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41. 发明授权

US08704020B2 Catalytic hydrothermal treatment of biomass 有权
标题翻译：催化水热处理生物质
公开(公告)号：US08704020B2
公开(公告)日：2014-04-22
申请号：US13285787
申请日：2011-10-31
申请人： Virginia M. Roberts , Michel Daage , James R. Bielenberg , Paul J. Berlowitz , Paul D. Oldenburg , David C. Long , Halou Oumar-Mahamat
发明人： Virginia M. Roberts , Michel Daage , James R. Bielenberg , Paul J. Berlowitz , Paul D. Oldenburg , David C. Long , Halou Oumar-Mahamat
IPC分类号： C07C1/00
CPC分类号： C10G3/50 , C10G3/42 , C10G3/44 , C10G3/45 , C10G3/52 , C10G3/62 , C10G45/08 , C10G45/26 , C10G45/50 , C10G47/06 , C10G65/12 , C10G2300/1011 , C10G2300/1014 , C10G2300/1018 , C10G2300/201 , C10G2300/202 , C10G2300/205 , C10G2300/4081 , C10G2300/44 , C10G2300/70 , C10G2300/805 , C10G2400/02 , C10G2400/04 , C10G2400/10 , Y02P30/20
摘要： Biomass based feeds are processed under hydrothermal treatment conditions, e.g., to produce a hydrocarbon liquid product and a solids portion. The hydrothermal treatment is performed in the presence of a dissolved catalyst or catalyst precursor. The presence of the dissolved catalyst or catalyst precursor can modify the nature of the hydrocarbon products produced from the hydrothermal treatment.
摘要翻译：基于生物质的饲料在水热处理条件下进行处理，例如产生烃液体产物和固体部分。在溶解的催化剂或催化剂前体的存在下进行水热处理。溶解的催化剂或催化剂前体的存在可以改变由水热处理产生的烃产物的性质。

42. 发明申请

US20140024869A1 PRODUCTION OF LUBRICANT BASE OILS FROM BIOMASS 有权
标题翻译：从生物量生产润滑油基础油
公开(公告)号：US20140024869A1
公开(公告)日：2014-01-23
申请号：US13917743
申请日：2013-06-14
申请人： Virginia M. Roberts , Michel Daage , Paul D. Oldenburg , Suzzy C. Ho , Kun Wang , Bradley R. Fingland
发明人： Virginia M. Roberts , Michel Daage , Paul D. Oldenburg , Suzzy C. Ho , Kun Wang , Bradley R. Fingland
IPC分类号： C07C1/207
CPC分类号： C07C1/2076 , B01J21/12 , B01J23/02 , B01J23/10 , C10G3/44 , C10G3/50 , C10G29/22 , C10G2300/1014 , C10G2300/1018 , C10G2400/10 , C11C3/00 , Y02E50/13 , Y02P30/20
摘要： Methods are provided for processing glycerides to form lubricant boiling range molecules in a single reactor and/or a single reaction zone. The glycerides are exposed to catalysts that are stable under the conditions present in the reaction zones during conversion of glycerides to fatty ketones via a coupling reaction in the presence of a first catalyst, and the subsequent deoxygenation and isomerization of the ketones in the presence of a second dewaxing catalyst. The glyceride-containing feedstock can further include free fatty acids or fatty acid derivatives that can also be used for formation of ketones and subsequent deoxygenation and isomerization. In some configuration, the processing can occur in a single reaction zone containing mixed beds of the first and second catalyst. Such configurations can be used to control the ratio of diesel boiling range molecules versus lubricant boiling range molecules generated by the methods.
摘要翻译：提供了用于处理甘油酯以在单个反应器和/或单个反应区中形成润滑剂沸程分子的方法。将甘油酯暴露于在第一催化剂存在下通过偶联反应将甘油酯转化成脂肪酮的反应区中存在的条件下稳定的催化剂，以及随后在存在下的酮的脱氧和异构化第二脱蜡催化剂。含甘油酯的原料还可以包括游离脂肪酸或脂肪酸衍生物，其还可用于形成酮和随后的脱氧和异构化。在一些配置中，处理可以发生在包含第一和第二催化剂的混合床的单个反应区中。这种配置可用于控制柴油沸程分子与通过该方法产生的润滑剂沸程分子的比例。

43. 发明授权

US08617383B2 Integrated hydrocracking and dewaxing of hydrocarbons 有权
标题翻译：烃的综合加氢裂化和脱蜡
公开(公告)号：US08617383B2
公开(公告)日：2013-12-31
申请号：US13169616
申请日：2011-06-27
申请人： Krista Marie Prentice , Michel Daage , Ajit Bhaskar Dandekar , Christopher Gordon Oliveri , Rohit Vijay , Stephen J. McCarthy , Wenyih F. Lai , Bradley R. Fingland
发明人： Krista Marie Prentice , Michel Daage , Ajit Bhaskar Dandekar , Christopher Gordon Oliveri , Rohit Vijay , Stephen J. McCarthy , Wenyih F. Lai , Bradley R. Fingland
IPC分类号： C10G45/64 , C10G45/02 , C10G65/02 , C10G47/00
CPC分类号： C10G65/043 , C10G45/06 , C10G45/08 , C10G45/44 , C10G45/52 , C10G45/58 , C10G45/62 , C10G45/64 , C10G47/16 , C10G47/18 , C10G65/046 , C10G65/12 , C10G69/02 , C10G2300/202 , C10G2300/302 , C10G2300/4018 , C10G2300/4081 , C10G2400/02 , C10G2400/04 , C10G2400/10
摘要： An integrated process for producing naphtha fuel, diesel fuel and/or lubricant base oils from feedstocks under sour conditions is provided. The ability to process feedstocks under higher sulfur and/or nitrogen conditions allows for reduced cost processing and increases the flexibility in selecting a suitable feedstock. The sour feed can be delivered to a catalytic dewaxing step without any separation of sulfur and nitrogen contaminants, or with only a high pressure separation so that the dewaxing still occurs under sour conditions. Various combinations of hydrotreating, catalytic dewaxing, hydrocracking, and hydrofinishing can be used to produce fuel products and lubricant base oil products.
摘要翻译：提供了一种在酸性条件下从原料生产石脑油燃料，柴油和/或润滑油基础油的综合方法。在更高硫和/或氮条件下处理原料的能力允许降低成本处理并增加选择合适原料的灵活性。酸进料可以被输送到催化脱蜡步骤，而没有硫和氮污染物的任何分离，或者只有高压分离，使得在酸性条件下仍然发生脱蜡。可以使用加氢处理，催化脱蜡，加氢裂化和加氢精加工的各种组合来生产燃料产品和润滑油基础油产品。

44. 发明申请

US20130341243A1 HYDROCRACKING PROCESS SELECTIVE FOR IMPROVED DISTILLATE AND IMPROVED LUBE YIELD AND PROPERTIES 有权
标题翻译：用于改进蒸馏和改进润滑油和特性的水解工艺选择
公开(公告)号：US20130341243A1
公开(公告)日：2013-12-26
申请号：US14011061
申请日：2013-08-27
申请人： William J. Novak , Robert Allen Bradway , Stuart S. Shih , Timothy Lee Hilbert , Michel Daage
发明人： William J. Novak , Robert Allen Bradway , Stuart S. Shih , Timothy Lee Hilbert , Michel Daage
IPC分类号： C10G65/10
CPC分类号： C10G65/10 , C10G47/18 , C10G49/04 , C10G65/12 , C10G2300/1074 , C10G2300/202 , C10G2300/301 , C10G2300/302 , C10G2300/304 , C10G2300/307 , C10G2300/4018 , C10G2300/4025 , C10G2400/04 , C10G2400/08 , C10G2400/10
摘要： This invention relates to a process involving hydrocracking of a feedstream in which a converted fraction can exhibit relatively high distillate product yields and maintained or improved distillate fuel properties, while an unconverted fraction can exhibit improved properties particularly useful in the lubricant area. In this hydrocracking process, it can be advantageous for the yield of converted/unconverted product for gasoline fuel application to be reduced or minimized, relative to converted distillate fuel and unconverted lubricant. Catalysts and conditions can be chosen to assist in attaining, or to optimize, desirable product yields and/or properties.
摘要翻译：本发明涉及一种包含进料流加氢裂化的方法，其中转化馏分可表现出相对较高的馏出物产物产率和维持或改善的馏出物燃料性质，而未转化的馏分可表现出在润滑剂区域特别有用的改进的性能。在该加氢裂化过程中，相对于转化的馏出物燃料和未转化的润滑剂，可以有利于减少或最小化汽油燃料应用的转化/未转化产物的产率。可以选择催化剂和条件以帮助实现或优化所需的产物产率和/或性能。

45. 发明申请

US20130092598A1 PRODUCTION OFLUBRICATING OIL BASESTOCKS 审中-公开
标题翻译：生产油基油
公开(公告)号：US20130092598A1
公开(公告)日：2013-04-18
申请号：US13547156
申请日：2012-07-12
申请人： Eric D. Joseck , Michael Brian Carroll , David Mentzer , Teck-Mui Hoo , Michel Daage , Ajit Bhaskar Dandekar
发明人： Eric D. Joseck , Michael Brian Carroll , David Mentzer , Teck-Mui Hoo , Michel Daage , Ajit Bhaskar Dandekar
IPC分类号： C10G65/12
CPC分类号： C10G65/12 , C10G45/60 , C10G45/62 , C10G45/64 , C10G47/14 , C10G49/22 , C10G65/14 , C10G2300/1074 , C10G2300/202 , C10G2300/301 , C10G2300/302 , C10G2300/304 , C10G2400/04 , C10G2400/10
摘要： Methods are provided for producing multiple lubricating oil basestocks from a feedstock. Prior to dewaxing, various fractions of the feedstock are exposed to hydrocracking conditions of different severity to produce a higher overall yield of basestocks. The hydrocracking conditions of different severity can represent exposing fractions of a feedstock to different processing conditions, exposing fractions of a feedstock to different amounts of hydrocracking catalyst, or a combination thereof.
摘要翻译：提供了用于从原料生产多个润滑油基础油料的方法。在脱蜡之前，原料的各种馏分暴露于不同强度的加氢裂化条件，以产生较高的基础油料总产率。不同严重程度的加氢裂化条件可以将原料暴露于不同加工条件的馏分，将原料馏分暴露于不同量的加氢裂化催化剂或其组合。

46. 发明申请

US20120209041A1 PROCESSING OF FEEDSTOCKS IN SEPARATED REACTOR VOLUMES 有权
标题翻译：分离反应器体积中的进料处理
公开(公告)号：US20120209041A1
公开(公告)日：2012-08-16
申请号：US13365328
申请日：2012-02-03
申请人： Patrick L. Hanks , Michel Daage
发明人： Patrick L. Hanks , Michel Daage
IPC分类号： C07C1/207
CPC分类号： C10G45/72 , B01J8/0214 , B01J8/0257 , B01J8/0453 , B01J8/0465 , B01J2208/00309 , B01J2208/00938 , B01J2208/025 , C10G3/42 , C10G3/50 , C10G47/36 , C10G49/002 , C10G65/02 , C10G65/14 , C10G2300/1011 , C10G2300/1044 , C10G2300/202 , C10G2300/4081 , Y02P30/20
摘要： Separated volumes can be created in a reactor using interior dividing wall or interior conduit structures. Feedstocks can be hydroprocessed in the separated volumes to allow multiple types of hydroprocessing conditions and/or feeds to be processed in a single reactor. The feedstocks can remain separate for the entire volume of the reactor, or the dividing barrier can end at some intermediate point in the reactor.
摘要翻译：可以在使用内部分隔壁或内部管道结构的反应器中产生分离体积。原料可以在分离的体积中加氢处理，以允许多种类型的加氢处理条件和/或进料在单个反应器中加工。原料可以在反应器的整个体积中保持分开，或者分隔壁可以在反应器中的某个中间点处结束。

47. 发明授权

US06800579B2 Catalyst regeneration 有权
标题翻译：催化剂再生
公开(公告)号：US06800579B2
公开(公告)日：2004-10-05
申请号：US10059926
申请日：2002-01-29
申请人： Michel Daage , Russell John Koveal , Min Chang
发明人： Michel Daage , Russell John Koveal , Min Chang
IPC分类号： B01J3812
CPC分类号： B01J23/96 , B01J23/75 , B01J23/94 , B01J38/10 , B01J38/12 , B01J38/56 , B01J38/68 , B01J2038/005 , C07C1/045 , C07C2523/75 , C10G2/331 , C10G2/332 , C10G2/333 , Y02P20/584 , C07C9/04
摘要： There is provided a process for regenerating the activity of used metal catalysts for the hydrogenation of carbon monoxide comprising decreasing the hydrocarbon content thereof, calcining under an oxidant-containing atmosphere, impregnating with a solution of at least one of a metal compound, calcining under an oxidant-containing atmosphere and activating by contacting with a hydrogen-contacting gas at elevated temperatures to form an active catalyst. The process regenerates and enhances both supported and dispersed active metal (DAM) catalysts. Used catalysts enhanced by the process are initially treated to decrease their hydrocarbon content. The treatment may be carried out in a single reactor, or by carrying out up to all steps after catalyst may be withdrawn from a reactor and returned to at least one reactor, both preferably during operation thereof. Up to all steps may be effected in a subsequent reactor, or in specialized apparatus.
摘要翻译：提供了一种用于再生用于一氧化碳氢化的所用金属催化剂的活性的方法，包括降低其含烃量，在含氧化剂的气氛下煅烧，用至少一种金属化合物的溶液浸渍，在氧化剂的气氛，并通过在高温下与接触氢的气体接触而形成活性催化剂。该方法再生并增强了负载和分散的活性金属（DAM）催化剂。首先处理通过该方法增强的使用的催化剂以降低它们的烃含量。处理可以在单个反应器中进行，或者在催化剂可以从反应器中取出并返回到至少一个反应器之后，最好在其操作期间进行到所有步骤。直到所有步骤都可以在随后的反应器中或在专门的装置中进行。

48. 发明授权

US06777451B2 Catalyst enhancement 有权
标题翻译：催化剂增强
公开(公告)号：US06777451B2
公开(公告)日：2004-08-17
申请号：US10059927
申请日：2002-01-29
申请人： Russell John Koveal , Michel Daage , Charles Harrison Mauldin , Janet Renee Clark
发明人： Russell John Koveal , Michel Daage , Charles Harrison Mauldin , Janet Renee Clark
IPC分类号： C07C2700
CPC分类号： B01J21/063 , B01J23/40 , B01J23/6567 , B01J23/70 , B01J23/75 , B01J23/8896 , B01J23/89 , B01J23/94 , B01J23/96 , B01J38/10 , B01J38/12 , B01J38/56 , B01J38/58 , B01J38/66 , C10G2/332 , C10G2/333
摘要： A process for enhancing metal catalysts for carbon monoxide hydrogenation comprising reducing the catalyst so that at least a portion is in the metallic state, impregnating under a non-oxidative atmosphere with a solution of a salt of at least one metal, optionally in combination with at least one of an ammonium salt, an alkyl ammonium salt, a weak organic acid and ammonia, oxidizing with a gaseous oxidant in the presence of the impregnating solution, and reducing to form an active catalyst. Used catalysts enhanced by the process are initially treated to decrease their hydrocarbon content. The treatment may be carried out in a single reactor, or by carrying out up to all steps after catalyst may be withdrawn from a reactor and returned to at least one reactor, both preferably during operations. Up to all steps may be effected in a subsequent reactor, or in specialized apparatus.
摘要翻译：一种用于增强用于一氧化碳氢化的金属催化剂的方法，包括将催化剂还原为至少一部分处于金属状态，在非氧化性气氛下用至少一种金属的盐溶液浸渍，任选地与至少一种铵盐，烷基铵盐，弱有机酸和氨，在浸渍溶液存在下用气态氧化剂氧化，还原形成活性催化剂。首先处理通过该方法增强的使用的催化剂以降低它们的烃含量。处理可以在单个反应器中进行，或者通过在催化剂可以从反应器中取出并返回到至少一个反应器中，两者优选在操作期间进行到所有步骤。直到所有步骤都可以在随后的反应器中或在专门的装置中进行。

49. 发明授权

US06753351B2 Supported catalyst activation 有权
标题翻译：负载催化剂活化
公开(公告)号：US06753351B2
公开(公告)日：2004-06-22
申请号：US10059918
申请日：2002-01-29
申请人： Janet Renee Clark , Michel Daage , Russell John Koveal
发明人： Janet Renee Clark , Michel Daage , Russell John Koveal
IPC分类号： C07C2700
CPC分类号： C10G2/332 , B01J23/75 , B01J37/0203 , B01J37/14 , B01J37/18 , C10G2/333
摘要： A process for activating a supported metal catalyst or catalyst precursor useful for the hydrogenation of carbon monoxide to form a mixture of hydrocarbons, comprising reducing with a hydrogen-containing gas at elevated temperature so that at least a portion is in the metallic state, impregnating under a non-oxidizing atmosphere with a solution of at least one member selected from the group consisting of ammonium salts, alkyl ammonium salts and weak organic acids, optionally further including ammonia, to the point where it has absorbed a volume of solution equal to at least about 10% of its calculated pore volume, oxidizing with a gaseous oxidant in the presence of the impregnating solution and reducing with hydrogen-containing gas at elevated temperatures to form an active catalyst. The steps beginning with the impregnation may be repeated. Optionally, the catalyst may be calcined after the oxidation step and/or passivated after activation.
摘要翻译：用于活化用于氢化一氧化碳以形成烃混合物的负载型金属催化剂或催化剂前体的方法，包括在高温下用含氢气体还原，使得至少一部分处于金属状态，浸渍在非氧化性气氛，其中选自铵盐，烷基铵盐和弱有机酸中的至少一种的溶液，任选地还包括氨，其吸收一定体积的溶液至少等于至少其计算的孔体积的约10％，在浸渍溶液存在下用气态氧化剂氧化，并在高温下用含氢气体还原形成活性催化剂。可以重复从浸渍开始的步骤。任选地，催化剂可以在氧化步骤之后煅烧和/或在活化后被钝化。

50. 发明授权

US5925239A Desulfurization and aromatic saturation of feedstreams containing refractory organosulfur heterocycles and aromatics 失效
$Desulfurization and aromatic saturation of feedstreams containing refractory organosulfur heterocycles and aromatics$
标题翻译：含有难熔有机硫杂环和芳烃的进料流的脱硫和芳族饱和
公开(公告)号：US5925239A
公开(公告)日：1999-07-20
申请号：US918639
申请日：1997-08-22
申请人： Darryl P. Klein , Michele S. Touvelle , Edward S. Ellis , Carl W. Hudson , Sylvain Hantzer , Jingguang G. Chen , David E. W. Vaughan , Michel Daage , James J. Schorfheide , William C. Baird, Jr. , Gary B. McVicker
发明人： Darryl P. Klein , Michele S. Touvelle , Edward S. Ellis , Carl W. Hudson , Sylvain Hantzer , Jingguang G. Chen , David E. W. Vaughan , Michel Daage , James J. Schorfheide , William C. Baird, Jr. , Gary B. McVicker
IPC分类号： C10G25/00 , C10G45/10 , C10G45/00
CPC分类号： C10G25/003 , C10G45/10
摘要： A process for the hydrodesulfurization (HDS) of multiple condensed ring heterocyclic organosulfur compounds present in petroleum and petrochemical streams and the saturation of aromatics over noble metal-containing catalysts under relatively mild conditions. The noble metal is selected from Pt, Pd, Ir, Rh and polymetallics thereof. The catalyst system also contains a hydrogen sulfide sorbent material.
摘要翻译：存在于石油和石油化学物流中的多种稠环杂环有机硫化合物的加氢脱硫（HDS）和在相对温和的条件下含贵金属的催化剂的芳族化合物的饱和过程。贵金属选自Pt，Pd，Ir，Rh及其多金属。催化剂体系还含有硫化氢吸附剂材料。

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