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41. 发明授权

US4874593A Conversion of pyrophoric P.sub.4 -containing material to P.sub.2 O.sub.5 material 失效
标题翻译：自燃含P4材料转化为P2O5材料
公开(公告)号：US4874593A
公开(公告)日：1989-10-17
申请号：US78430
申请日：1987-07-27
申请人： Auston K. Roberts , William E. Trainer , David L. Biederman
发明人： Auston K. Roberts , William E. Trainer , David L. Biederman
IPC分类号： C01B25/00 , C01B25/027 , C01B25/12 , C01B25/20
CPC分类号： C01B25/003 , C01B25/027 , C01B25/12 , C01B25/20
摘要： A process for treating a pyrophoric P.sub.4 -containing material to convert it to a substantially non-pyrophoric P.sub.2 O.sub.5 material is described. The process comprises supplying streams of fluid P.sub.4 -containing material and an oxygen-containing gas to a reactor filled with water. The P.sub.4 -containing material and the oxygen and the oxygen-containing gas react with one another after both have entered the aqueous medium within the reactor to thereby form the desired P.sub.2 O.sub.5 material.
摘要翻译：描述了一种用于处理含发火的含P4材料以将其转化为基本上不发火的P 2 O 5材料的方法。该方法包括将含有流体P4的材料和含氧气体的流供应到填充有水的反应器中。含二氧化硅的材料和氧气和含氧气体在两者都进入反应器内的水性介质之后相互反应，从而形成所需的P2O5材料。

42. 发明授权

US4774064A Conversion of calcium compounds into solid and gaseous compounds 失效
标题翻译：将钙化合物转化为固体和气态化合物
公开(公告)号：US4774064A
公开(公告)日：1988-09-27
申请号：US945859
申请日：1986-12-23
申请人： David Arnold , Daniel P. McDonald
发明人： David Arnold , Daniel P. McDonald
IPC分类号： C04B7/02 , B01J6/00 , C01B7/19 , C01B17/50 , C01B25/027 , C01B25/12 , C01F11/04 , C01F11/06 , C04B2/10 , C04B7/04 , C04B7/44 , C01F11/00 , C01F11/46
CPC分类号： C01F11/04 , B01J6/008 , C01B17/50 , C01B25/027 , C01B25/12 , C01B7/192 , C01F11/06 , C04B2/10 , C04B7/04 , C04B7/44 , C01P2004/03 , C01P2004/32 , C01P2004/61 , Y02P40/121 , Y02P40/42
摘要： The invention relates to a process for the conversion of a calcium mineral into a calcium containing solid product and a gaseous stream which comprises subjecting the calcium mineral to a temperature in excess of about 3400 degrees Fahrenheit for less than one minute.

43. 发明授权

US4744971A Process for treatment of phossy water for recycling 失效
标题翻译：处理phossy水回收利用的过程
公开(公告)号：US4744971A
公开(公告)日：1988-05-17
申请号：US931375
申请日：1986-11-14
申请人： Gordon H. Scherbel , David A. Crea , Jerry A. Keely , Ronald L. Andersen , Byron L. Nichols
发明人： Gordon H. Scherbel , David A. Crea , Jerry A. Keely , Ronald L. Andersen , Byron L. Nichols
IPC分类号： C01B25/027 , C01B25/01
CPC分类号： C01B25/027
摘要： In the electric arc furnace production of elemental phosphorus, cold phossy water is segregated from hot phossy water. The cold phossy water is discharged to a lined pond wherein solids settle to form a clarified cold water which is recycled for cooling and washing purposes. The hot phossy water is passed through a lamellar settler wherein phosphorus and solids are separated as a sludge to form a clarified hot water. The clarified hot water, without requiring additional heat, is recycled for process use. Phosphorus is recovered from the sludge to reduce to a minimum the amount of phosphorus discharged with dirt from the hot phossy water to the pond.
摘要翻译：在电弧炉生产元素磷中，冷热水与热磷水分离。冷冷的水排出到排水的池塘，其中固体沉淀形成澄清的冷水，再循环冷却和洗涤目的。热磷酸水通过层状沉降器，其中磷和固体作为污泥分离以形成澄清的热水。澄清的热水，不需要额外的热量，被回收用于工艺使用。从污泥中回收磷，将从污水中排出的磷的量减少到从热磷水到池塘的量。

44. 发明授权

US4656020A Production of phosphorus and phosphoric acid 失效
标题翻译：生产磷和磷酸
公开(公告)号：US4656020A
公开(公告)日：1987-04-07
申请号：US763288
申请日：1985-08-07
申请人： James C. Barber
发明人： James C. Barber
IPC分类号： C01B25/01 , C01B25/027 , C02F1/52 , C05B17/00
CPC分类号： C02F1/52 , C01B25/01 , C01B25/027 , C05B17/00
摘要： Processes are disclosed for recovering solid wastes containing elemental phosphorus. The wastes may cause serious environmental problems at phosphorus furnaces because elemental phosphorus is toxic to marine animals. Recovery of the wastes was considered for the following.1. At phosphorus furnace plants making phosphoric acid as one of the products, when the objective is to produce only high-quality phosphoric acid.2. At phosphorus furnace plants making elemental phosphorus as a final product, and the objective is to provide only high-quality phosphorus.3. At plant sites where neither phosphoric acid nor phosphorus is produced.The processes include recycling the wastes to phosphorus furnaces. All of the phosphoric acid produced in 1 can be highly concentrated with low impurities content. In 2, all the low-quality phosphorus is recycled to the phosphorus furnaces and all the produce is high grade. In 3, phosphorus furnaces are not available at the plant site and recycling the solid wastes is impractical. In this case processes are disclosed for recovering the elemental phosphorus from the waste, converting the residue to granular fertilizer, and making suspension fertilizer from water containing elemental phosphorus.
摘要翻译：公开了用于回收含有元素磷的固体废物的方法。由于元素磷对海洋动物有毒，废弃物可能对磷炉造成严重的环境问题。以下考虑废物的回收。在磷化炉厂将磷酸作为产品之一，目的是生产优质磷酸。 2.在磷炉厂制造元素磷作为最终产品，目的是提供高品质的磷。 3.在不生产磷酸和磷的植物地点。这些过程包括将废物回收到磷炉。 1中产生的所有磷酸都可以高度浓缩，杂质含量低。 2，所有低质量的磷被回收到磷炉，所有的产品都是高档的。 3，磷厂在厂址不可用，而且固体废物的再循环是不切实际的。在这种情况下，公开了用于从废物中回收元素磷的过程，将残余物转化为颗粒肥料，并从含有元素磷的水中制备悬浮肥料。

45. 发明授权

US4605540A Low volatile fluorine process for making elemental phosphorus 失效
标题翻译：用于制造元素磷的低挥发性氟工艺
公开(公告)号：US4605540A
公开(公告)日：1986-08-12
申请号：US794117
申请日：1985-11-01
申请人： John E. Stauffer
发明人： John E. Stauffer
IPC分类号： C01B25/02 , C01B25/027 , C01B25/01
CPC分类号： C01B25/027
摘要： The present invention concerns an improvement in the electric furnace process for making elemental phosphorus. The invention features the deliberate addition of an alkali to the burden or charge that is fed to the furnace. Several advantages are gained by the addition of an alkali: pollution is reduced by scavenging fluorine compounds, operating efficiencies are gained, and control over the process is simplified.
摘要翻译：本发明涉及用于制造元素磷的电炉方法的改进。本发明的特征在于有意地将碱加入到加入炉中的负担或电荷中。通过添加碱可以获得几个优点：通过清除氟化合物减少污染物，获得操作效率，并简化对该方法的控制。

46. 发明授权

US4595492A Recovery of phosphorus from dilute waste streams 失效
标题翻译：从稀废物流中回收磷
公开(公告)号：US4595492A
公开(公告)日：1986-06-17
申请号：US672524
申请日：1984-11-19
申请人： David A. Crea , James A. Robertson , Jerry A. Keely
发明人： David A. Crea , James A. Robertson , Jerry A. Keely
IPC分类号： C01B25/027 , B01D43/00
CPC分类号： C01B25/027 , Y10S210/907
摘要： Process for recovery of elemental phosphorus from phosphorus sludge produced in a phosphorus furnace by treating the sludge in a centrifugal separator and separating a fine dirt slimes fraction from a recovered heavy fraction containing the major portion of phosphorus; treating the slimes fraction in hydrocyclones not over one inch (24.4 mm) in diameter to separate two streams, a first phosphorus-poor stream containing particles smaller than 8-15 micrometers, and a second phosphorus-rich stream containing particles larger than 8-15 micrometers; recycling the second, phosphorus-rich stream to the centrifugal separator for phosphorus recovery, and discarding the first, phosphorus-poor stream.
摘要翻译：通过处理离心分离器中的污泥并从含有主要部分的磷的回收重馏分中分离出细小的污垢，从而在磷炉中回收磷污泥中的元素磷回收方法; 处理直径不超过1英寸（24.4mm）的水力旋流器中的粘液分数，以分离含有小于8-15微米的颗粒的第一贫磷流和含有大于8-15的颗粒的第二贫磷流微米; 将第二个富磷流回收到离心分离器中用于磷回收，并且丢弃第一个贫磷流。

47. 发明授权

US4537615A Fertilizer from phosphorus furnace waste stream 失效
标题翻译：磷炉废弃物的化肥
公开(公告)号：US4537615A
公开(公告)日：1985-08-27
申请号：US502921
申请日：1983-06-10
申请人： James C. Barber
发明人： James C. Barber
IPC分类号： C01B25/01 , C01B25/027 , C02F1/52 , C05B17/00 , C05B7/00 , C05B11/10
CPC分类号： C02F1/52 , C01B25/01 , C01B25/027 , C05B17/00
摘要： Processes and compositions of matter are disclosed for the production of liquid fertilizers wherein wastewater from a phosphorus smelting furnace is incorporated in liquid fertilizer processes. The wastewater replaces water evaporated and the wastewater dissolves fertilizer salts. A serious water pollution problem is avoided when wastewater is incorporated in liquid fertilizers. The invention discloses a process for making orthophosphate suspension fertilizer wherein impure phosphoric acid is neutralized in the condensing system, water from the condensing system is bled off, and a suspending clay is added to produce orthophosphate suspension fertilizer. In this process, phosphorus sludge made at phosphorus furnaces is used to produce suspension fertilizer, and wastewater from phosphate smelting furnaces is recovered. New compositions of matter are disclosed. A process is disclosed for making phosphoric acid with low impurities content wherein phosphorus sludge is burned to make impure orthophosphoric acid and the impure acid is recycled to an agglomerating step in a process for making elemental phosphorus.
摘要翻译：公开了用于生产液态肥料的物质的方法和组成，其中来自磷冶炼炉的废水被掺入液体肥料方法中。废水替代蒸发的水，废水溶解肥料盐。当废水掺入液体肥料时，避免了严重的水污染问题。本发明公开了一种制备正磷酸盐悬浮肥料的方法，其中在冷凝系统中中和不纯的磷酸，将来自冷凝系统的水排出，并加入悬浮粘土以生产正磷酸盐悬浮肥料。在这个过程中，磷磷制成的磷污泥用于生产悬浮肥料，回收了来自磷酸盐冶炼炉的废水。披露了新的物质组成。公开了一种制备低杂质含量的磷酸的方法，其中磷污泥被燃烧以制造不纯的正磷酸，并且在制造元素磷的过程中将不纯的酸再循环到附聚步骤。

48. 发明授权

US4478633A Method for processing wastes resulting from production of phosphorus, namely, slime and off-gasses, with utilization of the resultant products 失效
标题翻译：利用所得产物处理由磷生产产生的废物即粘泥和废气的方法
公开(公告)号：US4478633A
公开(公告)日：1984-10-23
申请号：US389271
申请日：1982-06-15
申请人： Vasily B. Chernogorenko , Tleubai M. Alzhanov , Kima A. Lynchak , Simon V. Muchnik , Evgeny S. Ishkhanov , Vladimir Y. Sergienko , Vladimir G. Sapian , Vladimir M. Koverya , Mendel E. Pobortsev , Evgeny A. Markovsky , Valentina V. Dmitrenko , Vladimir I. Bykov , Alexandr D. Kipchakvaev , Alexandr N. Vopilov
发明人： Vasily B. Chernogorenko , Tleubai M. Alzhanov , Kima A. Lynchak , Simon V. Muchnik , Evgeny S. Ishkhanov , Vladimir Y. Sergienko , Vladimir G. Sapian , Vladimir M. Koverya , Mendel E. Pobortsev , Evgeny A. Markovsky , Valentina V. Dmitrenko , Vladimir I. Bykov , Alexandr D. Kipchakvaev , Alexandr N. Vopilov
IPC分类号： B01D53/46 , C01B25/027 , C05B17/00 , C22B7/00 , C22B7/02 , C22B9/10 , C05B11/04
CPC分类号： C22B9/10 , B01D53/46 , C01B25/027 , C05B17/00 , C22B7/007 , C22B7/02 , Y02P10/234
摘要： The method comprises processing slime and off-gases resulting from the production of phosphorus with an aqueous solution of copper sulphate having a concentration of from 15 to 50% at a temperature within the range of from 20.degree. to 80.degree. C. As a result, two products are obtained, i.e. a liquid product and a solid one.The solid product containing mainly copper phosphide as well as fluorides and chlorides of alkali metals and silicon, and silicates of calcium and aluminium, is used as a modifying and refining agent for hypereutectic silumines and for the manufacture of a copper-phosphorus alloy.The liquid product containing phosphoric acid, sulphuric acid and copper sulphate is used as starting product for the preparation of a copper-containing fertilizer.The method according to the present invention makes it possible to modify the production of phosphorus so as to eliminate the formation of secondary wastes and improve the evnironmental control.
摘要翻译：该方法包括在20至80℃的温度范围内，用浓度为15-50％的硫酸铜水溶液处理由磷生成产生的粘液和废气。结果，获得两种产品，即液体产品和固体产品。主要使用磷化铜的固体产物以及碱金属和硅的氟化物和氯化物以及钙和铝的硅酸盐，被用作过共晶硅的改性和澄清剂，并用于制造铜 - 磷合金。使用含有磷酸，硫酸和硫酸铜的液体产物作为制备含铜肥料的起始产物。根据本发明的方法，可以改变磷的产生，从而消除二次废物的形成并改善环境控制。

49. 发明授权

US4451277A Production of fluid fertilizer from phosphorus furnace waste stream 失效
标题翻译：从磷炉废料流中生产流体肥料
公开(公告)号：US4451277A
公开(公告)日：1984-05-29
申请号：US428840
申请日：1982-09-30
申请人： James C. Barber
发明人： James C. Barber
IPC分类号： C01B25/01 , C01B25/027 , C02F1/52 , C05B17/00 , C05B11/10 , C05B7/00
CPC分类号： C02F1/52 , C01B25/01 , C01B25/027 , C05B17/00
摘要： Processes and compositions of matter are disclosed for the production of liquid fertilizers wherein wastewater from a phosphorus smelting furnace is incorporated in lqiuid fertilizer processes. The wastewater replaces water evaporated and the wastewater dissolves fertilizer salts. A serious water pollution problem is avoided when wastewater is incorporated in liquid fertilizers. The invention discloses a process for making orthophosphate suspension fertilizer wherein impure phosphoric acid is neutralized in the condensing system, water from the condensing system is bled off, and a suspending clay is added to produce orthophosphate suspension fertilizer. In this process, phosphorus sludge made at phosphorus furnaces is used to produce suspension fertilizer, and wastewater from phosphate smelting furnaces is recovered. New compositions of matter are disclosed. A process is disclosed for making phosphoric acid with low impurities content wherein phosphorus sludge is burned to make impure orthophosphoric acid and the impure acid is recycled to an agglomerating step in a process for making elemental phosphorus.
摘要翻译：公开了用于生产液体肥料的物质的方法和组合物，其中来自磷冶炼炉的废水被掺入肥料肥料方法中。废水替代蒸发的水，废水溶解肥料盐。当废水掺入液体肥料时，避免了严重的水污染问题。本发明公开了一种制备正磷酸盐悬浮肥料的方法，其中在冷凝系统中中和不纯的磷酸，将来自冷凝系统的水排出，并加入悬浮粘土以生产正磷酸盐悬浮肥料。在这个过程中，磷磷制成的磷污泥用于生产悬浮肥料，回收了来自磷酸盐冶炼炉的废水。披露了新的物质组成。公开了一种制备低杂质含量的磷酸的方法，其中磷污泥被燃烧以制造不纯的正磷酸，并且在制造元素磷的过程中将不纯的酸再循环到附聚步骤。

50. 发明授权

US4373893A Bench scale drum agglomerator and power means 失效
标题翻译：台式鼓式聚焦机和动力装置
公开(公告)号：US4373893A
公开(公告)日：1983-02-15
申请号：US316344
申请日：1981-10-29
申请人： James C. Barber
发明人： James C. Barber
IPC分类号： C01B25/01 , C01B25/027 , C02F1/52 , C05B17/00 , B22F3/00
CPC分类号： C02F1/52 , C01B25/01 , C01B25/027 , C05B17/00
摘要： A process and product of waste recovery at phosphorus furnaces is disclosed wherein small sized discrete particles of carbonaceous material or beneficiated phosphate ore are mixed with a mineral acid, an alkaline fluid and water, and the reacted mixture is tumbled in a horizontal cylinder at a temperature below that at which the carbonaceous material oxidizes to form agglomerates which are then indurated to discrete particulate size as desired for a charge component; the agglomerates are fed to a phosphorus smelting furnace together with other materials needed to make elemental phosphorus, furnace gases are cooled with recirculating water, a side stream of the water is taken off, treated, and used as feedstock in fluid fertilizers. Apparatus is disclosed for agglomerating coke and phosphate and, further, for measuring the abrasion and shatter resistance of agglomerates.
摘要翻译：公开了一种在磷炉中废物回收的方法和产物，其中将小尺寸的碳质材料或精选磷酸盐矿石的离散颗粒与无机酸，碱性流体和水混合，并将反应的混合物在水平圆筒中以温度低于碳质材料氧化以形成附聚物，然后根据需要将电荷组分饱和到离散的颗粒尺寸; 将附聚物与制造元素磷所需的其它材料一起进料到磷冶炼炉中，炉内气体用再循环水冷却，水的侧流被除去，处理并用作流体肥料中的原料。公开了用于凝结焦炭和磷酸盐的装置，此外，还用于测量附聚物的耐磨性和抗碎裂性。

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