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41. 发明授权

US09150490B2 Process for preparing diaryl carbonates and polycarbonates 有权
标题翻译：制备碳酸二芳基酯和聚碳酸酯的方法
公开(公告)号：US09150490B2
公开(公告)日：2015-10-06
申请号：US13074433
申请日：2011-03-29
申请人： Pieter Ooms , Andreas Bulan
发明人： Pieter Ooms , Andreas Bulan
IPC分类号： C25B1/00 , C25B15/00 , C07C68/02 , C08G64/30
CPC分类号： C07C68/02 , C08G64/307 , C25B1/26 , Y02P20/127 , C07C69/96
摘要： The present invention relates to a process for the continuous preparation of diaryl carbonates from phosgene and at least one monohydroxy compound (monophenol) in the presence of catalysts, and also the use thereof for preparing polycarbonates. The hydrogen chloride formed in the reaction is converted by electrochemical oxidation into chlorine, with the chlorine being recirculated to the preparation of phosgene. In particular, the process comprises utilization of the hydrogen chloride formed for the process for preparing diphenyl carbonate (DPC process).
摘要翻译：本发明涉及在催化剂存在下从光气和至少一种单羟基化合物（单酚）连续制备碳酸二芳酯的方法，以及其用于制备聚碳酸酯的方法。在反应中形成的氯化氢通过电化学氧化转化成氯，氯被再循环到光气的制备中。特别地，该方法包括利用形成的用于制备碳酸二苯酯的方法中的氯化氢（DPC工艺）。

42. 发明授权

US09045837B2 Electrolyser with coiled inlet hose 有权
标题翻译：电磁线圈带入口软管
公开(公告)号：US09045837B2
公开(公告)日：2015-06-02
申请号：US13994042
申请日：2011-11-15
申请人： Peter Woltering , Randolf Kiefer , Rainer Weber , Andreas Bulan
发明人： Peter Woltering , Randolf Kiefer , Rainer Weber , Andreas Bulan
IPC分类号： C25B9/08 , C25B15/08 , C25B1/46
CPC分类号： C25B15/08 , C25B1/46 , C25B9/08 , C25B9/18 , C25B15/06
摘要： Electrolyzer comprising at least one single electrolyzer element which comprises at least one anode compartment with an anode, one cathode compartment with a cathode and one ion exchange membrane arranged between the anode and the cathode compartments, with the anode and/or cathode being a gas diffusion electrode. A gap is provided between the gas diffusion electrode and the ion exchange membrane, with an electrolyte inlet arranged at the upper end of the gap and an electrolyte outlet at the lower end of the gap and a gas inlet and a gas outlet. The electrolyte outlet extending into a discharge header, and the electrolyte inlet connected to an electrolyte feed tank and having an overflow, the overflow connected to the discharge header, with a coiled hose connecting the electrolyte feed tank with the electrolyte inlet and with a coiled hose connecting the overflow with the discharge header.
摘要翻译：电解器包括至少一个单个电解器元件，其包括具有阳极的至少一个阳极室，具有阴极的一个阴极室和布置在阳极和阴极室之间的一个离子交换膜，阳极和/或阴极是气体扩散电极。在气体扩散电极和离子交换膜之间设置有间隙，电解液入口布置在间隙的上端，并且间隙的下端具有电解液出口，气体入口和气体出口。电解液出口延伸到排放集管中，电解质入口连接到电解质进料罐并具有溢流，溢流口连接到排出集管，连接软管将电解质进料罐与电解液入口连接，并且连接软管将溢流与排放管连接。

43. 发明授权

US08747647B2 Process and apparatus for the electrolysis of an aqueous solution of hydrogen chloride or alkali chloride in an electrolytic cell 失效
标题翻译：在电解池中电解氯化氢或氯化碱水溶液的方法和装置
公开(公告)号：US08747647B2
公开(公告)日：2014-06-10
申请号：US13375327
申请日：2010-05-28
申请人： Walter Bachleitner , Christoph Erdmann , Joachim Rohovec , Andreas Bulan , Mathias Weis
发明人： Walter Bachleitner , Christoph Erdmann , Joachim Rohovec , Andreas Bulan , Mathias Weis
IPC分类号： C25B1/26 , C25B1/46 , C25B15/08 , H01M8/04
CPC分类号： C25B15/08 , C25B1/26 , C25B1/46 , H01M8/04097
摘要： In a process for chlorine-alkali electrolysis, use is made of an oxygen depletion cathode. The process is run with a high excess of oxygen. The oxygen needed for this is provided for a device of the gas separation, for example a VPSA plant or an air fractionation plant. The large quantities of oxygen produced lead to considerable costs of the process. According to the invention, the oxygen-rich atmosphere remaining after passing through the process is fed back into the device for gas separation as input gas. The device the gas separation is therefore operated with an oxygen-rich input gas and therefore produces a larger quantity of oxygen-rich gas, which in turn is fed to the oxygen depletion cathode. As a result of the circulation of the gas, the economy of the overall process is increased considerably.
摘要翻译：在氯碱电解的过程中，使用耗氧阴极。该过程以大量的氧气运行。为此需要的氧气用于气体分离装置，例如VPSA装置或空气分馏装置。生产的大量氧气导致了相当大的成本。根据本发明，将通过该工序后剩余的富氧气氛作为输入气体反馈至气体分离装置。因此，气体分离装置用富氧输入气体运行，因此产生更大量的富氧气体，其又被供给到氧耗尽阴极。由于天然气的流通，整体流程的经济性大大增加。

44. 发明申请

US20130236797A1 OXYGEN-CONSUMING ELECTRODE AND METHOD FOR PRODUCING SAME 审中-公开
标题翻译：氧消耗电极及其制造方法
公开(公告)号：US20130236797A1
公开(公告)日：2013-09-12
申请号：US13818832
申请日：2011-08-23
申请人： Andreas Bulan , Norbert Wagner , Gregor Polcyn , Lisa Rossrucker , Michael Marx
发明人： Andreas Bulan , Norbert Wagner , Gregor Polcyn , Lisa Rossrucker , Michael Marx
IPC分类号： C25B11/04
CPC分类号： C25B11/0442 , C25B11/035 , C25B11/0478 , H01M4/8605 , H01M4/921 , H01M12/06
摘要： An oxygen-consuming electrode, in particular for use in chloralkali electrolysis, having a novel catalyst coating and also an electrolysis apparatus are described. Furthermore, its use in chloralkali electrolysis, fuel cell technology or metal/air batteries is described. The oxygen-consuming electrode comprises at least a support which in particular is electrically conductive, a layer containing a catalyst and a hydrophobic layer, characterized in that it contains gallium in addition to silver as catalytically active component.
摘要翻译：描述了一种特别用于氯碱电解的耗氧电极，具有新的催化剂涂层和电解装置。此外，还描述了其在氯碱电解，燃料电池技术或金属/空气电池中的应用。耗氧电极至少包括一种特别是导电的载体，含有催化剂和疏水层的层，其特征在于除了银作为催化活性组分之外，其含有镓。

45. 发明授权

US08318971B2 Process for preparing methylenediphenyl diisocyanates 有权
标题翻译：亚甲基二苯基二异氰酸酯的制备方法
公开(公告)号：US08318971B2
公开(公告)日：2012-11-27
申请号：US12394149
申请日：2009-02-27
申请人： Fritz Pohl , Andreas Bulan , Rainer Weber , Richard Adamson , Matthias Böhm , Christian Six
发明人： Fritz Pohl , Andreas Bulan , Rainer Weber , Richard Adamson , Matthias Böhm , Christian Six
IPC分类号： C07C249/00
CPC分类号： C25B15/08 , C07C209/78 , C07C263/10 , C25B1/26 , C07C211/50 , C07C265/14
摘要： The invention relates to a process for preparing methylenediphenyl diisocyanates which comprises at least the steps: A) reaction of aniline with formaldehyde in the presence of hydrochloric acid as catalyst to give a mixture of diamines and polyamines of the diphenylmethane series (MDA) and subsequent at least partial neutralization of the hydrochloric acid by means of alkali metal hydroxide, B) reaction of the mixture of diamines and polyamines of the diphenylmethane series obtained in step A) with phosgene to give a mixture of diisocyanates and polyisocyanates of the diphenylmethane series (MDI) and hydrogen chloride, wherein C) the hydrochloric acid which has been neutralized in step A) is separated off in the form of a solution containing alkali metal chloride and is subsequently at least partly fed to an electrochemical oxidation to form chlorine, alkali metal hydroxide and optionally hydrogen and D) at least part of the chlorine produced in step C) is used for preparing the phosgene used in step B).
摘要翻译：本发明涉及一种制备亚甲基二苯基二异氰酸酯的方法，其至少包括以下步骤：A）在盐酸作为催化剂存在下苯胺与甲醛的反应，得到二苯基甲烷系列（MDA）的二胺和多胺的混合物，通过碱金属氢氧化物最小程度地中和盐酸，B）将步骤A）中得到的二苯基甲烷系列的二胺和多胺的混合物与光气反应，得到二苯基甲烷系列（MDI）的二异氰酸酯和多异氰酸酯的混合物，和氯化氢，其中C）在步骤A）中已中和的盐酸以含有碱金属氯化物的溶液的形式分离，随后至少部分地进料至电化学氧化以形成氯，碱金属氢氧化物和任选地氢和D）步骤C）中产生的至少一部分氯用于制备磷在步骤B）中使用的烯。

46. 发明申请

US20110245527A1 PROCESS FOR PREPARING DIARYL CARBONATES AND POLYCARBONATES 有权
标题翻译：制备二元碳酸酯和聚碳酸酯的方法
公开(公告)号：US20110245527A1
公开(公告)日：2011-10-06
申请号：US13071944
申请日：2011-03-25
申请人： Pieter Ooms , Andreas Bulan
发明人： Pieter Ooms , Andreas Bulan
IPC分类号： C07C68/02
CPC分类号： C08G64/307 , C01B7/04 , C01B7/0731 , C07C68/02 , Y02P20/127 , C07C69/96
摘要： The present invention relates to a process for the continuous preparation of diaryl carbonates from phosgene and at least one monohydroxy compound (monophenol) in the presence of catalysts, and also the use thereof for preparing polycarbonates. The hydrogen chloride formed in the reaction is converted by thermal oxidation into chlorine, with the chlorine being recirculated to the preparation of phosgene. In particular, the process comprises utilization of the hydrogen chloride formed for the process for preparing diphenyl carbonate (DPC process).
摘要翻译：本发明涉及在催化剂存在下从光气和至少一种单羟基化合物（单酚）连续制备碳酸二芳酯的方法，以及其用于制备聚碳酸酯的方法。反应中形成的氯化氢通过热氧化转化成氯，氯被再循环到光气的制备中。特别地，该方法包括利用形成的用于制备碳酸二苯酯的方法中的氯化氢（DPC工艺）。

47. 发明申请

US20110073491A1 ELECTROCHEMICAL CELL 审中-公开
标题翻译：电化学细胞
公开(公告)号：US20110073491A1
公开(公告)日：2011-03-31
申请号：US12957805
申请日：2010-12-01
申请人： Andreas Bulan , Michael Großholz , Volker Michele , Hans-Joachim Brockhaus , Hans-Dieter Pinter , Fritz Gestermann , Rainer Weber
发明人： Andreas Bulan , Michael Großholz , Volker Michele , Hans-Joachim Brockhaus , Hans-Dieter Pinter , Fritz Gestermann , Rainer Weber
IPC分类号： C25B9/10 , C25B9/08 , C25B1/14 , C25B15/08
CPC分类号： C25B9/08
摘要： The present invention describes an electrochemical cell, comprising at least an anode half-cell with an anode, a cathode half-cell with a cathode, and an ion exchange membrane arranged between the anode half-cell and the cathode half-cell, the anode and/or the cathode is a gas diffusion electrode. And a gap is provided between the gas diffusion electrode and the ion exchange membrane, and the half-cell with the gas diffusion electrode has an electrolyte feed and an electrolyte discharge as well as a gas inlet and a gas outlet. The electrochemical cell preferably has an electrolyte feed that is hermetically connected to the gap.
摘要翻译：本发明描述了一种电化学电池，其至少包括具有阳极的阳极半电池，具有阴极的阴极半电池和布置在阳极半电池和阴极半电池之间的离子交换膜，阳极和/或阴极是气体扩散电极。并且在气体扩散电极和离子交换膜之间设置有间隙，并且具有气体扩散电极的半电池具有电解质进料和电解液排出以及气体入口和气体出口。电化学电池优选地具有气密地连接到间隙的电解质进料。

48. 发明授权

US07858727B2 Process for the preparation of polycarbonate 有权
标题翻译：制备聚碳酸酯的方法
公开(公告)号：US07858727B2
公开(公告)日：2010-12-28
申请号：US12390794
申请日：2009-02-23
申请人： Pieter Ooms , Andreas Bulan , Rainer Weber , Johann Rechner
发明人： Pieter Ooms , Andreas Bulan , Rainer Weber , Johann Rechner
IPC分类号： C08G64/00 , C08G63/02
CPC分类号： C08G64/24 , C01D3/06 , Y02P20/582
摘要： The invention relates to a combined process for the preparation of polycarbonate by the phase boundary process and downstream electrolysis of sodium chloride-containing process wastewater.
摘要翻译：本发明涉及通过相边界法制备聚碳酸酯的方法和含氯化钠的工艺废水的下游电解。

49. 发明申请

US20080053836A1 PROCESS FOR THE PRODUCTION OF DIARYL CARBONATES AND TREATMENT OF ALKALICHLORIDE SOLUTIONS RESULTING THEREFROM 审中-公开
标题翻译：生产二氧化碳的方法和治疗其结果的碱性溶液
公开(公告)号：US20080053836A1
公开(公告)日：2008-03-06
申请号：US11849542
申请日：2007-09-04
申请人： Andreas Bulan , Pieter Ooms , Rainer Weber , Johann Rechner , Marc Buts , Johan Vanden Eynde
发明人： Andreas Bulan , Pieter Ooms , Rainer Weber , Johann Rechner , Marc Buts , Johan Vanden Eynde
IPC分类号： C25B3/02
CPC分类号： C25B1/34 , C01D3/04 , C01D3/06 , C07C68/02 , C07C69/96
摘要： Processes comprising: (a) reacting phosgene and a monohydroxyl aryl compound in the presence of a suitable catalyst to form a diaryl carbonate and a solution comprising an alkali chloride; (b) separating the diaryl carbonate from the solution; (c) adjusting the pH of the solution to a value of less than or equal to 8 to form a pH-adjusted solution; (d) treating the pH-adjusted solution with an adsorbent to form a treated solution; (e) subjecting at least a portion of the treated solution to electrochemical oxidation to form chlorine and an alkali hydroxide solution; and (f) recycling at least a portion of one or both of the chlorine and the alkali hydroxide solution.
摘要翻译：方法包括：（a）在合适的催化剂存在下使光气和单羟基芳基化合物反应，形成碳酸二芳酯和包含碱金属氯化物的溶液; （b）从溶液中分离碳酸二芳酯; （c）将溶液的pH调节至小于或等于8的值以形成pH调节的溶液; （d）用吸附剂处理pH调节的溶液以形成处理溶液; （e）使经处理的溶液的至少一部分进行电化学氧化以形成氯和碱金属氢氧化物溶液; 和（f）回收氯和氢氧化碱溶液中的一种或两种的至少一部分。

50. 发明授权

US06890418B2 Process for the electrolysis of an aqueous solution of alkali metal chloride 有权
标题翻译：电解碱金属氯化物水溶液的方法
公开(公告)号：US06890418B2
公开(公告)日：2005-05-10
申请号：US10308736
申请日：2002-12-03
申请人： Andreas Bulan , Fritz Gestermann , Hans-Dieter Pinter
发明人： Andreas Bulan , Fritz Gestermann , Hans-Dieter Pinter
IPC分类号： C25B15/02 , C25B1/46 , C25B9/08
CPC分类号： C25B1/46
摘要： The invention describes a process for the electrolysis of an aqueous solution of alkali metal chloride, in particular sodium chloride, by the membrane process with an aqueous solution of alkali metal hydroxide, in particular sodium hydroxide, as catholyte, where the temperature of the alkali metal chloride solution in the anode half-element and/or the volume flow rate of the alkali metal chloride solution in the anode half-element are set in such a way that the difference between the temperature of the alkali metal hydroxide solution at the entry into the cathode half-element and the temperature of the alkali metal hydroxide solution at the exit from the cathode half-element are not greater than 15° C.
摘要翻译：本发明描述了通过膜法将碱金属氯化物水溶液，特别是氯化钠水溶液与碱金属氢氧化物，特别是氢氧化钠的水溶液电解为阴极电解液的方法，其中碱金属阳极半元件中的氯化物溶液和/或阳极半元件中的碱金属氯化物溶液的体积流速设定为使得碱金属氢氧化物溶液在入口处的温度之间的差异阴极半体元件和阴极半元件出口处的碱金属氢氧化物溶液的温度不大于15℃。

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