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41. 发明申请

US20120114521A1 STABILIZED METAL NANOPARTICLES AND METHODS FOR PRODUCTION THEREOF 有权
标题翻译：稳定的金属纳米颗粒及其生产方法
公开(公告)号：US20120114521A1
公开(公告)日：2012-05-10
申请号：US13228411
申请日：2011-09-08
申请人： Alfred A. ZINN
发明人： Alfred A. ZINN
IPC分类号： B22F9/20 , C22C9/00 , B82Y40/00
CPC分类号： B22F1/0018 , B22F1/0062 , B22F9/24 , B22F2999/00 , B82Y30/00 , H05K1/097 , H05K3/125 , H05K2201/0218 , H05K2201/0257 , H05K2203/0514 , H05K2203/107 , B22F2301/10 , B22F2304/054
摘要： Processes for synthesizing metal nanoparticles, particularly copper nanoparticles, are described. The processes can involve reacting an insoluble complex of a metal salt with a reducing agent in a reaction mixture containing a primary amine first surfactant, a secondary amine second surfactant, and a diamine chelating agent third surfactant. More specifically, processes for forming copper nanoparticles can involve forming a first solution containing a copper salt, a primary amine first surfactant, a secondary amine second surfactant, and a diamine chelating agent third surfactant; allowing an insoluble complex of the copper salt to form from the first solution; combining a second solution containing a reducing agent with the insoluble complex; and forming copper nanoparticles from the insoluble complex. Such copper nanoparticles can be about 10 nm or smaller in size, more particularly about 3 nm to about 6 nm in size, and have a fusion temperature of about 200° C. or lower.
摘要翻译：描述了合成金属纳米颗粒，特别是铜纳米颗粒的方法。该方法可以包括在含有伯胺第一表面活性剂，仲胺第二表面活性剂和二胺螯合剂第三表面活性剂的反应混合物中使金属盐的不溶性络合物与还原剂反应。更具体地，形成铜纳米颗粒的方法可以包括形成含有铜盐，伯胺第一表面活性剂，仲胺第二表面活性剂和二胺螯合剂第三表面活性剂的第一溶液; 允许从第一溶液形成铜盐的不溶性络合物; 将含有还原剂的第二溶液与不溶性络合物组合; 并从不溶性络合物形成铜纳米颗粒。这种铜纳米颗粒的尺寸可以为约10nm或更小，更特别地约3nm至约6nm，熔融温度为约200℃或更低。

42. 发明申请

US20120042750A1 PROCESS FOR PRODUCING MAGNETIC METAL PARTICLES FOR MAGNETIC RECORDING, AND MAGNETIC RECORDING MEDIUM 审中-公开
标题翻译：用于制造用于磁记录的磁性金属颗粒和磁记录介质的方法
公开(公告)号：US20120042750A1
公开(公告)日：2012-02-23
申请号：US13285035
申请日：2011-10-31
申请人： Mineko OHSUGI , Toshiharu HARADA , Takahiro MATSUO , Yosuke YAMAMOTO , Kazuyuki HAYASHI
发明人： Mineko OHSUGI , Toshiharu HARADA , Takahiro MATSUO , Yosuke YAMAMOTO , Kazuyuki HAYASHI
IPC分类号： B22F9/20
CPC分类号： G11B5/712 , B22F9/22 , B22F2998/10 , B22F2999/00 , C22C33/0235 , C22C2202/02 , G11B5/70642 , H01F1/11 , H01F1/112 , H01F1/113 , C01B13/00 , B22F1/0088 , B22F1/0085 , B22F2201/013
摘要： The present invention relates to a process for producing magnetic metal particles for magnetic recording, comprising:heat-treating goethite particles having an aluminum content of 4 to 50 atom % in terms of Al based on whole Fe to obtain hematite particles; andheat-reducing the hematite particles at a temperature of 200 to 600° C.,the goethite particles being obtained by adding a peroxodisulfate to a reaction solution comprising:a ferrous salt aqueous solution anda mixed alkali aqueous solution comprising:an alkali hydrogen carbonate aqueous solution or alkali carbonate aqueous solution andan alkali hydroxide aqueous solution before initiation of an oxidation reaction of the reaction solution, and then conducting the oxidation reaction.
摘要翻译：本发明涉及一种磁记录用磁性金属粒子的制造方法，其特征在于，以全Fe为基准，以Al为基准热处理铝含量为4〜50原子％的针铁矿粒子，得到赤铁矿粒子; 并在200〜600℃的温度下还原赤铁矿颗粒，通过向反应溶液中加入过二硫酸盐而得到的针铁矿颗粒，所述反应溶液包含：亚铁盐水溶液和混合碱水溶液，所述混合碱水溶液包含：碱金属氢氧化物水溶液或碱金属碳酸盐水溶液和碱性氢氧化物水溶液，然后进行氧化反应。

43. 发明申请

US20110206864A1 ORGANOMETALLIC COMPOUNDS, PROCESSES FOR THE PREPARATION THEREOF AND METHODS OF USE THEREOF 审中-公开
标题翻译：有机化合物，其制备方法及其使用方法
公开(公告)号：US20110206864A1
公开(公告)日：2011-08-25
申请号：US13101328
申请日：2011-05-05
申请人： David Walter Peters , David M. Thompson
发明人： David Walter Peters , David M. Thompson
IPC分类号： C07F17/00 , B22F9/20 , H05H1/24 , C23C16/18
CPC分类号： C07F17/00
摘要： This invention relates to organometallic precursor compounds represented by the formula (Cp(R′)x)yM(H)z-y, a process for producing the organometallic precursor compounds, and a method for depositing a metal and/or metal carbide layer, e.g., Ta metal and/or TaC layer, on a substrate by the thermal or plasma enhanced disassociation of the organometallic precursor compounds, e.g., by CVD or ALD techniques. The metal and/or metal carbide layer is useful as a liner or barrier layer for conducting metals and high dielectric constant materials in integrated circuit manufacturing.
摘要翻译：本发明涉及由式（Cp（R'）x）yM（H）zy表示的有机金属前体化合物，有机金属前体化合物的制备方法，以及沉积金属和/或金属碳化物层的方法， Ta金属和/或TaC层，通过有机金属前体化合物的热或等离子体增强的分离，例如通过CVD或ALD技术在基底上。金属和/或金属碳化物层可用作集成电路制造中用于导电金属和高介电常数材料的衬垫或阻挡层。

44. 发明申请

US20110023656A1 METHOD FOR PRODUCING GRANULAR METALLIC IRON 审中-公开
标题翻译：生产颗粒金属铁的方法
公开(公告)号：US20110023656A1
公开(公告)日：2011-02-03
申请号：US12937054
申请日：2009-04-06
申请人： Kazutaka Kunii , Takahiro Kudo
发明人： Kazutaka Kunii , Takahiro Kudo
IPC分类号： B22F9/20
CPC分类号： C21B13/008 , C21B13/0046 , C21B13/006 , C21B13/105 , C21C5/54 , C21C7/076 , Y02P10/136 , Y02P10/216 , Y02P10/242
摘要： A method for producing granular metallic iron by heating and reducing a raw material mixture which includes an iron oxide-containing material, a carbonaceous reductant and a Li2O supplying material in a thermal reduction furnace, wherein the iron oxide-containing material includes a hematite-containing material, and the raw material mixture includes at least Fe, Ca, Mg, Si and Li as constituent elements in such a manner that slag which forms as a by-product during heating and reduction contains CaO, MgO, SiO2 and Li2O, has a Li2O content of 0.05% by mass or more, and the slag has a basicity [(CaO+MgO)/SiO2] in a range of from 1.5 to 1.9. This method enables granular metallic iron to be produced at a high productivity even when a hematite-containing material is used as the iron oxide-containing material.
摘要翻译：一种通过在热还原炉中加热还原包含含氧化铁的材料，碳质还原剂和Li2O供应材料的原料混合物来生产颗粒状金属铁的方法，其中含氧化铁的材料包括含赤铁矿的材料原料混合物至少包含Fe，Ca，Mg，Si和Li作为构成元素，使得在加热和还原期间作为副产物形成的炉渣含有CaO，MgO，SiO 2和Li 2 O，具有 Li2O含量为0.05质量％以上，炉渣的碱度[（CaO + MgO）/ SiO2]为1.5〜1.9。这种方法使得即使使用含赤铁矿的材料作为含铁氧化物的材料也能以高生产率生产粒状金属铁。

45. 发明申请

US20100316882A1 NANOMATERIAL AND METHOD FOR GENERATING NANOMATERIAL 审中-公开
标题翻译：用于产生纳米材料的纳米材料和方法
公开(公告)号：US20100316882A1
公开(公告)日：2010-12-16
申请号：US12866832
申请日：2009-02-25
申请人： Andrey V. Filippov , Clinton Damon Osterhout , Martin Andrew Sala , Kamal Kishore Soni , Carlton Maurice Truesdale
发明人： Andrey V. Filippov , Clinton Damon Osterhout , Martin Andrew Sala , Kamal Kishore Soni , Carlton Maurice Truesdale
IPC分类号： B32B15/02 , B22F9/20 , B22F9/30 , B05D1/12 , B32B9/00 , B32B15/04 , B29B9/12
CPC分类号： C01B33/03 , B82Y30/00 , C23C16/24 , Y10T428/12028 , Y10T428/31678
摘要： Nanomaterial and methods for generating nanomaterial are described wherein a reaction, for example, decomposition, for generating nanomaterial occurs utilizing a hot wall reactor.
摘要翻译：描述了用于产生纳米材料的纳米材料和方法，其中利用热壁反应器发生用于产生纳米材料的反应，例如分解。

46. 发明授权

US07766992B2 Producing metallic articles by reduction of nonmetallic precursor compounds and melting 有权
标题翻译：通过还原非金属前体化合物并熔化生产金属制品
公开(公告)号：US07766992B2
公开(公告)日：2010-08-03
申请号：US11059715
申请日：2005-02-16
申请人： Andrew Philip Woodfield , Clifford Earl Shamblen , Eric Allen Ott
发明人： Andrew Philip Woodfield , Clifford Earl Shamblen , Eric Allen Ott
IPC分类号： B22F9/20
CPC分类号： C22B34/1295 , C22B4/005 , C22B4/06 , C22B34/1263 , C22B34/129
摘要： A metallic article is produced by furnishing one or more nonmetallic precursor compound comprising the metallic constituent element(s), and chemically reducing the nonmetallic precursor compound(s) to produce an initial metallic particle, preferably having a size of no greater than about 0.070 inch, without melting the initial metallic particle. The initial metallic particle is thereafter melted and solidified to produce the metallic article. By this approach, the incidence of chemical defects in the metal article is minimized. The melted-and-solidified metal may be used in the as-cast form, or it may be converted to billet and further worked to the final form.
摘要翻译：通过提供一种或多种包含金属构成元素的非金属前体化合物和化学还原非金属前体化合物以产生初始金属颗粒，优选具有不大于约0.070英寸，而不熔化初始金属颗粒。然后将初始金属颗粒熔化并固化以制备金属制品。通过这种方法，金属制品中的化学缺陷的发生率被最小化。熔融和固化的金属可以铸造形式使用，或者可以转化成坯料并进一步加工成最终形式。

47. 发明授权

US07695543B2 Process for the production of silver filaments having micrometric or sub-micrometric diameter and product thereof 有权
标题翻译：用于生产具有微米或亚微米直径的银丝的方法及其制品
公开(公告)号：US07695543B2
公开(公告)日：2010-04-13
申请号：US11370181
申请日：2006-03-08
申请人： Brunetto Martorana , Luigi Nicolais , Gianfranco Carotenuto , Piero Perlo
发明人： Brunetto Martorana , Luigi Nicolais , Gianfranco Carotenuto , Piero Perlo
IPC分类号： B22F9/20 , B22F1/00
CPC分类号： B22F9/30 , B22F1/004 , B22F2999/00 , B22F3/1216 , C22C21/00
摘要： The present invention relates to a process for the production of continuous silver wires having micrometric or sub-micrometric diameter comprising a step of thermal decomposition of silver dodecyl-mercaptide in the presence of metallic aluminum.
摘要翻译：本发明涉及一种制备具有微米或亚微米直径的连续银丝的方法，包括在金属铝存在下热分解十二烷基硫醇银的步骤。

48. 发明申请

US20100031848A1 ALLOY NANOPARTICLES OF SN-CU-AG, PREPARATION METHOD THEREOF AND INK OR PASTE USING THE ALLOY NANOPARTICLES 审中-公开
标题翻译： SN-CU-AG的合金纳米颗粒，其制备方法和使用合金纳米颗粒的油墨或油墨
公开(公告)号：US20100031848A1
公开(公告)日：2010-02-11
申请号：US12437945
申请日：2009-05-08
申请人： Kwi-Jong LEE , Hyuck-Mo Lee , Hyun-Joon Song , Yun-Hwan Jo , Ji-Chan Park , Jung-Up Bang , Dong-Hoon Kim
发明人： Kwi-Jong LEE , Hyuck-Mo Lee , Hyun-Joon Song , Yun-Hwan Jo , Ji-Chan Park , Jung-Up Bang , Dong-Hoon Kim
IPC分类号： C09D11/00 , C22C13/00 , B22F9/20
CPC分类号： C22C13/00 , B22F1/0018 , B22F9/24 , B22F2999/00 , B82Y30/00 , C09D11/52 , Y10T428/12708 , Y10T428/12715 , B22F2207/07
摘要： The invention relates to Sn—Cu—Ag alloy nanoparticles, preparation method thereof and ink or paste using the alloy nanoparticles in which the alloy nanoparticles are suitable for metal ink having excellent electrical conductivity or solder materials having low calcinating temperature.
摘要翻译：本发明涉及Sn-Cu-Ag合金纳米粒子，其制备方法和使用合金纳米颗粒的油墨或糊料，其中合金纳米颗粒适用于具有优良导电性的金属油墨或具有低煅烧温度的焊料。

49. 发明授权

US07431751B2 Magnesium removal from magnesium reduced metal powders 有权
标题翻译：从镁中除去镁还原金属粉末
公开(公告)号：US07431751B2
公开(公告)日：2008-10-07
申请号：US10953163
申请日：2004-09-29
申请人： Leonid Natan Shekhter , Leonid Lanin , Anastasis M. Conlon
发明人： Leonid Natan Shekhter , Leonid Lanin , Anastasis M. Conlon
IPC分类号： B22F9/20
CPC分类号： C22B5/04 , B22F9/20 , B22F9/22 , C22B26/22 , C22B34/24 , C22C1/045 , H01G9/0525
摘要： A method of producing a refractory metal powder that includes providing a metal powder containing magnesium tantalate or magnesium niobate; and heating the powder in an inert atmosphere in the presence of magnesium, calcium and/or aluminum to a temperature sufficient to remove magnesium tantalate or magnesium niobate from the powder and/or heating the powder under vacuum to a temperature sufficient to remove magnesium tantalate or magnesium niobate from the powder, the heating steps being performed in any order. The metal powder can be formed into pellets at an appropriate sintering temperature, which can be formed into electrolytic capacitors.
摘要翻译：一种制造难熔金属粉末的方法，其包括提供含有钽酸镁或铌酸镁的金属粉末; 并在镁，钙和/或铝的存在下在惰性气氛中加热粉末至足以从粉末中除去钽酸镁或铌酸镁的温度和/或在真空下加热粉末至足以除去钽酸镁或从粉末中获得铌酸镁，加热步骤以任何顺序进行。金属粉末可以在可以形成为电解电容器的适当烧结温度下形成粒料。

50. 发明申请

US20080072706A1 Method for manufacturing copper nanoparticles using microwaves 有权
标题翻译：使用微波制造铜纳米粒子的方法
公开(公告)号：US20080072706A1
公开(公告)日：2008-03-27
申请号：US11892711
申请日：2007-08-27
申请人： Young-Il Lee , Jae-Woo Joung
发明人： Young-Il Lee , Jae-Woo Joung
IPC分类号： B22F9/20
CPC分类号： B22F9/24 , B22F2998/00 , B22F2999/00 , B82Y30/00 , C30B7/14 , C30B29/602 , Y10S977/773 , Y10S977/775 , Y10S977/777 , Y10S977/81 , Y10S977/932 , B22F1/0018 , B22F2202/11
摘要： The present invention relates to a method for manufacturing copper nanoparticles, in particular, to a method for manufacturing copper nanoparticles, wherein the method includes preparing a mixture solution including a copper salt, a dispersing agent, a reducing agent and an organic solvent; raising temperature of the mixture solution up to 30-50° C. and agitating; irradiating the mixture solution with microwaves; and obtaining the copper nanoparticles by lowering temperature of the mixture solution.According to the present invention, several tens of nm of copper nanoparticles having a narrow particle size distribution and good dispersibility can be synthesized in mass production.
摘要翻译：本发明涉及一种制造铜纳米颗粒的方法，特别涉及一种制造铜纳米颗粒的方法，其中该方法包括制备包括铜盐，分散剂，还原剂和有机溶剂的混合溶液; 将混合溶液的温度升高至30-50℃并搅拌; 用微波照射混合溶液; 并通过降低混合溶液的温度来获得铜纳米颗粒。根据本发明，可以在批量生产中合成数十nm的粒径分布窄，分散性好的铜纳米粒子。

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