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41. 发明授权

US4384102A Process for the preparation of compounds having s-triazine units and epoxide groups 失效
标题翻译：制备具有三嗪单元和环氧基团的化合物的方法
公开(公告)号：US4384102A
公开(公告)日：1983-05-17
申请号：US336659
申请日：1982-01-04
申请人： Werner Rasshofer , Gerhard Grogler , Richard Kopp
发明人： Werner Rasshofer , Gerhard Grogler , Richard Kopp
IPC分类号： C07D405/14 , C07D405/12 , C08G18/00 , C08G18/79 , C08G18/80 , C08G18/77
CPC分类号： C07D405/12 , C08G18/003 , C08G18/8058
摘要： Compounds having both s-triazine units and epoxide groups present are prepared by reacting an epoxide containing an isocyanate-reactive group with a triisocyanate corresponding to the formula: ##STR1## in which X is as defined herein. These reactants are used in quantities such that the equivalent ratio of isocyanate groups to isocyanate-reactive groups is maintained at less than or equal to 1 to 1. The compounds thus produced are particularly useful as reactive cross-linkers in the production of polyurethanes and polyepoxides.
摘要翻译：通过使含有异氰酸酯反应性基团的环氧化物与对应于下式的其中X如本文所定义的下式的三异氰酸酯反应来制备具有均三嗪单元和环氧基团的化合物。这些反应物的用量使得异氰酸酯基团与异氰酸酯反应性基团的当量比保持在小于或等于1比1。由此制备的化合物特别可用作聚氨酯和聚环氧化物生产中的反应性交联剂。

42. 发明授权

US4360603A Process for the preparation of compounds containing s-triazine units and isocyanate groups or isocyanate-reactive groups and the production of polyurethanes containing these fillers 失效
标题翻译：用于制备含有三嗪单元和异氰酸酯基团或异氰酸酯反应性基团的化合物的方法以及含有这些填料的聚氨酯的生产方法
公开(公告)号：US4360603A
公开(公告)日：1982-11-23
申请号：US323331
申请日：1981-11-20
申请人： Gerhard Grogler , Werner Rasshofer , Richard Kopp
发明人： Gerhard Grogler , Werner Rasshofer , Richard Kopp
IPC分类号： C08G18/00 , C07D251/70 , C08G18/38 , C08G18/79 , C08G18/80 , C08L75/00 , C08L75/04 , C08G18/14
CPC分类号： C08G18/8003 , C07D251/70 , C08G18/3851 , C08G18/8058
摘要： This invention relates to a process for the preparation of compounds which contain s-triazine units and isocyanate groups or isocyanate-reactive groups and which melt without decomposition, by the reaction of triisocyanates containing s-triazine units with compounds containing isocyanate-reactive groups, and the use of these products as fillers which can be chemically fixed in the production of polyurethanes by the isocyanate polyaddition process.
摘要翻译：本发明涉及一种制备含有三嗪单元和异氰酸酯基团或异氰酸酯反应性基团并通过含有三嗪单元的三异氰酸酯与含有异氰酸酯反应性基团的化合物反应熔融而不分解的化合物的方法，以及这些产品的使用可以通过异氰酸酯加聚方法在化学上固定在聚氨酯的生产中。

43. 发明授权

US06428895B1 Stable adhesive composite material made of polyurethane and of another thermoplastic material, a process for its production and a method for its use in motor vehicles 失效
标题翻译：由聚氨酯和另一种热塑性材料制成的稳定的粘合剂复合材料，其生产方法及其用于机动车辆的方法
公开(公告)号：US06428895B1
公开(公告)日：2002-08-06
申请号：US09919384
申请日：2001-07-31
申请人： Karsten Reihs , Werner Rasshofer , Holger Warth , Dirk Wegener , Manfred Schmidt , Peter Heitkämper
发明人： Karsten Reihs , Werner Rasshofer , Holger Warth , Dirk Wegener , Manfred Schmidt , Peter Heitkämper
IPC分类号： B32B710
CPC分类号： B32B27/40 , B32B5/18 , B32B27/32 , B32B27/34 , B32B27/365 , B32B2266/0278 , B32B2323/04 , B32B2323/10 , B32B2367/00 , B32B2369/00 , B32B2375/00 , C08J5/12 , C08J2375/04 , C09J175/08 , Y10T428/31507 , Y10T428/31551 , Y10T428/31562 , Y10T428/31565 , Y10T428/31587 , Y10T428/31598 , Y10T428/31739
摘要： The present invention relates to composite materials made of at least one composite layer of a polyurethane and of a second composite layer which is directly bonded to the first layer and which consists of a thermoplastic material that is different from the polyurethane of layer A). The polyurethane material of layer A) is characterized by a residual content of free reaction components containing ether groups of no more than 400 ppm, and preferably of no more than 100 ppm. The invention also relates to a process for the production of these composite materials and to a method of their use as materials in motor vehicles.
摘要翻译：本发明涉及由聚氨酯和第二复合层的至少一个复合层制成的复合材料，所述复合层直接结合到第一层，并且由不同于层A）的聚氨酯的热塑性材料组成。层A）的聚氨酯材料的特征在于含有不超过400ppm，优选不超过100ppm的醚基的游离反应组分的残留含量。本发明还涉及一种生产这些复合材料的方法及其作为机动车辆材料的方法。

44. 发明授权

US6020386A Process for the production of hydroxyfunctional compounds from (polyurethane) polyurea waste 失效
标题翻译：从（聚氨酯）聚脲废料生产羟基官能化合物的方法
公开(公告)号：US6020386A
公开(公告)日：2000-02-01
申请号：US189861
申请日：1994-02-01
申请人： Thomas Munzmay , Walter Meckel , Ulrich Liman , Hartmut Nefzger , Werner Rasshofer , Karl-Heinz Dorner , Andreas Ruckes
发明人： Thomas Munzmay , Walter Meckel , Ulrich Liman , Hartmut Nefzger , Werner Rasshofer , Karl-Heinz Dorner , Andreas Ruckes
IPC分类号： C08G18/83 , C08G18/32 , C08J11/22 , C08L75/00 , C08J11/04
CPC分类号： C08J11/22 , C08J2375/00 , Y02P20/582 , Y02W30/706
摘要： Hydroxyfunctional compounds suitable for use in the polyisocyanate polyaddition process are obtained from polyurethane and/or polyurethane polyurea waste by decomposition with an alcohol and subsequent reaction of the alcoholysis products to reduce their content of low molecular weight, sterically unhindered aromatic amines. In this process, polyurethane and/or polyurethane polyurea waste is first treated with a low molecular weight diol or polyol at a temperature of from about 160 to 260.degree. C. The resultant alcoholysis product may then either be further heated at a temperature lower than that used in the first step within the ranger of from about 50 to 180.degree. C. or reacted with a dialkyl carbonate and/or 1,3-dicarbonyl compound.
摘要翻译：适用于多异氰酸酯加聚方法的羟基官能化合物通过用醇分解从聚氨酯和/或聚氨酯聚脲废物中获得，随后醇解产物的反应降低其低分子量空间不受阻碍的芳族胺的含量。在该方法中，聚氨酯和/或聚氨酯聚脲废物首先在约160至260℃的温度下用低分子量二醇或多元醇进行处理。然后可以在低于该温度的温度下进一步加热得到的醇解产物。在第一步中用于约50至180℃的游C.，或与碳酸二烷基酯和/或1,3-二羰基化合物反应。

45. 发明授权

US5879608A Molded polyurethane articles prepared from recycled polyols and processes for their production and use 失效
标题翻译：由回收多元醇制备的模制聚氨酯制品及其生产和使用方法
公开(公告)号：US5879608A
公开(公告)日：1999-03-09
申请号：US740551
申请日：1996-10-30
申请人： Adolf Lammeck , Werner Rasshofer
发明人： Adolf Lammeck , Werner Rasshofer
IPC分类号： C08G18/40 , C08G18/83 , C08G101/00 , C08J11/24 , B27N3/08 , B28B19/00 , B29C51/00 , B29C53/00
CPC分类号： C08J11/24 , C08J2375/04 , Y02W30/706
摘要： Molded polyurethane articles are made by reacting polyisocyanates with polyol compositions obtained by chemical decomposition of polyurethane and/or polyurea waste in a mold. The polyol compositions employed in this invention have an OH value of from about 100 to about 500 mg KOH/g, a water content of from 0 to about 5 wt. % and a viscosity at 20.degree. C. of more than 2,000 mPa.multidot.s. These molded polyurethane articles preferably have a sandwich structure in which the core is a polyurethane and there is at least one outer layer made from an optionally fiber-reinforced plastic material. These molded polyurethane articles are useful in the motor vehicle, furniture, machine and equipment manufacturing industries.
摘要翻译：聚氨酯制品是通过使多异氰酸酯与通过在模具中化学分解聚氨酯和/或聚脲废物获得的多元醇组合物而制成的。用于本发明的多元醇组合物的OH值为约100至约500mg KOH / g，水含量为0至约5wt。％，在20℃下的粘度超过2,000mPax。这些模制的聚氨酯制品优选具有夹心结构，其中芯是聚氨酯，并且存在由任选的纤维增强塑料材料制成的至少一个外层。这些模塑聚氨酯制品可用于机动车辆，家具，机器和设备制造业。

46. 发明授权

US5210127A Free-flowing, thermoplastically processible and post-crosslinkable polyurethane powders 失效
标题翻译：自由流动，热塑性可交联聚氨酯粉末
公开(公告)号：US5210127A
公开(公告)日：1993-05-11
申请号：US964592
申请日：1992-10-21
申请人： Joachim Werner , Walter Meckel , Ulrich Liman , Dirk Wegener , Werner Rasshofer , James W. Rosthauser
发明人： Joachim Werner , Walter Meckel , Ulrich Liman , Dirk Wegener , Werner Rasshofer , James W. Rosthauser
IPC分类号： C08G18/00 , C08G18/08 , C08G18/10 , C08G18/79 , C08G18/80 , C08J3/12 , C08J3/24 , C08J5/18 , C08J9/10 , C08J9/16 , C08L75/00 , C08L75/04
CPC分类号： C08J3/24 , C08G18/0871 , C08G18/10 , C08G18/8064 , C08G2101/00 , C08G2140/00 , C08G2350/00 , C08G2410/00 , C08J2375/04
摘要： Novel powders useful in the slush molding process are produced by reacting an emulsion of either an isocyanate or an isocyanate reactive material with either an isocyanate reactive material or an isocyanate, depending upon the nature of the component used to make the emulsion in the presence of an at least partially blocked isocyanate and an organic carrier. The final reaction product is subsequently removed from the carrier.
摘要翻译：通过将异氰酸酯或异氰酸酯反应性材料的乳液与异氰酸酯反应性材料或异氰酸酯反应来制备可用于搪塑成型方法的新型粉末，这取决于在存在下制备乳液的组分的性质至少部分封端的异氰酸酯和有机载体。随后从载体中除去最终的反应产物。

47. 发明授权

US5077339A Heat-curing reactive powders based on polyurethanes 失效
标题翻译：基于聚氨酯的热固化活性粉末
公开(公告)号：US5077339A
公开(公告)日：1991-12-31
申请号：US621200
申请日：1990-11-30
申请人： Gerhard Grogler , Heinrich Hess , Richard Kopp , Werner Rasshofer
发明人： Gerhard Grogler , Heinrich Hess , Richard Kopp , Werner Rasshofer
IPC分类号： C08G18/00 , C08G18/08 , C08G18/42 , C08G18/46 , C08G18/50 , C08G18/65 , C08G18/70 , C08G18/76 , C08G18/78 , C08G18/79 , C08G18/80 , C09D5/46
CPC分类号： C08G18/7818 , C08G18/0871 , C08G18/4238 , C08G18/4615 , C08G18/5048 , C08G18/6505 , C08G18/6529 , C08G18/703 , C08G18/7678 , C08G18/798 , C08G18/8038 , C08G2140/00 , C08G2150/20 , C08G2170/20 , Y10S525/902 , Y10S525/936
摘要： The present invention relates to the preparation of powdered heat-curable reaction mixtures in which melt suspension of (a) solid polyisocyanates having melting points above about 60.degree. C., (b) molten high molecular weight isocyanate-reactive compounds having molecular weights of from 400 to 10,000 that have melting or softening points of 50.degree. C. to 150.degree. C., and (c) optionally, solid or liquid low molecular weight chain-extending or crosslinking compounds having molecular weights of from 62 to 399, are added to an inert solvent containing an emulsifier, thereby forming powdered heat-curable reaction mixtures in which components (a), (b), and (c) remain in uncrossedlinked form. The invention further relates to the use of the heat-curing reaction mixtures for the preparation of high-quality polyurethane polyurea plastics.
摘要翻译：本发明涉及粉末状热固化反应混合物的制备，其中（a）熔点高于约60℃的固体聚异氰酸酯的熔体悬浮液，（b）熔融的高分子量异氰酸酯反应性化合物，其分子量为 400至10,000，其熔点或软化点为50℃至150℃，和（c）任选地，分子量为62至399的固体或液体低分子量链延长或交联化合物加入到含有乳化剂的惰性溶剂，从而形成其中组分（a），（b）和（c）保持非交联形式的粉末状热固化反应混合物。本发明还涉及热固化反应混合物用于制备高品质聚氨酯聚脲塑料的用途。

48. 发明授权

US5064600A Process for production of moldings or films from polyisocyanate polyadducts by rim procedure 失效
标题翻译：通过RIM程序从聚异氰酸酯多糖生产模具或薄膜的工艺
公开(公告)号：US5064600A
公开(公告)日：1991-11-12
申请号：US614798
申请日：1990-11-14
申请人： Joachim Wagner , Werner Rasshofer , Ulrich Eisele , Eberhard Jurgens , Christian Weber , Erich Meier
发明人： Joachim Wagner , Werner Rasshofer , Ulrich Eisele , Eberhard Jurgens , Christian Weber , Erich Meier
IPC分类号： C08G18/65 , B29C43/00 , B29K75/00 , C08G18/10 , C08G18/50 , C08G18/66 , C08G18/80
CPC分类号： C08G18/8019 , C08G18/10 , C08G18/5048 , C08G18/6685 , C08G2120/00
摘要： The present invention relates to a process for the preparation of moldings or films based on polyisocyanate polyadducts comprising thermoplastically molding, at a temperature of at least 50.degree. C. and at a pressure of at least 5 bar, polyisocyanate polyadducts obtained by reacting in closed molds using the reaction injection molding technique aromatic polyisocyanates; compounds having a molecular weight of from 1800 to 12,000 and containing on a statistical average at least 2.5 isocyanate-reactive groups; and one or more components selected from a diamine containing two primary and/or secondary aromatically bound amino groups and and an aliphatic or cycloaliphatic polyol or polyamine; with the provisos that the quantity of isocyanate-reactive compound is at least 30% by weight based on the total quantity of the components and that at least one of the diamine, polyol, or polyamine components comprises at least 5% by weight based on the weight of the isocyanate-reactive compound.
摘要翻译：本发明涉及一种用于制备基于多异氰酸酯多加成物的模制品或薄膜的方法，所述方法包括在至少50℃和至少5巴的压力下热塑性模塑，所述多异氰酸酯加合物通过在封闭模具使用反应注塑技术芳族聚异氰酸酯; 化合物的分子量为1800至12,000，并且统计平均含有至少2.5个异氰酸酯反应性基团; 和选自含有两个伯和/或二个芳族结合氨基的二胺的一种或多种组分和脂族或脂环族多元醇或多胺; 条件是异氰酸酯反应性化合物的量基于组分的总量为至少30重量％，并且至少一种二胺，多元醇或多胺组分包含至少5重量％，基于异氰酸酯反应性化合物的重量。

49. 发明授权

US5009950A Composite structures 失效
标题翻译：复合结构
公开(公告)号：US5009950A
公开(公告)日：1991-04-23
申请号：US323454
申请日：1989-03-14
申请人： Joachim Wagner , Karl Peltzer , Werner Rasshofer
发明人： Joachim Wagner , Karl Peltzer , Werner Rasshofer
IPC分类号： B32B25/14 , B32B18/00 , B32B27/08 , B32B27/40 , C08G18/50 , C08G18/65
CPC分类号： B32B27/08 , Y10T428/2495 , Y10T428/263 , Y10T428/31551 , Y10T442/67
摘要： The present invention is directed to composite structures by thermoplastically shaping an assembly of at least two flat thermoplastically formable plastic materials placed in layers one above the other and optionally at least one upper, lower and/or intermediate layer containing a reinforcing or filler material under such conditions of temperature and pressure that shaping is accompanied by intimate union of the individual layers of the assembly, characterized in that at least one of the flat plastic materials is based on a polyisocyanate polyaddition product having a density of at least 0.8 g/cm.sup.3 which has been prepared by the reaction of(a) aromatic polyisocyanates,(b) compounds having a molecular weight of 1800 to about 12000 and containing a statistical average of at least 2.5 isocyanate-reactive groups, optionally(c) diamines in the molecular weight range of 108 to 400 containing two primary and/or secondary aromatically bound amino groups, and optionally(d) (cyclo)alkanepolyols and/or (cyclo)alkanepolyamines in the molecular weight range of 60 to 1799 optionally containing ether groups,by a single stage or multi-stage process at an isocyanate index of 60 to 140, wherein at least one of components (c) or (d) is used in a quantity such that the total quantity of components (c) and (d) is at least 5% by weight, based on the weight of component (b).
摘要翻译：本发明涉及复合结构，其通过将至少两个平坦的可塑成形塑料材料的组件热塑成形，一个层叠在另一层之上，以及任选地至少一层含有增强或填充材料的上，下和/或中间层温度和压力的条件是成形伴随着组件的各个层的紧密结合，其特征在于，所述扁平塑料材料中的至少一种基于密度为至少0.8g / cm 3的多异氰酸酯加聚产物，其具有通过（a）芳族多异氰酸酯的反应制备，（b）分子量为1800至约12000的化合物，并且含有至少2.5个异氰酸酯反应性基团的统计平均值，任选（c）分子量范围内的二胺 108至400，其含有两个伯和/或二次芳香结合的氨基，以及任选的（d）（环）烷撑多糖通过在异氰酸酯指数为60至140的单级或多级方法，任选地含有醚基的分子量范围为60至1799的（环）链烷多胺和/或（环）链烷多胺，其中至少一种组分（c）或（d）的使用量使得组分（c）和（d）的总量基于组分（b）的重量为至少5重量％。

50. 发明授权

US4843107A Process for the preparation of polyamines and their use for the preparation of polyurethanes 失效
标题翻译：制备多胺的方法及其用于制备聚氨酯的用途
公开(公告)号：US4843107A
公开(公告)日：1989-06-27
申请号：US173204
申请日：1988-03-24
申请人： Andreas Ruckes , Werner Rasshofer , Klaus Konig , Richard Kopp
发明人： Andreas Ruckes , Werner Rasshofer , Klaus Konig , Richard Kopp
IPC分类号： C08G18/64 , C08G18/10 , C08G18/50 , C08G73/02
CPC分类号： C08G18/5048 , C08G18/10
摘要： Polyamines containing primary amino groups are made by a one-shot process for the hydrolysis of prepolymers containing isocyanate end groups and having an isocyanate content of from 0.5 to 40 weight % with 0.75 to 40 mol of water per equivalent of isocyanate groups in the presence of very small quantities of sodium hydroxide in certain organic, polar solvents. The compounds containing isocyanate groups used for this process are isocyanate prepolymers (preferably containing urethane groups). Hydrolysis according to this process leads directly to the polyamines with elimination of carbon dioxide. These polyamines may be isolated by the usual methods and the removal of the small quantities of catalyst may advantageously be omitted. These polyamines are useful for the preparation of polyurethane(urea)s.
摘要翻译：含有伯氨基的多胺通过一步法制备，用于水解包含异氰酸酯端基并且异氰酸酯含量为0.5至40重量％的预聚物，每当异氰酸酯基为0.75至40摩尔水时，某些有机极性溶剂中极少量的氢氧化钠。用于该方法的含有异氰酸酯基团的化合物是异氰酸酯预聚物（优选含有氨基甲酸酯基团）。根据该方法的水解直接导致多胺消除二氧化碳。这些多胺可以通过常规方法分离，并且可以有利地省略少量催化剂的去除。这些多胺可用于制备聚氨酯（尿素）。

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