heteroatom in said heterocyclic group being selected from the group consisting of O, N, and S, or R3 and R4 are hydrocarbyl groups having from 1 to 3 carbon atoms joined to form a nitrogen-containing heterocyclic structure; and Q− is a anion.
摘要翻译：包含菱沸石型骨架分子筛的结晶材料，特别是高硅石沸石的合成在具有下式的有机导向剂的存在下进行：[R 1 R 2 R 3 N-R 4] + Q-，其中R 1和R 2是独立地选自具有1至3个碳原子的烃基和羟基取代的烃基，条件是R 1和R 2可以连接形成含氮杂环结构，R 3是具有2至4个碳原子的烷基，R 4是选自4至8元环烷基，任选被1至3个具有1至3个碳原子的烷基取代; 和具有1至3个杂原子的4至8元杂环基，所述杂环基任选被1至3个具有1至3个碳原子的烷基取代，并且所述杂环基中的每个杂原子被选定由O，N和S组成的组，或R3和R4是具有1至3个碳原子的烃基连接以形成含氮杂环结构; 和Q-是阴离子。

55. 发明申请

US20090111959A1 High silica DDR-type molecular sieve, its synthesis and use 审中-公开
标题翻译：高二氧化硅DDR型分子筛，其合成与使用
公开(公告)号：US20090111959A1
公开(公告)日：2009-04-30
申请号：US11599231
申请日：2006-11-14
申请人： Guang Cao , Machteld Maria Mertens , Karl G. Strohmaier , Hailian Li , Robert J. Saxton , Anil S. Guram , Jeffrey C. Yoder , Mark T. Muraoka , Anthony F. Volpe, JR.
发明人： Guang Cao , Machteld Maria Mertens , Karl G. Strohmaier , Hailian Li , Robert J. Saxton , Anil S. Guram , Jeffrey C. Yoder , Mark T. Muraoka , Anthony F. Volpe, JR.
IPC分类号： C08F4/12 , B01J29/04 , B01D53/62 , B01J29/06
CPC分类号： B01J35/002 , B01D69/148 , B01D71/028 , B01J29/035 , B01J29/70 , B01J2229/62 , C01B37/02 , C01B39/48 , C07C1/20 , C07C1/207 , C07C1/2076 , C07C1/2078 , C07C1/30 , C07C1/322 , C07C1/323 , C07C7/144 , C07C2521/12 , C07C2527/12 , C07C2531/02 , C07C11/02 , C07C9/04
摘要： A crystalline material has a DDR framework type and, in its calcined, anhydrous form, has a composition involving the molar relationship: (n)X2O3:YO2, wherein X is a trivalent element, Y is a tetravalent element and n is from 0 to less than 0.01 and wherein the crystals of said material have an average diameter less than or equal to 2 microns. The material is synthesized in the presence of an N-ethyltropanium compound as directing agent.
摘要翻译：结晶材料具有DDR框架型，并且以其煅烧的无水形式具有涉及摩尔关系的组成：<？in-line-formula description =“In-line formula”end =“lead”？>（n） X 2 O 3：YO 2，<β在线式描述=“在线式”末端=“尾”→其中X为三价元素，Y为四价元素，n为0至小于0.01，其中所述材料的晶体具有小于或等于2微米的平均直径。该物质在N-乙基anium化合物作为引导剂的存在下合成。

56. 发明授权

US06649061B2 Membrane process for separating sulfur compounds from FCC light naphtha 有权
公开(公告)号：US06649061B2
公开(公告)日：2003-11-18
申请号：US10021800
申请日：2001-12-12
申请人： Bhupender S. Minhas , Michael R. Chuba , Robert J. Saxton
发明人： Bhupender S. Minhas , Michael R. Chuba , Robert J. Saxton
IPC分类号： C02F144
CPC分类号： B01J20/28033 , B01D61/246 , B01D61/362 , B01J47/12 , C10G2400/02
摘要： A process for the separation of sulfur compounds from a hydrocarbon mixture using a membrane is provided. Preferred hydrocarbon mixtures are oil refining fractions such as light cracked naphtha. Membranes are composed of either ionic or non-ionic materials and preferentially permeate sulfur compounds over other hydrocarbons. A single or multi-stage membrane system separates the hydrocarbon mixture into a sulfur-rich fraction and a sulfur-lean fraction. The sulfur-lean fraction may be used in fuel mixtures and the sulfur-rich fraction may be further treated for sulfur reduction.

57. 发明授权

US5688484A Non-hydrothermal method of making a titanium-containing zeolite 失效
标题翻译：制备含钛沸石的非水热法
公开(公告)号：US5688484A
公开(公告)日：1997-11-18
申请号：US681585
申请日：1996-07-29
申请人： Robert J. Saxton , John G. Zajacek
发明人： Robert J. Saxton , John G. Zajacek
IPC分类号： C01B37/00 , C01B33/34
CPC分类号： C01B37/005 , Y10S423/22
摘要： A process for producing a titanium-containing zeolite such as TS-1 titanium silicalite is disclosed. A precursor mixture comprising a silica source such as tetraalkylorthosilicate, a titanium source such as titanium alkoxide, a growth medium comprising a nitrogen-containing organic base such as an amine, a fluoride-containing mineralizing agent such as hydrogen fluoride, and an optional organic solvent, is formed then heated to yield the titanium-containing zeolite as solid crystals. A controlled amount of water may be present in the growth medium. The process is capable of providing good yields of high purity zeolites containing framework titanium atoms even in the absence of a quaternary ammonium salt.
摘要翻译：公开了一种生产含钛沸石如TS-1钛硅沸石的方法。包含二氧化硅源的前体混合物，例如原硅酸四烷基酯，钛源如钛醇盐，生长介质，其包含含氮有机碱如胺，含氟化物的矿化剂如氟化氢和任选的有机溶剂，然后加热形成含钛沸石作为固体晶体。受控量的水可能存在于生长培养基中。该方法即使在不存在季铵盐的情况下也能够提供含有骨架钛原子的高纯度沸石的良好产率。

58. 发明授权

US5684170A Epoxidation process 失效
标题翻译：环氧化工艺
公开(公告)号：US5684170A
公开(公告)日：1997-11-04
申请号：US650230
申请日：1996-05-20
申请人： Robert J. Saxton , John G. Zajacek , Guy L. Crocco
发明人： Robert J. Saxton , John G. Zajacek , Guy L. Crocco
IPC分类号： B01J29/89 , C01B37/00 , C07D301/12 , C07D301/19 , C07D303/04
CPC分类号： C07D301/19 , B01J29/89 , C01B37/005 , C07D301/12 , C07D303/04 , Y10S423/27
摘要： A crystalline molecular sieve having a framework structure isomorphous with zeolite beta and containing Si and Ti, but essentially no framework Al, usefully catalyzes olefin epoxidation wherein hydrogen peroxide is the oxidant.
摘要翻译：具有与β沸石同晶并且含有Si和Ti，但基本上不含骨架A1的骨架结构的结晶分子筛有效地催化其中过氧化氢是氧化剂的烯烃环氧化。

59. 发明授权

US5679749A Olefin epoxidation using niobium-containing zeolites 失效
标题翻译：使用含铌沸石的烯烃环氧化
公开(公告)号：US5679749A
公开(公告)日：1997-10-21
申请号：US779144
申请日：1997-01-03
申请人： Robert J. Saxton , John G. Zajacek
发明人： Robert J. Saxton , John G. Zajacek
IPC分类号： B01J29/04 , C01B37/00 , C01B39/08 , C07D301/12 , C08F8/08
CPC分类号： B01J29/04 , C01B37/005 , C01B39/08 , C07D301/12 , Y10S423/22
摘要： Molecular sieve zeolites containing niobium isomorphously substituted in their framework lattice are obtained by hydrothermal crystallization using quaternary ammonium templates. The zeolites are useful catalysts, particularly for the oxidation of hydrocarbons such as olefins.
摘要翻译：通过使用季铵模板的水热结晶获得含有在其框架晶格中同晶取代的铌的分子筛沸石。沸石是有用的催化剂，特别是用于烃类如烯烃的氧化。

60. 发明授权

US5663384A Asymetric epoxidation using a titanium-containing zeolite and a chiral hydroperoxide 失效
标题翻译：使用含钛沸石和手性氢过氧化物进行不对称环氧化
公开(公告)号：US5663384A
公开(公告)日：1997-09-02
申请号：US611732
申请日：1996-03-06
申请人： Wilfred Po-sum Shum , Robert J. Saxton , John G. Zajacek
发明人： Wilfred Po-sum Shum , Robert J. Saxton , John G. Zajacek
IPC分类号： C07B53/00 , C07D301/19
CPC分类号： C07D301/19 , C07B53/00
摘要： Prochiral ethylenically unsaturated substrates are converted to chiral epoxides by reaction with optically active hydroperoxides in the presence of titanium-containing zeolites such as titanium zeolite beta. The method is particularly suitable for producing epoxides from unsubstituted aliphatic olefins which have exceptionally high optical purity as measured by enantiomeric excess.
摘要翻译：通过在含钛沸石如钛沸石β的存在下与光学活性氢过氧化物反应，将前手性烯属不饱和基材转化为手性环氧化物。该方法特别适用于通过对映异构体过量测定的具有非常高的光学纯度的未取代的脂族烯烃制备环氧化物。

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