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41. 发明申请

US20140039088A1 DENTAL COMPOSITION 审中-公开
标题翻译：牙科成分
公开(公告)号：US20140039088A1
公开(公告)日：2014-02-06
申请号：US13979815
申请日：2011-10-18
申请人： Simon Stelzig , Joachim E. Klee , Andreas Facher , Christoph Weber
发明人： Simon Stelzig , Joachim E. Klee , Andreas Facher , Christoph Weber
IPC分类号： A61K6/087 , A61K6/083
CPC分类号： A61K6/0091 , A61K6/0023 , A61K6/08 , A61K6/083 , A61K6/0835 , A61K6/087 , A61K6/09 , C07C231/02 , C08L33/00 , C08L75/16 , C08L33/10 , C07C233/38
摘要： Dental composition comprising (i) a particulate filler; (ii) a polymerizable hydrolysis-stable compound of the following formula (1) AXn wherein A is a linker group containing at least n nitrogen atoms and optionally one or more acidic groups, X are moieties containing a polymerizable double bond and forming an amide bond with a nitrogen atom of A, which X may be the same or different and are represented by the following formula (2) wherein R1 and R2 are independent from each other and represent a hydrogen atom, a C1-6 alkyl group or a group —(CH2)m—Z, wherein Z is COOM, OPO3M2, PO3M2, SO3M, and M is independently a hydrogen atom or a metal atom, and m is an integer of from 0 to 6, L is a bond, a C1-6 alkylene group; and n is an integer of at least 1; provided that at least one X cannot be a (meth)acryl group; and (iii) an initiator system.
摘要翻译：牙科组合物，其包含（i）颗粒填料; （ii）下式（1）的可聚合水解稳定化合物AXn其中A是至少含有n个氮原子和任选一个或多个酸性基团的连接基团，X是含有可聚合双键并形成酰胺键的部分与A的氮原子一起，X可以相同或不同，并由下式（2）表示，其中R 1和R 2彼此独立地表示氢原子，C 1-6烷基或基团 - （CH 2）m Z，其中Z为COOM，OPO3M2，PO3M2，SO3M和M独立地为氢原子或金属原子，m为0-6的整数，L为键，C1-6亚烷基 ; n为1以上的整数。条件是至少一个X不能是（甲基）丙烯酰基; 和（iii）引发剂体系。

42. 发明申请

US20140039087A1 DENTAL COMPOSITION 有权
标题翻译：牙科成分
公开(公告)号：US20140039087A1
公开(公告)日：2014-02-06
申请号：US13979811
申请日：2011-10-18
申请人： Simon Stelzig , Joachim E. Klee , Andreas Facher , Christoph Weber
发明人： Simon Stelzig , Joachim E. Klee , Andreas Facher , Christoph Weber
IPC分类号： A61K6/083
CPC分类号： A61K6/083 , A61K6/0023 , A61K6/0835 , C07C233/20 , C08L33/00
摘要： Dental composition comprising a water-soluble polymerizable compound of the following formula (1): wherein A is a linear or branched linker group represented by the following formula (3), wherein the nitrogen atom of at least two of the termini forms an amide bond with an X moiety; wherein R′ represents a hydrogen atom or a substituted or unsubstituted aliphatic or cycloaliphatic hydrocarbon group, wherein each R may be the same or different L1, L2, and L3 which may be the same or different, independently represent a single bond, or a C2-20 straight-chain, branched or cyclic hydrocarbon group optionally containing from 1 to 6 heteroatoms selected from nitrogen and oxygen in the backbone of the hydrocarbon group, and optionally from 1 to 6 functional groups selected from carboxylic acid groups or a salt thereof, hydroxyl groups, thiol groups and amino groups, and in case a plurality of L1 and L2 are present, each of L1 and L2 may be the same or different; Q1 and Q2, which may be the same or different, independently represent a single bond or a linkage selected from an amide, a urethane, a urea and a thiourea linkage; k is an integer of at least 0, X are moieties containing a polymerizable double bond and forming an amide bond with a nitrogen atom of A, wherein each X may be the same or different and are represented by the following formula (2): wherein R1 and R2 are independent from each other and represent a hydrogen atom, a C1-6 alkyl group or a group —(CH2)m—COOM, wherein M represents a hydrogen atom or a metal atom, m is an integer of from 0 to 6, L is a bond or a C1-6 alkylene group; and n is an integer of at least 2; (ii) an initiator system; optionally a polyacidic polymer; optionally water and/or a water soluble solvent; and optionally a particulate filler.
摘要翻译： 1.一种牙科用组合物，其含有下述式（1）所示的水溶性聚合性化合物：式中，A为下述通式（3）所示的直链或支链连接基团，其中，所述末端中的至少2个的氮原子形成酰胺键与X部分; 其中R'表示氢原子或取代或未取代的脂族或脂环族烃基，其中每个R可以相同或不同，可以相同或不同的L1，L2和L3独立地表示单键，或C2 -20个直链，支链或环状烃基，任选地含有1至6个选自氮原子和氧的杂原子在烃基的主链中，以及任选地1-6个选自羧酸基团或其盐的官能团，羟基基团，硫醇基和氨基，并且在存在多个L1和L2的情况下，L1和L2中的每一个可以相同或不同; Q1和Q2可以相同或不同，独立地表示单键或选自酰胺，氨基甲酸酯，脲和硫脲键的键; k是至少为0的整数，X是含有可聚合双键并与A的氮原子形成酰胺键的部分，其中每个X可以相同或不同，并由下式（2）表示：其中 R 1和R 2彼此独立地表示氢原子，C 1-6烷基或基团 - （CH 2）m -COOM，其中M表示氢原子或金属原子，m表示0〜 6，L是键或C1-6亚烷基; 且n为至少2的整数; （ii）引发剂体系; 任选的多酸聚合物; 任选的水和/或水溶性溶剂; 和任选的颗粒填料。

43. 发明授权

US08198388B2 One-part self-etching, self-priming dental adhesive composition 有权
标题翻译：一部分自蚀刻，自吸牙科粘合剂组合物
公开(公告)号：US08198388B2
公开(公告)日：2012-06-12
申请号：US10596747
申请日：2004-12-15
申请人： Joachim E. Klee , Uwe Lehmann , Uwe Walz
发明人： Joachim E. Klee , Uwe Lehmann , Uwe Walz
IPC分类号： C08F30/02
CPC分类号： A61K6/0023 , C07F9/091 , C08L33/00 , C08L43/02
摘要： One-part self-etching, self-priming dental adhesive composition having a pH of at most 2, which comprises (a) a polymerizable acidic phosphoric acid ester monomer (b) one or more polymerizable acidic monomers (c) a polymerizable N-substituted alkylacrylic or acrylic acid amide monomer; (d) optionally an organic and/or inorganic acid; (e) an organic water soluble solvent and/or water; and (f) polymerization initiator, inhibitor and stabilizer.
摘要翻译：一部分自蚀刻自粘牙科粘合剂组合物，其pH最多为2，其包含（a）可聚合酸性磷酸酯单体（b）一种或多种可聚合酸性单体（c）可聚合的N-取代的烷基丙烯酸或丙烯酰胺单体; （d）任选的有机和/或无机酸; （e）有机水溶性溶剂和/或水; 和（f）聚合引发剂，抑制剂和稳定剂。

44. 发明授权

US08044113B2 Dental root canal filling material 有权
标题翻译：牙根管填充材料
公开(公告)号：US08044113B2
公开(公告)日：2011-10-25
申请号：US10596742
申请日：2004-12-17
申请人： Joachim E. Klee
发明人： Joachim E. Klee
IPC分类号： A61K6/08
CPC分类号： A61K6/0038 , C08L79/02
摘要： A dental root canal sealing composition curable in the absence of a polymerisation initiator, which comprises (i) an amino terminated prepolymer having a viscosity at 23° C. of less than 100 Pas. (ii) a compound capable of undergoing polyaddition with the aminoterminated prepolymer (i); (iii) 40 to 85 wt.-% of a filler for providing a minimum radioopacity of at least 3 mm/mm Al.
摘要翻译：在不存在聚合引发剂的情况下可固化的牙根管密封组合物，其包含（i）氨基封端的预聚物，其在23℃下的粘度小于100Pa·s。（ii）能够与氨基发生预聚物（i）进行加聚的化合物; （iii）用于提供至少3mm / mm Al的最小放射能力的填料的40至85wt。％。

45. 发明申请

US20100028832A1 Dental device for use in the obturation of a root canal 审中-公开
标题翻译：用于根管封堵的牙科装置
公开(公告)号：US20100028832A1
公开(公告)日：2010-02-04
申请号：US12587347
申请日：2009-10-06
申请人： Andreas E. Gutzner , Joachim E. Klee
发明人： Andreas E. Gutzner , Joachim E. Klee
IPC分类号： A61C5/02
CPC分类号： A61C5/50
摘要： Kit-of-parts containing (i) a dental device for use in the obturation of a root canal which comprises a tapered obturating point portion integrally connected at the distal end of a functional portion, whereby the functional portion comprises (a) a neck portion adjacent to the obturating point portion, and (b) a handle portion, and (ii) a dental sealant composition, wherein the dental device is made of a material obtainable by curing a composition containing one or more curable components contained in the dental sealant.
摘要翻译：零件包含（i）用于根管密封的牙科装置，其包括在功能部分的远端处一体地连接的锥形闭塞点部分，由此所述功能部分包括（a）颈部邻近密闭点部分，和（b）手柄部分，和（ii）牙科密封剂组合物，其中牙科装置由可通过固化含有牙科密封剂中所含的一种或多种可固化组分的组合物获得的材料制成。

46. 发明申请

US20090215922A1 Dental root canal filling cones 审中-公开
标题翻译：牙根管填充锥体
公开(公告)号：US20090215922A1
公开(公告)日：2009-08-27
申请号：US12387173
申请日：2009-04-29
申请人： Joachim E. Klee
发明人： Joachim E. Klee
IPC分类号： A61K6/08
CPC分类号： A61K6/0038 , A61K6/087 , C08L63/00
摘要： Dental root canal filling cones are prepared from a filler and a thermoplastic polymer, wherein the thermoplastic polymer is formed by polymerization of polymerizable diepoxide monomer and amine monomer. The amine monomers are primary monoamine and/or a disecondary diamine. The filler has about 40 to 90 weight-% of the cones providing a radio-opacity of at least 3 mm/mm aluminum.
摘要翻译：牙根管填充锥由填料和热塑性聚合物制备，其中热塑性聚合物通过可聚合的二环氧化物单体和胺单体的聚合而形成。胺单体是伯胺和/或二仲二胺。填料具有约40至90重量％的锥体，其提供至少3mm / mm铝的无线电不透明度。

47. 发明申请

US20090043008A1 Dental adhesive 审中-公开
标题翻译：牙科粘合剂
公开(公告)号：US20090043008A1
公开(公告)日：2009-02-12
申请号：US12148568
申请日：2008-04-21
申请人： Joachim E. Klee , Uwe Lehmann
发明人： Joachim E. Klee , Uwe Lehmann
IPC分类号： A61K6/08
CPC分类号： A61K6/0029 , A61K6/0023 , C08L33/26 , C08L43/02
摘要： A one-part self-etching, self-priming dental adhesive having a pH of at most 2, which comprises an aqueous mixture containing (i) one or more polymerizable monomers optionally containing an acidic group, (ii) optionally one or more organic or inorganic acids, (iii) a polymerization initiator, and (iv) a thermal polymerisation inhibitor of the following formula (I): wherein R′1 represents a hydrogen atom, or a saturated hydrocarbon group having 1 to 18 carbon atoms. R′2, which may be the same or different if more than one R′2 is present, independently represent a saturated hydrocarbon group having 1 to 18 carbon atoms, and c represents an integer of from 1 to 4.
摘要翻译：一种具有pH至多为2的一部分自蚀刻自吸牙科粘合剂，其包含含有（i）一种或多种任选含有酸性基团的可聚合单体的水性混合物，（ii）任选的一种或多种有机或无机酸，（iii）聚合引发剂，和（iv）下式（I）的热聚合抑制剂：其中R'1表示氢原子或具有1至18个碳原子的饱和烃基。 R'2可以相同或不同，如果多于一个R'2存在，独立地表示具有1至18个碳原子的饱和烃基，c表示1至4的整数。

48. 发明申请

US20080274442A1 Laser curable polymerisable composition for the protection of hard tissue 审中-公开
标题翻译：用于保护硬组织的激光可固化聚合组合物
公开(公告)号：US20080274442A1
公开(公告)日：2008-11-06
申请号：US12215821
申请日：2008-06-30
申请人： Joachim E. Klee , Andreas Facher , Christoph Weber , Rolf Mulhaupt , Martin Schmider
发明人： Joachim E. Klee , Andreas Facher , Christoph Weber , Rolf Mulhaupt , Martin Schmider
IPC分类号： A61C5/04 , A61K6/083 , C08F4/34
CPC分类号： A61K6/0017 , C08L33/00 , C08L63/00
摘要： One-component heat-curable sealant composition for the protection of exposed dental surfaces, comprising (a) a polymerisable monomer and/or oligomer which has at least two polymerizable double bonds per molecule, and (b) an initiator system comprising benzoylperoxide in an amount of at least 2 wt.-% based on the total composition.
摘要翻译：用于保护暴露的牙齿表面的单组分可热固化的密封剂组合物，其包含（a）每分子具有至少两个可聚合双键的可聚合单体和/或低聚物，和（b）包含量为过氧化苯甲酰的引发剂体系至少为2重量％。

49. 发明申请

US20080274439A1 Dental device for use in the obturation of a root canal 审中-公开
标题翻译：用于根管封堵的牙科装置
公开(公告)号：US20080274439A1
公开(公告)日：2008-11-06
申请号：US11890411
申请日：2007-08-06
申请人： Andreas E. Gutzner , Joachim E. Klee
发明人： Andreas E. Gutzner , Joachim E. Klee
IPC分类号： A61C5/02 , B65D83/00
CPC分类号： A61C5/50
摘要： Kit-of-parts containing (i) a dental device for use in the obturation of a root canal which comprises a tapered obturating point portion integrally connected at the distal end of a functional portion, whereby the functional portion comprises (a) a neck portion adjacent to the obturating point portion, and (b) a handle portion, and (ii) a dental sealant composition, wherein the dental device is made of a material obtainable by curing a composition containing one or more curable components contained in the dental sealant.
摘要翻译：零件包含（i）用于根管密封的牙科装置，其包括在功能部分的远端处一体地连接的锥形闭塞点部分，由此所述功能部分包括（a）颈部邻近密闭点部分，和（b）手柄部分，和（ii）牙科密封剂组合物，其中牙科装置由可通过固化含有牙科密封剂中所含的一种或多种可固化组分的组合物获得的材料制成。

50. 发明申请

US20080237907A1 Process for the preparation of a polymerizable dental composition 审中-公开
标题翻译：制备可聚合牙科组合物的方法
公开(公告)号：US20080237907A1
公开(公告)日：2008-10-02
申请号：US12156794
申请日：2008-06-04
申请人： Joachim E. Klee , Uwe Walz , Andreas Facher , Christoph Weber , Rolf Mulhaupt , Holger Frey , Ekkehard Muh
发明人： Joachim E. Klee , Uwe Walz , Andreas Facher , Christoph Weber , Rolf Mulhaupt , Holger Frey , Ekkehard Muh
IPC分类号： A61C13/20
CPC分类号： A61K6/083 , A61K6/093 , C08L33/00 , C08L83/10
摘要： A process for the preparation of a polymerizable dental composition comprising the steps of (a) preparing a liquid mixture comprising (i) 1 to 99% w/w of a hybrid monomer component containing at least one hybrid monomer compound having one hydrolysable siloxane group and at least one polymerizable organic moiety, and (ii) 99 to 1% w/w of a monomer component polymerizable with the polymerizable organic moiety of the hybrid monomer compounds; and (b) adding at least a stoichiometrically sufficient amount of water to the mixture to hydrolyse the hydrolysable siloxane group of the hybrid monomer compound and to form spherical polymerizable nanoparticles having an average particle size of from 1 to 100 nm dispersed in the monomer component, whereby the nanoparticles have a structure with Si—O—Si bonds and peripherally exposed polymerizable organic moieties.
摘要翻译：一种制备可聚合牙科用组合物的方法，包括以下步骤：（a）制备液体混合物，其包含（i）1至99％w / w的含有至少一种具有一个可水解硅氧烷基团的杂化单体化合物的杂化单体组分和至少一个可聚合的有机部分，和（ii）99-1％w / w的可与所述杂化单体化合物的可聚合有机部分聚合的单体组分; 和（b）向所述混合物中加入至少一种化学计量的足够量的水以水解所述杂化单体化合物的可水解硅氧烷基团并形成分散在单体组分中的平均粒度为1至100nm的球形可聚合纳米颗粒，由此纳米颗粒具有具有Si-O-Si键和外围暴露的可聚合有机部分的结构。

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