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41. 发明授权

US4466908A Isopropyl tetramethylindan musk, organoleptic use thereof 失效
标题翻译：异丙基四甲基丹麝香，其感官用途
公开(公告)号：US4466908A
公开(公告)日：1984-08-21
申请号：US431999
申请日：1982-09-30
申请人： Mark A. Sprecker , Robert P. Belko , Roger E. Greene
发明人： Mark A. Sprecker , Robert P. Belko , Roger E. Greene
IPC分类号： C07C5/29 , C07C45/46 , C07C49/792 , C11B9/00
CPC分类号： C11B9/0049 , C07C45/46 , C07C49/792 , C07C5/29
摘要： Described are isopropyl tetramethylindan musks defined according to the generic structure: ##STR1## wherein R.sub.3 and R.sub.4 are each acetyl or methyl with the provisos:(a) one of R.sub.3 or R.sub.4 is methyl;(b) when R.sub.4 is methyl, then R.sub.3 is acetyl and(c) when R.sub.4 is acetyl, R.sub.3 is methyland organoleptic uses thereof in augmenting or enhancing the aroma of perfume compositions, colognes and perfumed articles. Also described is a process for preparing same by means of first rearranging a tetralin derivative defined according to the structure: ##STR2## to form at least one compound defined according to the structure: ##STR3## and then reacting the compound having the structure: ##STR4## with a compound of the genus: ##STR5## wherein Z represents acetoxy, chloro or bromo in order to form at least one compound defined according to the structure: ##STR6## wherein one of R.sub.1 or R.sub.2 is methyl and the other of R.sub.1 or R.sub.2 is hydrogen. The compound defined according to the structure: ##STR7## is a novel compound.
摘要翻译：描述了根据通用结构定义的异丙基四甲基茚满麝香：其中R 3和R 4各自为乙酰基或甲基，条件是：（a）R 3或R 4中的一个为甲基; （b）当R 4为甲基时，R 3为乙酰基，（c）当R 4为乙酰基时，R 3为甲基和感官用途，用于增强或增强香水组合物，古龙水和香料制品的香味。还描述了通过首先重排根据以下结构定义的四氢化萘衍生物来制备其的方法：形成至少一种根据以下结构定义的化合物：，然后使具有以下结构的化合物： IMAGE>具有以下化合物：其中Z表示乙酰氧基，氯或溴，以形成根据以下结构定义的至少一种化合物：其中R1或R2之一为甲基，R1中的另一个为R1 或R2是氢。根据以下结构定义的化合物：是一种新型化合物。

42. 发明授权

US4427708A Use of cyclohexenyl-alpha-alkyl acrolein derivatives in augmenting or enhancing the aroma or taste of foodstuffs 失效
标题翻译：使用环己烯基-α-烷基丙烯醛衍生物来增强或增强食品的香气或味道
公开(公告)号：US4427708A
公开(公告)日：1984-01-24
申请号：US505421
申请日：1983-06-16
申请人： Mark A. Sprecker , Philip T. Klemarczyk , Robert P. Belko
发明人： Mark A. Sprecker , Philip T. Klemarczyk , Robert P. Belko
IPC分类号： A23L27/20 , A24B15/34 , C07C45/74 , C07C45/82 , C07C47/225 , C11B9/00 , A23L1/226
CPC分类号： C11B9/0034 , A24B15/34 , C07C403/14 , C07C45/74 , C07C45/82 , C07C47/225 , C07C2101/16
摘要： Described are cyclohexenyl-alpha-alkyl acrolein derivatives defined according to the generic structure: ##STR1## wherein R.sub.1, R.sub.2, R.sub.3 and R.sub.4 represent hydrogen or methyl with the proviso that one, two or three of R.sub.1, R.sub.2, R.sub.3 and R.sub.4 represent methyl; wherein R.sub.5 represents methyl or ethyl; wherein one of the dashed lines represents a carbon-carbon double bond and the other of the dashed lines represents a carbon-carbon single bond; wherein the wavy lines represent the "cis" or "trans" juxtaposition of the moieties hydrogen, R.sub.5, cyclohexenyl and carboxaldehyde about the carbon-carbon double bond useful for augmenting or enhancing the aroma or taste of foodstuffs or chewing gums.
摘要翻译：描述了根据通用结构定义的环己烯基-α-烷基丙烯醛衍生物：其中R 1，R 2，R 3和R 4表示氢或甲基，条件是R 1，R 2，R 3和R 4中的一个，两个或三个表示甲基 ; 其中R 5表示甲基或乙基; 其中一条虚线表示碳 - 碳双键，另一条虚线表示碳 - 碳单键; 其中波浪线代表可用于增强或增强食品或口香糖香气或味道的碳 - 碳双键部分氢，R 5，环己烯基和甲醛的“顺式”或“反式”并置。

43. 发明授权

US06919477B2 Fruity musk compositions 有权
标题翻译：水果麝香组成
公开(公告)号：US06919477B2
公开(公告)日：2005-07-19
申请号：US10845935
申请日：2004-05-14
申请人： James O. Bledsoe , Michael Britten-Kelly , Mark A. Sprecker , Robert P. Belko , Manfred Pawlak , Michael G. Monteleone
发明人： James O. Bledsoe , Michael Britten-Kelly , Mark A. Sprecker , Robert P. Belko , Manfred Pawlak , Michael G. Monteleone
IPC分类号： A61K8/37 , A61Q13/00 , C07C69/36 , C07C69/38 , C07C69/96 , C11B9/00 , C07C69/34
CPC分类号： C07C69/38 , A61K8/37 , A61Q13/00 , C07C69/36 , C07C69/96 , C07C2601/14 , C11B9/0034
摘要： Novel ester compounds and the use of these esters as a fragrance chemicals, suitable for use in creating fragrance, and scents in items such as perfumes, colognes and personal care products are disclosed.
摘要翻译：公开了新颖的酯化合物和这些酯作为芳香剂的用途，适用于制造香料，以及香料，古龙水和个人护理产品中的香料。

44. 发明授权

US5077273A Epoxyoctahydrodimethylacetonaphthones, and perfumery uses thereof 失效
标题翻译：环氧三氢二甲基螺环酮及其香料用途
公开(公告)号：US5077273A
公开(公告)日：1991-12-31
申请号：US701085
申请日：1991-05-16
申请人： Mark A. Sprecker , Robert P. Belko , Kathleen E. Boardwick
发明人： Mark A. Sprecker , Robert P. Belko , Kathleen E. Boardwick
IPC分类号： C07D303/32 , C11B9/00 , C11D3/50
CPC分类号： C11B9/0076 , C07D303/32 , C11D3/50
摘要： Described are epoxyoctahydrodimethylacetonaphthones defined according to the generic structure: ##STR1## wherein R.sub.1, R.sub.2, R.sub.3 and R.sub.4 each represents methyl or hydrogen with the proviso that one of R.sub.3 or R.sub.4 is methyl and the other of R.sub.3 or R.sub.4 is hydrogen; and perfumery uses thereof in augmenting or enhancing the aroma of perfume compositions, colognes and perfumed articles, including solid or liquid anionic, cationic, nonionic or zwitterionic detergents, fabric softener compositions, fabric softener articles, cosmetic powders, hair preparations and perfumed polymers.
摘要翻译：描述了根据通用结构定义的环氧八氢二甲基乙酮萘酮：其中R 1，R 2，R 3和R 4各自表示甲基或氢，条件是R 3或R 4中的一个为甲基，R 3或R 4中的另一个为氢; 香料和香水制品，包括固体或液体阴离子，阳离子，非离子或两性离子洗涤剂，织物柔软剂组合物，织物柔软剂制品，化妆粉，头发制剂和加香聚合物。

45. 发明授权

US4681976A Process for preparing alkyl substituted and unsubstituted para-carboalkoxy cyclohexanones 失效
标题翻译：制备烷基取代和未取代的对 - 烷氧羰基环己酮的方法
公开(公告)号：US4681976A
公开(公告)日：1987-07-21
申请号：US842783
申请日：1986-03-21
申请人： Mark A. Sprecker , Wilhelmus J. Wiegers , Robert P. Belko , Richard M. Boden
发明人： Mark A. Sprecker , Wilhelmus J. Wiegers , Robert P. Belko , Richard M. Boden
IPC分类号： C08K5/101 , C11B9/00 , C11D3/50 , C07C69/74
CPC分类号： C11D3/50 , C08K5/101 , C11B9/0034
摘要： Described are para-carboalkoxy cyclohexanones defined according to the structure: ##STR1## wherein R.sub.1 represents hydrogen or C.sub.1 -C.sub.7 alkyl and R.sub.2 represents methyl or ethyl and uses thereof in augmenting or enhancing the aroma of consumable materials including foodstuffs, chewing gums, toothpastes, medicinal products, chewing tobaccos, perfume compositions, colognes and perfumed articles (e.g., solid or liquid anionic, cationic, nonionic or zwitterionic detergents, cosmetic compositions, fabric softener compositions, fabric softener articles, hair preparations and perfumed polymers. The compounds defined according to the structure: ##STR2## wherein R.sub.1 ' represents C.sub.4 -C.sub.7 alkyl and R.sub.2 represents methyl or ethyl are novel compounds.
摘要翻译：描述了根据以下结构定义的对 - 烷氧基环己酮：其中R 1表示氢或C 1 -C 7烷基，R 2表示甲基或乙基，并且其用于增强或增强消耗材料的香气，包括食品，口香糖，牙膏，药用产品，咀嚼烟草，香水组合物，古龙水和香料制品（例如固体或液体阴离子，阳离子，非离子或两性离子洗涤剂，化妆品组合物，织物柔软剂组合物，织物柔软剂制品，毛发制剂和加香聚合物。结构：其中R 1'表示C 4 -C 7烷基，R 2表示甲基或乙基是新化合物。

46. 发明授权

US4616095A Isomer-directed process for producing asymmetric ketones using catalytic claisen rearrangement of allylic ethers, intermediates, and uses of products and intermediates of process in perfumery 失效
标题翻译：使用烯丙基醚的催化裂化重排，中间体以及香料中的产品和中间体的产物和中间体来生产不对称酮的异构体定向方法
公开(公告)号：US4616095A
公开(公告)日：1986-10-07
申请号：US765342
申请日：1985-08-13
申请人： Mark A. Sprecker , Robert P. Belko , William L. Schreiber , Michael Licciardello
发明人： Mark A. Sprecker , Robert P. Belko , William L. Schreiber , Michael Licciardello
IPC分类号： C07C43/305 , C07C45/51 , C07C49/21 , C07C49/217 , C11B9/00
CPC分类号： C07C403/16 , C07C43/305 , C07C45/515 , C11B9/0015 , C11B9/0034 , C11B9/0061 , C07C2101/14 , C07C2101/16
摘要： Described is an isomer-directed process for producing asymmetric ketones defined according to the generic structure: ##STR1## wherein one of Z.sub.1 or Z.sub.2 is the moiety: ##STR2## and the other of Z.sub.1 or Z.sub.2 is hydrogen; wherein R.sub.11 and R.sub.21 represent hydrogen or the same or different alkyl or alkenyl with the proviso that R.sub.11 and R.sub.21 are not both hydrogen or wherein R.sub.11 and R.sub.21 taken together:(i) complete a cycloalkyl, cycloalkenyl, bicycloalkyl, mono or polyalkyl cycloakyl or mono or polyalkyl cycloalkenyl ring, or(ii) represent alkylidene, cycloalkenyl alkylidene, aralkylidene, mono or polyalkyl cycloalkenyl alkylidene or mono or polyalkyl aralkylidene;and wherein R.sub.6, R.sub.7 and R.sub.8 are the same or different and each represents hydrogen or methyl, using a catalytic Claisen rearrangement of allylic ethers previously formed by reacting substituted or unsubstituted allylic alcohols defined according to the structure: ##STR3## with dialkyl ketals defined according to the structure: ##STR4## wherein R.sub.4 and R.sub.5 represent the same or different C.sub.1 -C.sub.4 alkyl.Also described are compounds and processes for using same in perfumery defined according the structures: ##STR5## Also described are certain diallylic ethers defined according to the generic structure: ##STR6##
摘要翻译：描述了根据通用结构定义的不对称酮的异构体定向方法：其中Z1或Z2之一为部分：Z1和Z2中的另一个为氢; 其中R11和R21表示氢或相同或不同的烷基或烯基，条件是R11和R21不同时为氢或其中R11和R21一起组合：（i）完成环烷基，环烯基，双环烷基，单或多烷基环烷基或单或聚烷基环烯基环，或（ii）代表亚烷基，环烯基亚烷基，亚烷叉基，单或多烷基环烯基亚烷基或单或多烷基亚烷基; 并且其中R 6，R 7和R 8相同或不同，并且各自表示氢或甲基，使用以前通过使根据以下结构定义的取代或未取代的烯丙基醇反应形成的烯丙基醚的催化Claisen重排：＆lt; IMAGE＆gt; 结构：其中R 4和R 5表示相同或不同的C 1 -C 4烷基。还描述了在根据以下结构定义的香料中使用它们的化合物和方法：其中描述了根据以下结构定义的某些二烯丙基醚：到通用结构：

47. 发明授权

US4576741A Isomer-directed process for producing asymmetric ketones using catalytic Claisen rearrangement of allylic ethers, intermediates, and uses of products and intermediates of process in perfumery 失效
标题翻译：使用烯丙基醚的催化Claisen重排，中间体以及香料中产品和方法中间体的用途来生产不对称酮的异构体定向方法
公开(公告)号：US4576741A
公开(公告)日：1986-03-18
申请号：US671473
申请日：1984-11-14
申请人： Mark A. Sprecker , Robert P. Belko , William L. Schreiber , Michael Licciardello
发明人： Mark A. Sprecker , Robert P. Belko , William L. Schreiber , Michael Licciardello
IPC分类号： C07C43/305 , C07C45/51 , C11B9/00 , C11D3/50 , A61K7/46
CPC分类号： C07C403/16 , C07C43/305 , C07C45/515 , C11B9/0015 , C11B9/0034 , C11B9/0061 , C07C2101/14 , C07C2101/16
摘要： Described in an isomer-directed process for producing asymmetric ketones defined according to the generic structure: ##STR1## wherein one of Z.sub.1 or Z.sub.2 is the moiety: ##STR2## and the other of Z.sub.1 or Z.sub.2 is hydrogen; wherein R.sub.11 and R.sub.21 represent hydrogen or the same or different alkyl or alkenyl with the proviso that R.sub.11 and R.sub.21 are not both hydrogen or wherein R.sub.11 and R.sub.21 taken together:(i) complete a cycloalkyl, cycloalkenyl, bicycloalkyl, mono or polyalkyl cycloalkyl or mono or polyalkyl cycloalkenyl ring, or(ii) represent alkylidene, cycloalkenyl alkylidene, aralkylidene, mono or polyalkyl cycloalkenyl alkylidene or mono or polyalkyl aralkylidene;and wherein R.sub.6, R.sub.7 and R.sub.8 are the same or different and each represents hydrogen or methyl, using a catalytic Claisen rearrangement of allylic ethers previously formed by reacting substituted or unsubstituted allylic alcohols defined according to the structure: ##STR3## with dialkyl ketals defined according to the structure: ##STR4## wherein R.sub.4 and R.sub.5 represent the same or different C.sub.1 -C.sub.4 alkyl.Also described are compounds and processes for using same in perfumery defined according the structures: ##STR5## Also described are certain diallylic ethers defined according to the generic structure: ##STR6##
摘要翻译：描述于根据通用结构定义的用于制备不对称酮的异构体定向方法：其中Z1或Z2之一为部分：Z1或Z2中的另一个为氢; 其中R11和R21表示氢或相同或不同的烷基或烯基，条件是R11和R21不同时为氢或其中R11和R21一起组合：（i）完成环烷基，环烯基，双环烷基，单或多烷基环烷基或单或聚烷基环烯基环，或（ii）代表亚烷基，环烯基亚烷基，亚烷叉基，单或多烷基环烯基亚烷基或单或多烷基亚烷基; 并且其中R 6，R 7和R 8相同或不同，并且各自表示氢或甲基，使用以前通过使根据以下结构定义的取代或未取代的烯丙基醇反应形成的烯丙基醚的催化Claisen重排：＆lt; IMAGE＆gt; 结构：其中R 4和R 5表示相同或不同的C 1 -C 4烷基。还描述了在根据以下结构定义的香水中使用该化合物的化合物和方法：还描述了根据通用物质定义的某些二烯丙基醚结构：

48. 发明授权

US4549982A 1-Oxoalkyl-2-isopropylnorbornane derivatives, uses thereof in augmenting or enhancing the aroma of consumable materials and processes for preparing same 失效
标题翻译： 1-氧代烷基-2-异丙基降冰片烷衍生物，其用于增强或增强消耗材料的香气及其制备方法
公开(公告)号：US4549982A
公开(公告)日：1985-10-29
申请号：US644058
申请日：1984-08-24
申请人： John B. Hall , Mark A. Sprecker , Robert P. Belko , Augustinus G. Van Loveren , Marie R. Hanna
发明人： John B. Hall , Mark A. Sprecker , Robert P. Belko , Augustinus G. Van Loveren , Marie R. Hanna
IPC分类号： C07C31/137 , C07C33/12 , C07C45/62 , C07C45/69 , C07C49/323 , C07C49/553 , C11B9/00 , C07C49/115 , A61K7/46
CPC分类号： C11B9/0046 , C07C31/137 , C07C33/12 , C07C45/62 , C07C45/69 , C07C49/323 , C07C49/553
摘要： Described are 1-oxoalkyl-2-isopropylnorbornane derivatives defined according to the generic structure: ##STR1## wherein X represents a moiety selected from the group consisting of: ##STR2## wherein the dashed line represents a carbon-carbon double bond or a carbon-carbon single bond and wherein R.sub.1 and R.sub.2 represent hydrogen or methyl with the proviso that R.sub.1 and R.sub.2 are not both methyl, and uses thereof in augmenting or enhancing the aroma of consumable materials selected from the group consisting of perfume compositions, colognes and perfumed articles. Also described are processes for preparing said 1-oxoalkyl-2-isopropylnorbornane derivatives by means of a low temperature catalytic Diels Alder reaction or high temperature thermal Diels Alder reaction between a bicyclopentadiene derivative and 2-methyl-3- buten-5-one according to the reaction: ##STR3## wherein R represents methyl or hydrogen.
摘要翻译：描述根据以下通用结构定义的1-氧代烷基-2-异丙基降冰片烷衍生物：其中X表示选自以下的部分：其中虚线表示碳 - 碳双键或碳 - 碳单键，其中R 1和R 2表示氢或甲基，条件是R 1和R 2不是甲基，以及其用于增强或增强从由香料组合物，古龙水和香料制品组成的组中选择的可消耗材料的香气的用途。还描述了通过低温催化Diels Alder反应或双环戊二烯衍生物与2-甲基-3-丁烯-5-酮之间的高温热狄尔斯阿尔德反应制备所述1-氧代烷基-2-异丙基降冰片烷衍生物的方法，根据反应：其中R表示甲基或氢。

49. 发明授权

US4537704A Alkyl substituted and unsubstituted para-carboalkoxy cyclohexanones and organoleptic uses thereof 失效
公开(公告)号：US4537704A
公开(公告)日：1985-08-27
申请号：US563801
申请日：1983-12-21
申请人： Mark A. Sprecker , Wilhelmus J. Wiegers , Robert P. Belko , Richard M. Boden
发明人： Mark A. Sprecker , Wilhelmus J. Wiegers , Robert P. Belko , Richard M. Boden
IPC分类号： C08K5/101 , C11B9/00 , C11D3/50
CPC分类号： C11B9/0034 , C08K5/101 , C11D3/50
摘要： Described are para-carboalkoxy cyclohexanones defined according to the structure: ##STR1## wherein R.sub.1 represents hydrogen or C.sub.1 -C.sub.7 alkyl and R.sub.2 represents methyl or ethyl and uses thereof in augmenting or enhancing the aroma of consumable materials including foodstuffs, chewing gums, toothpastes, medicinal products, chewing tobaccos, perfume compositions, colognes and perfumed articles (e.g., solid or liquid anionic, cationic, nonionic or zwitterionic detergents, cosmetic compositions, fabric softener compositions, fabric softener articles, hair preparations and perfumed polymers. The compounds defined according to the structure: ##STR2## wherein R.sub.1 ' represents C.sub.4 -C.sub.7 alkyl and R.sub.2 represents methyl or ethyl are novel compounds.

50. 发明授权

US4524020A Isopropyl substituted cyclohexenyl methyl ketones and perfumery uses thereof 失效
标题翻译：异丙基取代的环己烯基甲基酮及其香料用途
公开(公告)号：US4524020A
公开(公告)日：1985-06-18
申请号：US643827
申请日：1984-08-24
申请人： Mark A. Sprecker , Robert P. Belko , Augustinus G. Van Loveren , Marie R. Hanna
发明人： Mark A. Sprecker , Robert P. Belko , Augustinus G. Van Loveren , Marie R. Hanna
IPC分类号： C07C45/69 , C07C49/543 , C11B9/00 , A61K7/46 , C07C49/21
CPC分类号： C11B9/0034 , C07C45/69 , C07C49/543
摘要： Described are isopropyl substituted cyclohexenyl methyl ketones defined according to the structure: ##STR1## wherein R.sub.1, R.sub.2, R.sub.11 and R.sub.21 each represents hydrogen or methyl with the provisos that:(a) at least two of R.sub.1, R.sub.21, R.sub.2 and R.sub.11 represent hydrogen;(b) either R.sub.2 is methyl and R.sub.21 is hydrogen or R.sub.21 is methyl and R.sub.2 is hydrogen; and(c) R.sub.1 is methyl only when R.sub.2 is methyl and R.sub.11 is methyl only when R.sub.21 is methyl,as well as uses thereof in augmenting or enhancing the aroma of perfume compositions, colognes and perfumed articles including solid or liquid anionic, cationic, nonionic or zwitterionic detergents, fabric softener compositions, fabric softener articles, hair preparations and perfumed polymers.
摘要翻译：描述了根据以下结构定义的异丙基取代的环己烯基甲基酮：其中R 1，R 2，R 11和R 21各自表示氢或甲基，条件是：（a）R 1，R 21，R 2和R 11中的至少两个表示氢 ; （b）R2是甲基，R21是氢或R21是甲基，R2是氢; 和（c）仅当R 2为甲基时，R 1为甲基，R 21为甲基时，R 21为甲基时，R 11为甲基，以及其用于增强或增强香料组合物，古龙水和香料的芳香物质的用途，包括固体或液体阴离子，阳离子，非离子或两性离子洗涤剂，织物柔软剂组合物，织物柔软剂制品，头发制剂和加香聚合物。

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