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41. 发明授权

US07304182B2 Crystalline parahydroxybenzoic acid anhydride and process for preparing the same 有权
标题翻译：结晶对羟基苯甲酸酐及其制备方法
公开(公告)号：US07304182B2
公开(公告)日：2007-12-04
申请号：US10553451
申请日：2004-04-12
申请人： Ryuzo Ueno , Masaya Kitayama , Nobutaka Izumichi , Masaharu Kittaka
发明人： Ryuzo Ueno , Masaya Kitayama , Nobutaka Izumichi , Masaharu Kittaka
IPC分类号： C07C51/56
CPC分类号： C07C51/43 , C07B2200/13 , C07C65/03
摘要： The present invention provides a process for preparing crystalline parahydroxybenzoic acid anhydride, comprising the step of precipitating and isolating parahydroxybenzoic acid in an aqueous solvent at a temperature equal to or above the transition temperature of parahydroxybenzoic acid.
摘要翻译：本发明提供一种制备结晶对羟基苯甲酸酐的方法，包括在等于或高于对羟基苯甲酸的转变温度的温度下在水性溶剂中沉淀和分离对羟基苯甲酸的步骤。

42. 发明申请

US20050043564A1 Process for dehydrating hydrous sodium beta-naphtholate 审中-公开
标题翻译：脱水含水β-萘酚钠的方法
公开(公告)号：US20050043564A1
公开(公告)日：2005-02-24
申请号：US10915354
申请日：2004-08-11
申请人： Ryuzo Ueno , Masaya Kitayama , Nobutaka Izumichi , Akira Obata
发明人： Ryuzo Ueno , Masaya Kitayama , Nobutaka Izumichi , Akira Obata
IPC分类号： C07C37/70 , C07C39/235 , C07C51/15 , C07C65/11 , C07C37/68
CPC分类号： C07C51/15 , C07C65/11
摘要： The present invention provides a process for dehydrating hydrous sodium β-naphtholate comprising: the step of heating the hydrous sodium β-naphtholate or a mixture of the hydrous sodium β-naphtholate and β-naphthol which comprises no more than 0.2 mole of β-naphthol per one mole of sodium β-naphtholate in a solvent at a temperature of 260-300° C. under an inert gas. The process makes it possible to dehydrate hydrous sodium β-naphtholate thoroughly in a short time with less production of tarry components.
摘要翻译：本发明提供了一种脱水含水β-萘酚钠的方法，包括：加氢含水β-萘酚钠或β-萘酚钠水合β-萘酚的混合物的步骤，其包含不超过0.2摩尔β-萘酚每摩尔β-萘酚钠在溶剂中，在惰性气体下，温度为260-300℃。该方法使得可以在短时间内彻底地脱水β-萘酚钠水合物，同时产生较少的焦油组分。

43. 发明授权

US06673962B2 Granule of parahydroxybenzoic acid or parahydroxybenzoic ester and process for producing the same 有权
标题翻译：对羟基苯甲酸或对羟基苯甲酸酯的颗粒及其制备方法
公开(公告)号：US06673962B2
公开(公告)日：2004-01-06
申请号：US10311633
申请日：2002-12-18
申请人： Ryuzo Ueno , Masaya Kitayama , Nobutaka Izumichi , Masaharu Kittaka
发明人： Ryuzo Ueno , Masaya Kitayama , Nobutaka Izumichi , Masaharu Kittaka
IPC分类号： C07C6501
CPC分类号： C07C65/03 , C07C69/88
摘要： Granular product of parahydroxybenzoic acid or its ester which exhibits well suppressed dusting and caking tendency and a process for preparing the product are provided. The granular product of parahydroxybenzoic acid or its ester according to the instant invention has an average particle size of equal to or more than 150 &mgr;m and a hardness of 10-3000 g. The granular product of the invention can be prepared by dry compressing powdery parahydroxybenzoic acid or its ester to give compressed material, pulverizing and classifying the material.
摘要翻译：提供了显示良好抑制粉尘和结块倾向的对羟基苯甲酸或其酯的颗粒产物和制备该产品的方法。本发明的对羟基苯甲酸或其酯的粒状产物的平均粒径为150μm以上，硬度为10〜3000g。本发明的颗粒状产品可以通过干燥压制粉末状的对羟基苯甲酸或其酯来制备，得到压缩材料，粉碎和分级材料。

44. 发明授权

US06562998B1 Granules of 2-hydroxynaphthalene-3-carboxylic acid and method for preparing the same 有权
标题翻译： 2-羟基萘-3-羧酸颗粒及其制备方法
公开(公告)号：US06562998B1
公开(公告)日：2003-05-13
申请号：US09869143
申请日：2001-06-26
申请人： Ryuzo Ueno , Masaya Kitayama , Nobutaka Izumichi , Syungo Nara , Masaharu Kittaka
发明人： Ryuzo Ueno , Masaya Kitayama , Nobutaka Izumichi , Syungo Nara , Masaharu Kittaka
IPC分类号： C07C6334
CPC分类号： C07C65/11
摘要： Granular product of 2-hydroxynaphthalene-3-carboxylic acid with well-suppressed dusting tendency, and process for preparing the same is provided. Granular product of 2-hydroxynaphthalene-3-carboxylic acid having an average particle size of 150 &mgr;m or more and a hardness of 70-3000 g, and a process for preparing the same comprising the steps of dry compressing powdery 2-hydroxynaphthalene-3-carboxylic acid to give compressed material and pulverizing and classifying the same.
摘要翻译：提供具有良好抑制粉尘倾向的2-羟基萘-3-羧酸的颗粒产物及其制备方法。平均粒度为150μm以上的2-羟基萘-3-羧酸的粒状产物和硬度为70-3000g，其制备方法包括以下步骤：将粉末状2-羟基萘-3-羧酸干燥，得到压缩材料并粉碎和分级。

45. 发明授权

US6020470A Water-soluble azo compounds and process for producing the same 失效
标题翻译：水溶性偶氮化合物及其制备方法
公开(公告)号：US6020470A
公开(公告)日：2000-02-01
申请号：US254949
申请日：1999-03-22
申请人： Ryuzo Ueno , Masaya Kitayama , Kenji Minami , Masaharu Kittaka
发明人： Ryuzo Ueno , Masaya Kitayama , Kenji Minami , Masaharu Kittaka
IPC分类号： C09B62/008 , C09B62/085 , C09B62/245 , D06P1/382
CPC分类号： C09B62/0083 , C09B62/085 , C09B62/245
摘要： The present invention provides novel water-soluble azo compounds derived from 2-hydroxynaphthalene-3,6-dicarboxylic acid or derivatives thereof and diazonium salts having sulfo group(s). These compounds are useful as raw materials for dyes having excellent dyeing properties and fastness.
摘要翻译： PCT No.PCT / JP98 / 03750 Sec。 371日期1999年3月22日 102（e）1999年3月22日PCT提交1998年8月25日PCT公布。出版物WO99 / 11717 1999年3月11日本发明提供了由2-羟基萘-3,6-二羧酸或其衍生物衍生的新型水溶性偶氮化合物和具有磺基的重氮盐。这些化合物可用作染色性和牢度优异的染料的原料。

46. 发明授权

US5847233A Naphthol derivatives and process for producing the same 失效
标题翻译：萘酚衍生物及其制备方法
公开(公告)号：US5847233A
公开(公告)日：1998-12-08
申请号：US975189
申请日：1997-11-20
申请人： Ryuzo Ueno , Shigeru Ito , Kenji Minami , Masaya Kitayama
发明人： Ryuzo Ueno , Shigeru Ito , Kenji Minami , Masaya Kitayama
IPC分类号： C07C65/11 , C07C65/24 , C07C69/94 , C07C235/64 , C07C235/66 , C07C275/54 , C07C311/46 , C07D209/88 , C07D235/26 , C07C39/14
CPC分类号： C07C235/64 , C07C235/66 , C07C275/54 , C07C311/46 , C07C65/11 , C07C65/24 , C07C69/94 , C07D209/88 , C07D235/26 , C07C2103/24
摘要： A naphthol derivative represented by the general formula (I) �wherein Y and Y' indicate --(CONH).sub.n --X or --COR; X is a phenyl group, a naphthyl group, an anthraquinonyl group, a benzimidazolonyl group or a carbazolyl group; R is a hydroxyl group, an alkoxy group having 1 to 6 carbon atoms, a halogen atom, a benzyloxy group, a phenyloxy group or a phenacyloxy group; R.sub.2 is a hydrogen atom, an alkaline metal, an alkyl group having 1 to 6 carbon atoms, an acyl group having 1 to 6 carbon atoms or a phenylalkyl group; Z is a group selected from the group consisting of a hydrogen atom, a halogen atom, a nitro group, a nitroso group and an amino group (Z may be substituted on any ring of the naphthalene ring); and n is an integer of 1 or 2; provided that R.sub.2 and Z do not simultaneously indicate a hydrogen atom when both R simultaneously indicate a hydroxyl group!, and a process for producing the same. This naphthol derivative can be used as raw materials for synthesis, such as dyes, pigments, photosensitive materials and the like. ##STR1##
摘要翻译：由通式（I）表示的萘酚衍生物[其中Y和Y'表示 - （CONH）n -X或-COR; X是苯基，萘基，蒽醌基，苯并咪唑啉基或咔唑基; R为羟基，碳原子数为1〜6的烷氧基，卤原子，苄氧基，苯氧基或苯甲酰氧基。 R2是氢原子，碱金属，碳原子数1〜6的烷基，碳原子数1〜6的酰基或苯基烷基; Z是选自氢原子，卤素原子，硝基，亚硝基和氨基的基团（Z可以在萘环的任意环上被取代）; n为1或2的整数; 条件是当两个R同时表示羟基时，R2和Z不同时表示氢原子]及其制备方法。该萘酚衍生物可以用作合成原料，如染料，颜料，感光材料等。（一）

47. 发明授权

US5770766A Method for separating and purifying hydroxynaphtalenecarboxylic acids 失效
标题翻译：羟基萘甲酸分离纯化方法
公开(公告)号：US5770766A
公开(公告)日：1998-06-23
申请号：US860803
申请日：1997-07-10
申请人： Ryuzo Ueno , Masaya Kitayama , Kuniyo Yanagawase , Yoshiro Uchiyama , Shigeji Mori
发明人： Ryuzo Ueno , Masaya Kitayama , Kuniyo Yanagawase , Yoshiro Uchiyama , Shigeji Mori
IPC分类号： C07C51/47 , C07C63/34
CPC分类号： C07C51/47
摘要： The present invention provides a method for effectively separating independent hydroxynaphthalene-carboxylic acids by treating a mixture containing various kinds of hydroxynaphthalene-carboxylic acids with nonionic porous synthetic adsorbents having as a basic structure aromatic copolymers mainly composed of styrene and divinyl benzene or methacryl copolymers mainly composed of monomethacrylates and dimethacrylates.
摘要翻译： PCT No.PCT / JP96 / 03314 Sec。 371日期1997年7月10日 102（e）1997年7月10日PCT PCT 1996年11月12日PCT公布。公开号WO97 / 18182 日期1997年5月22日本发明提供了一种通过用主要由苯乙烯和二乙烯基苯构成的芳族共聚物作为碱性结构的非离子多孔合成吸附剂处理含有各种羟基萘羧酸的混合物来有效分离独立的羟基萘羧酸的方法，主要由单甲基丙烯酸酯和二甲基丙烯酸酯组成的甲基丙烯酸共聚物。

48. 发明授权

US07355071B2 Method for preparing 2,6-naphthalene dicarboxylic acid 有权
标题翻译： 2,6-萘二甲酸的制备方法
公开(公告)号：US07355071B2
公开(公告)日：2008-04-08
申请号：US11090054
申请日：2005-03-28
申请人： Masaya Kitayama , Hiroyuki Wakamori
发明人： Masaya Kitayama , Hiroyuki Wakamori
IPC分类号： C07C51/42
CPC分类号： C07C51/09 , C07C63/38
摘要： Disclosed is an improved method for preparing 2,6-naphthalene dicarboxylic acid from di-lower alkyl 2,6-naphthalene dicarboxylate, which is characterized in that hydrolyzing di-lower alkyl 2,6-naphthalene dicarboxylate in a specified amount of water in the presence of specified amount of hydrophobic organic solvent and an additive; that hydrolyzing di-lower alkyl 2,6-naphthalene dicarboxylate in a specific amount of a mixed solvent of non-water miscible alcohol and water; or in that di-lower alkyl 2,6-naphthalene dicarboxylate is hydrolyzed in two steps wherein the 1st step comprises hydrolyzing said ester in a water miscible organic solvent in the presence of a small amount of water, and the 2nd step comprises further hydrolyzing the reaction.
摘要翻译：本发明公开了一种从2,6-二萘基二羧酸二低级烷基酯制备2,6-萘二羧酸的改进方法，其特征在于将2,6-萘二羧酸二低级烷基酯在规定量的水中存在规定量的疏水性有机溶剂和添加剂; 在特定量的非水混溶性醇和水的混合溶剂中水解2,6-萘二甲酸二低级烷基酯; 或者在2,6-二羧酸二低级烷基酯中以两个步骤水解，其中第一步包括在少量水存在下在水混溶性有机溶剂中水解所述酯，第二步包括进一步水解反应。

49. 发明授权

US06664341B2 Liquid-crystal polyester resin composition 有权
公开(公告)号：US06664341B2
公开(公告)日：2003-12-16
申请号：US10009639
申请日：2001-12-14
申请人： Masaya Kitayama , Kiichi Kometani , Naoshi Saito
发明人： Masaya Kitayama , Kiichi Kometani , Naoshi Saito
IPC分类号： C08L6703
CPC分类号： C08G63/605 , C08G63/065 , C08G63/60
摘要： A liquid crystal polyester resin composition which suppresses the formation of a blister caused by a heat treatment at a high temperature and has excellent moldability. This composition comprises (A) a liquid crystal polyester comprising at least two aromatic oxycarbonyl recurring units and (B) a liquid crystal polyester comprising at least two aromatic oxycarbonyl recurring units, at least one aromatic dioxy recurring unit and at least one aromatic dicarbonyl recurring unit. The weight ratio of the liquid crystal polyester (A) to the liquid crystal polyester (B) is 90/10 to 30/70.

50. 发明申请

US20050256289A1 Method for joining liquid-crystalline polyester resin composition parts and jointed article made of liquid-crystalline polyester resin composition 有权
标题翻译：液晶聚酯树脂组合物部分的接合方法和由液晶聚酯树脂组合物制成的接合体
公开(公告)号：US20050256289A1
公开(公告)日：2005-11-17
申请号：US11125240
申请日：2005-05-10
申请人： Masaya Kitayama , Naoshi Saito
发明人： Masaya Kitayama , Naoshi Saito
IPC分类号： C08J5/12 , C08G63/60 , F16B19/00 , C08G63/00
CPC分类号： C08G63/605 , B29C65/02 , B29C65/04 , B29C65/06 , B29C65/0672 , B29C65/08 , B29C65/222 , B29C65/224 , B29C65/36 , B29C65/38 , B29C66/126 , B29C66/54 , B29C66/71 , B29C66/721 , B29C66/7212 , B29C66/73115 , B29C66/73776 , B29C66/73921 , B29C66/73941 , B29K2509/10 , B29K2067/00 , B29K2309/08 , B29K2309/02 , B29K2307/04 , B29K2277/10
摘要： The present invention provides a method for joining liquid-crystalline polyester resin composition parts, characterized in that the melting point of the liquid crystalline polyester resin measured by differential scanning calorimeter is 190-250° C. and that the parts are jointed by means of welding. By using the method of the present invention, jointed articles with sufficient joint strength are provided with accuracy.
摘要翻译：本发明提供了一种用于接合液晶聚酯树脂组合物部件的方法，其特征在于用差示扫描量热计测量的液晶聚酯树脂的熔点为190-250℃，通过焊接将部件接合。通过使用本发明的方法，提供了具有足够接合强度的接合制品。

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