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41. 发明授权

US4764300A Preparation of finely divided and acicular hexagonal ferrites and their use for the production of magnetic recording media and plastoferrites 失效
标题翻译：精细和针状的六方晶系铁氧体的制备及其用于生产磁记录介质和塑性铁素体的用途
公开(公告)号：US4764300A
公开(公告)日：1988-08-16
申请号：US865121
申请日：1986-05-20
申请人： Hartmut Hibst , Peter Rudolf , Helmut Jakusch
发明人： Hartmut Hibst , Peter Rudolf , Helmut Jakusch
IPC分类号： H01F1/11 , C01G29/00 , C01G49/00 , C01G51/00 , C09D5/23 , G11B5/706 , H01F1/113 , C04B35/26
CPC分类号： H01F1/113 , C01G49/0036 , C01G49/0063 , C01G49/009 , C01G51/006 , G11B5/70678 , C01P2002/54 , C01P2004/10 , C01P2004/54 , C01P2006/12 , C01P2006/42 , C01P2006/60
摘要： A process for the preparation of finely divided and acicular hexagonal ferrites of the general formula AMe.sub.x Fe.sub.12-x O.sub.19, where x is .ltoreq.4, A is barium and/or strontium and Me is indium or equimolar amounts of zinc or cobalt and titanium, and their use for the production of magnetic recording media and plastoferrites.
摘要翻译：制备通式为AMexFe12-xO19的细碎和针状六方晶系铁氧体的方法，其中x为4，A为钡和/或锶，Me为铟或等摩尔量的锌或钴和钛，以及它们用于生产磁记录介质和plastoferrites。

42. 发明授权

US4680130A Preparation of finely divided isotropic ferrite powders having the spinel structure 失效
标题翻译：制备具有尖晶石结构的细碎各向同性铁氧体粉末
公开(公告)号：US4680130A
公开(公告)日：1987-07-14
申请号：US780458
申请日：1985-09-26
申请人： Hartmut Hibst
发明人： Hartmut Hibst
IPC分类号： C01G49/00 , C01G51/00 , C01G53/00 , C04B35/26 , C08K3/24 , C09C1/22 , C09C1/24 , C09D5/23 , G11B5/706 , H01F1/117 , H01F1/36 , H01F1/44
CPC分类号： B82Y30/00 , C01G49/0018 , C01G49/0036 , C01G49/0063 , C01G49/0072 , C01G51/00 , C01G53/00 , C04B35/26 , C08K3/24 , C09C1/22 , C09C1/24 , G11B5/70678 , H01F1/117 , H01F1/445 , C01P2002/32 , C01P2004/62 , C01P2004/64 , C01P2006/12 , C01P2006/42
摘要： A process for the preparation of ferrite powders which have a particle fineness which can be set to a defined value, of the general compositionM(II).sub.x Fe(II).sub.1-x Fe(III).sub.2 O.sub.4andM(II).sub.x Fe(III).sub.3-x O.sub.4.5-0.5xwhere M is Mg, Mn, Co, Ni, Cu and/or Zn and x is from 0 to 1, and have an essentially isotropic particle shape.
摘要翻译：一般组合物M（II）x Fe（II）1-xFe（III）2O 4和M（II）x Fe（III）的制备具有可以设定为规定值的颗粒细度的铁氧体粉末的方法 3-xO4.5-0.5x其中M是Mg，Mn，Co，Ni，Cu和/或Zn，x是0至1，并且具有基本上各向同性的颗粒形状。

43. 发明授权

US09156693B2 Synthesis of lithium-metal-phosphates under hydrothermal conditions 有权
标题翻译：在水热条件下合成锂金属磷酸盐
公开(公告)号：US09156693B2
公开(公告)日：2015-10-13
申请号：US13142606
申请日：2009-12-22
申请人： Kirill Bramnik , Hartmut Hibst , Jordan Keith Lampert , Simon Schroedle
发明人： Kirill Bramnik , Hartmut Hibst , Jordan Keith Lampert , Simon Schroedle
IPC分类号： H01M4/88 , H01B1/06 , H01B1/12 , C01B25/45 , H01M4/58 , H01M4/62 , H01M10/0525
CPC分类号： C01B25/45 , H01M4/5825 , H01M4/625 , H01M10/0525
摘要： The present invention relates to a process for the preparation of compounds of general formula (I) Lia-bM1bQ1-cM2cPd-eM3eOx (l), wherein Q has the oxidation state +2 and M1, M2, M3,a, b, c, d, e and x are: Q: Fe, Mn, Co, Ni, M1: Na, K, Rb and/or Cs, M2: Mg, Al, Ca, Ti, Co, Ni, Cr, V, Fe, Mn, wherein Q and M2 are different from each other,M3: Si, S, F a: 0.8-1.9, b: 0-0.3, c: 0-0.9, d: 0.8-1.9, e: 0-0.5, x: 1.0-8, depending on the amount and oxidation state of Li, M1, M2, P, M3, wherein compounds of general formula (I) are neutrally charged, comprising the following steps (A) providing a mixture comprising at least one lithium-comprising compound, at least one Q-comprising compound, in which Q has at least partially an oxidation state higher than +2, and at least one M1-comprising compound, if present, and/or at least one M2-comprising compound, if present, and/or least one M3-comprising compound, if present, and at least one reducing agent which is oxidized to at least one compound comprising at least one phosphorous atom in oxidation state +5, and (B) heating the mixture obtained in step (A) at a temperature of 100 to 500° C. and at an autogeneous pressure to reduce Q to oxidation state +2 and to obtain a compound of general formula (I).
摘要翻译：本发明涉及制备通式（I）Lia-bM1bQ1-cM2cPd-eM3eOx（1）的化合物的方法，其中Q具有氧化态+2和M1，M2，M3，a，b，c， d，e和x为：Q：Fe，Mn，Co，Ni，M1：Na，K，Rb和/或Cs，M2：Mg，Al，Ca，Ti，Co，Ni，Cr，V，Fe，Mn 其中Q和M2彼此不同，M3：Si，S，F a：0.8-1.9，b：0-0.3，c：0-0.9，d：0.8-1.9，e：0-0.5，x：取决于Li，M1，M2，P，M3的量和氧化态，其中通式（I）的化合物是中性带电的，包括以下步骤（A），提供包含至少一种锂 - 包含化合物，至少一种含Q的化合物，其中Q至少部分具有高于+2的氧化态，以及至少一种含M1化合物（如果存在）和/或至少一种含M2化合物，如果存在和/或至少一种含M3化合物（如果存在）和至少一种被氧化成至少一种化合物com的还原剂至少提供一个氧化态+5的磷原子，（B）在100〜500℃的温度和自发压力下加热步骤（A）中得到的混合物，将Q降低至氧化态+2，得到通式（I）的化合物。

44. 发明授权

US09023523B2 Synthesis of lithium-iron-phosphates under hydrothermal conditions 有权
标题翻译：在水热条件下合成磷酸铁锂
公开(公告)号：US09023523B2
公开(公告)日：2015-05-05
申请号：US13257137
申请日：2010-03-16
申请人： Kirill Bramnik , Hartmut Hibst , Jordan Keith Lampert
发明人： Kirill Bramnik , Hartmut Hibst , Jordan Keith Lampert
IPC分类号： H01M4/58 , C01B25/30 , C01B25/45
CPC分类号： C01B25/45 , H01M4/5825
摘要： The present invention relates to a process for the preparation of compounds of general formula (I) Lia-bMb1Fe1-cMc2Pd-eMe3Ox, wherein Fe has the oxidation state +2 and M1, M2, M3, a, b, c, d, e and x are: M1: Na, K, Rb and/or Cs, M2: Mn, Mg, Al, Ca, Ti, Co, Ni, Cr, V, M3: Si, S, F a: 0.8-1.9, b: 0-0.3, c: 0-0.9, d: 0.8-1.9, e: 0-0.5, x: 1.0-8, depending on the amount and oxidation state of Li, M1, M2, P, M3, wherein compounds of general formula (I) are neutrally charged, comprising the following steps (A) providing a mixture comprising at least one lithium-comprising compound, at least one iron-comprising compound, in which iron has the oxidation state 0, and at least one M1-comprising compound, if present, and/or at least one M2-comprising compound, if present, and/or least one M3-comprising compound, if present, and at least one compound comprising at least one phosphorous atom in oxidation state +5, and (B) heating the mixture obtained in step (A) at a temperature of 100 to 500° C. and at an autogeneous pressure to obtain a compound of general formula (I).
摘要翻译：本发明涉及制备通式（I）Lia-bMb1Fe1-cMc2Pd-eMe3Ox的化合物的方法，其中Fe具有氧化态+2和M1，M2，M3，a，b，c，d，e 和x为：M1：Na，K，Rb和/或Cs，M2：Mn，Mg，Al，Ca，Ti，Co，Ni，Cr，V，M3：Si，S，F a：0.8-1.9，b ：0-0.3，c：0-0.9，d：0.8-1.9，e：0-0.5，x：1.0-8，这取决于Li，M1，M2，P，M3的量和氧化态，其中化合物通式（I）是中性带电的，包括以下步骤（A），提供包含至少一种含锂化合物，至少一种含铁化合物的混合物，其中铁具有氧化态0，和至少一种M1 和/或至少一种含M2的化合物（如果存在）和/或至少一种含M3的化合物（如果存在）和至少一种包含至少一个氧化态的磷原子的化合物+5 ，（B）在100〜500℃的温度下加热步骤（A）中得到的混合物。和自动压力下，得到通式（I）的化合物。

45. 发明授权

US08673497B2 Process for the preparation of crystalline lithium-, iron- and phosphate-comprising materials 有权
标题翻译：制备结晶的含锂，铁和磷酸盐的材料的方法
公开(公告)号：US08673497B2
公开(公告)日：2014-03-18
申请号：US12988222
申请日：2009-04-16
申请人： Hartmut Hibst , Brian Roberts , Jordan Keith Lampert , Kirill Bramnik
发明人： Hartmut Hibst , Brian Roberts , Jordan Keith Lampert , Kirill Bramnik
IPC分类号： H01M4/58 , C01B25/30
CPC分类号： C01B25/45 , H01M4/136 , H01M4/5825 , H01M10/052
摘要： The present invention relates to a Process for the preparation of compounds of general formula (I), Lia-bM1bFe1-cM2cPd-eM3eOx, wherein M1, M2, M3, a, b, c, d and e: M1: Na, K, Rb and/or Cs, M2: Mn, Mg, Ca, Ti, Co, Ni, Cr, V, M3: Si, S, a: 0.8-1.9, b: 0-0.3, c: 0-0.9, d: 0.8-1.9, e: 0-0.5, x: 1.0-8, depending on the amount and oxidation state of Li, M1, Fe, M2, P, M3, wherein compounds of general formula (I) are neutrally charged, comprising the following steps (A) providing a mixture comprising at least one lithium-comprising compound, at least one iron-comprising compound, in which iron has the oxidation state +3, and at least one M1-comprising compound, if present, and/or at least one M2-comprising compound, if present, and/or least one M3-comprising compound, if present, and at least one reducing agent which is oxidized to at least one compound comprising at least one phosphorous atom in oxidation state +5, (B) optionally drying the mixture provided in step (A), in order to obtain a solid compound and (C) calcining the solid compound obtained from step (A) or (B) at a temperature of 300 to 1000° C.
摘要翻译：本发明涉及制备通式（I）化合物Lia-bM1bFe1-cM2cPd-eM3eOx的方法，其中M1，M2，M3，a，b，c，d和e：M1：Na，K， Rb和/或Cs，M2：Mn，Mg，Ca，Ti，Co，Ni，Cr，V，M3：Si，S，a：0.8-1.9，b：0-0.3，c：0-0.9，d： 0.8-1.9，e：0-0.5，x：1.0-8，这取决于Li，M1，Fe，M2，P，M3的量和氧化态，其中通式（I）的化合物是中性带电的，提供包含至少一种含锂化合物的混合物的步骤（A），至少一种含铁化合物，其中铁具有+3的氧化态和至少一种含M1化合物（如果存在）和/或至少一种含M2的化合物（如果存在）和/或至少一种含M3化合物（如果存在）和至少一种还原剂被氧化成至少一种包含至少一个氧化态的磷原子+5的化合物，（B）任选地干燥步骤（A）中提供的混合物，以获得a 固体化合物和（C）在300〜1000℃的温度下煅烧由步骤（A）或（B）得到的固体化合物。

46. 发明申请

US20110315938A1 PROCESS FOR PREPARING LITHIUM MIXED METAL OXIDES AND THEIR USE AS CATHODE MATERIAL 有权
标题翻译：制备锂复合金属氧化物的方法及其作为阴极材料的使用
公开(公告)号：US20110315938A1
公开(公告)日：2011-12-29
申请号：US13167079
申请日：2011-06-23
申请人： Simon SCHROEDLE , Hartmut Hibst , Jordan Keith Lampert , Mark Schweter , Ivan Petrovic
发明人： Simon SCHROEDLE , Hartmut Hibst , Jordan Keith Lampert , Mark Schweter , Ivan Petrovic
IPC分类号： H01B1/02
CPC分类号： H01B1/08 , C01G53/50 , C01P2002/50 , C01P2004/51 , C01P2006/10 , C01P2006/11 , C01P2006/40 , H01M4/505 , H01M4/525 , Y02E60/122
摘要： Process for preparing lithium mixed metal oxides which comprise essentially lithium, manganese, cobalt and nickel as metal atoms and have a stoichiometric ratio of lithium to the total transition metals of greater than 1, which comprises a) the preparation of a mixture designated as intermediate (B) which comprises essentially lithium-comprising mixed metal hydroxides and lithium-comprising mixed metal oxide hydroxides, where manganese, cobalt and nickel are comprised in the ratio (1−a−b):a:b and the oxidation state averaged over all ions of manganese, cobalt and nickel is at least 4-1.75a-1.75b, where 0≦a≦0.5 and 0.1≦b≦0.8, by a thermal treatment carried out with continual mixing and in the presence of oxygen of a mixture (A) comprising at least one transition metal compound and at least one lithium salt (L), during which L does not melt, and b) the thermal treatment carried out without mixing and in the presence of oxygen of the intermediate (B).
摘要翻译：制备锂复合金属氧化物的方法，其基本上包含锂，锰，钴和镍作为金属原子并且具有大于1的总过渡金属的化学计量比的锂，其包括a）制备称为中间体 B），其基本上由含锂的混合金属氢氧化物和含锂的混合金属氧化物氢氧化物组成，其中锰，钴和镍以（1-a-b）：a:b的比率包含，并且所有离子的平均氧化态的锰，钴和镍的含量至少为4-1.75a-1.75b，其中0＆nlE; a＆nlE; 0.5和0.1＆nlE; b＆nlE; 0.8，通过连续混合和在混合物的氧气存在下进行的热处理 A）包含至少一种过渡金属化合物和至少一种锂盐（L），在此期间L不熔化，以及b）在不混合的情况下和在中间体（B）的氧气存在下进行热处理。

47. 发明申请

US20110284806A1 ELECTRODE MATERIAL AND USE THEREOF FOR PRODUCTION OF ELECTROCHEMICAL CELLS 失效
标题翻译：电极材料及其生产电化学电池的用途
公开(公告)号：US20110284806A1
公开(公告)日：2011-11-24
申请号：US13111263
申请日：2011-05-19
申请人： Martin SCHULZ-DOBRICK , Hartmut Hibst , Jordan Keith Lampert , Robert Glaum , Helmut Ehrenberg , Katharina Gerber , Markus Herklotz , Frieder Scheiba
发明人： Martin SCHULZ-DOBRICK , Hartmut Hibst , Jordan Keith Lampert , Robert Glaum , Helmut Ehrenberg , Katharina Gerber , Markus Herklotz , Frieder Scheiba
IPC分类号： H01B1/18 , H01M4/525 , H01M4/485 , H01M4/505
CPC分类号： H01B1/24 , C01B25/45 , H01M4/0404 , H01M4/136 , H01M4/505 , H01M4/525 , H01M4/5825 , H01M10/0525 , H01M10/0568 , H01M10/0569
摘要： A compound of the general formula (I) AaMbPcOd (I) in which the variables are each defined as follows: M is at least one transition metal selected from Co, Ni, Mn, Fe and Cr, A is Li or LixNa1-x where x is in the range from 0.2 to 1.0, a is in the range from 3.5 to 4.5, b is in the range from 0.8 to 1.2, c is in the range from 1.8 to 2.2 and d is in the range from 7.2 to 8.8.
摘要翻译：通式（I）AaMbPcOd（I）的化合物，其变量各自定义如下：M是选自Co，Ni，Mn，Fe和Cr中的至少一种过渡金属，A是Li或Li x Na 1-x，其中 x在0.2至1.0的范围内，a在3.5至4.5的范围内，b在0.8至1.2的范围内，c在1.8至2.2的范围内，d在7.2至8.8的范围内。

48. 发明申请

US20110130273A1 MODIFIED ZINC OXIDE PARTICLES 有权
标题翻译：改性氧化锌颗粒
公开(公告)号：US20110130273A1
公开(公告)日：2011-06-02
申请号：US13054636
申请日：2009-07-14
申请人： Andrey Karpov , Hartmut Hibst , Simon Schambony , Richard Riggs , Sylke Haremza
发明人： Andrey Karpov , Hartmut Hibst , Simon Schambony , Richard Riggs , Sylke Haremza
IPC分类号： C07F3/06 , B01J23/06 , C09K15/32
CPC分类号： C09C1/043 , C01G9/02 , C01P2002/84
摘要： Process for the preparation of modified ZnO particles in which a zinc salt and a base are mixed in a polar solvent and, if appropriate after the precipitation of a precipitation product, the polar solvent is removed and a residue is obtained, where the residue is taken up in a nonpolar solvent, surface-active substances are added, optionally further effect substances are added and then the modified ZnO particles are separated off from further by-products. Materials such as plastics, coatings or paints comprising modified ZnO particles. Methods for the incorporation of modified ZnO particles into materials, where the modified ZnO particles are incorporated into the materials in the form of dispersions or suspensions. Use of modified ZnO particles for protecting material against the effect of light, heat, oxygen or free radicals, as catalysts, for semiconductive films or cosmetic applications.
摘要翻译：制备其中将锌盐和碱在极性溶剂中混合的改性ZnO颗粒的制备方法，并且如果适当，在析出产物沉淀后，除去极性溶剂，得到残留物，其中残留物被在非极性溶剂中加入表面活性物质，任选地添加另外的效果物质，然后将改性的ZnO颗粒与进一步的副产物分离。诸如塑料，涂料或包含改性ZnO颗粒的涂料的材料。将改性的ZnO颗粒引入到材料中的方法，其中将改性的ZnO颗粒以分散体或悬浮液的形式引入材料中。使用改性ZnO颗粒来保护材料免受光，热，氧或自由基作为半导体膜或化妆品应用的催化剂的影响。

49. 发明申请

US20110037032A1 PROCESS FOR THE PREPARATION OF CRYSTALLINE LITHIUM-, IRON- AND PHOSPHATE-COMPRISING MATERIALS 有权
标题翻译：制备结晶锂，铁和磷酸盐包覆材料的方法
公开(公告)号：US20110037032A1
公开(公告)日：2011-02-17
申请号：US12988222
申请日：2009-04-16
申请人： Hartmut Hibst , Brian Roberts , Jordan Keith Lampert , Kirill Bramnik
发明人： Hartmut Hibst , Brian Roberts , Jordan Keith Lampert , Kirill Bramnik
IPC分类号： H01M4/88 , B29B9/00 , H01M4/58 , B82Y99/00
CPC分类号： C01B25/45 , H01M4/136 , H01M4/5825 , H01M10/052
摘要： The present invention relates to a Process for the preparation of compounds of general formula (I), Lia-bM1bFe1-cM2cPd-eM3eOx, wherein M1, M2, M3, a, b, c, d and e: M1: Na, K, Rb and/or Cs, M2: Mn, Mg, Ca, Ti, Co, Ni, Cr, V, M3: Si, S, a: 0.8-1.9, b: 0-0.3, c: 0-0.9, d: 0.8-1.9, e: 0-0.5, x: 1.0-8, depending on the amount and oxidation state of Li, M1, Fe, M2, P, M3, wherein compounds of general formula (I) are neutrally charged, comprising the following steps (A) providing a mixture comprising at least one lithium-comprising compound, at least one iron-comprising compound, in which iron has the oxidation state +3, and at least one M1-comprising compound, if present, and/or at least one M2-comprising compound, if present, and/or least one M3-comprising compound, if present, and at least one reducing agent which is oxidized to at least one compound comprising at least one phosphorous atom in oxidation state +5, (B) optionally drying the mixture provided in step (A), in order to obtain a solid compound and (C) calcining the solid compound obtained from step (A) or (B) at a temperature of 300 to 1000° C.
摘要翻译：本发明涉及制备通式（I）化合物Lia-bM1bFe1-cM2cPd-eM3eOx的方法，其中M1，M2，M3，a，b，c，d和e：M1：Na，K， Rb和/或Cs，M2：Mn，Mg，Ca，Ti，Co，Ni，Cr，V，M3：Si，S，a：0.8-1.9，b：0-0.3，c：0-0.9，d： 0.8-1.9，e：0-0.5，x：1.0-8，这取决于Li，M1，Fe，M2，P，M3的量和氧化态，其中通式（I）的化合物是中性带电的，提供包含至少一种含锂化合物的混合物的步骤（A），至少一种含铁化合物，其中铁具有+3的氧化态和至少一种含M1化合物（如果存在）和/或至少一种含M2的化合物（如果存在）和/或至少一种含M3化合物（如果存在）和至少一种还原剂被氧化成至少一种包含至少一个氧化态的磷原子+5的化合物，（B）任选地干燥步骤（A）中提供的混合物，以获得a 固体化合物和（C）在300〜1000℃的温度下煅烧由步骤（A）或（B）得到的固体化合物。

50. 发明申请

US20100204488A1 SILVER- AND VANADIUM-CONTAINING MULTIMETAL OXIDE AND ITS USE 有权
标题翻译：含钒和含钒的多种氧化物及其用途
公开(公告)号：US20100204488A1
公开(公告)日：2010-08-12
申请号：US12701600
申请日：2010-02-07
申请人： Thomas Heidemann , Hartmut Hibst , Stefan Bauer , Ulf Dietrich
发明人： Thomas Heidemann , Hartmut Hibst , Stefan Bauer , Ulf Dietrich
IPC分类号： C07D307/89 , C07C51/567 , C07C51/265
CPC分类号： B01J23/682 , B01J23/683 , C01G31/00 , C01G31/006 , C01G39/006 , C01P2002/50 , C01P2002/54 , C01P2002/72 , C01P2002/74 , C01P2002/77 , C01P2004/10 , C01P2004/54 , C01P2004/61 , C01P2004/80 , C01P2006/12 , C01P2006/60 , C01P2006/80 , C01P2006/82 , C07C51/265 , C07C51/313 , C07C63/16
摘要： A multimetal oxide of the formula I Aga-bMbV2Ox*cH2O, I where M is a metal selected from the group consisting of Li, Na, K, Rb, Cs, Tl, Mg, Ca, Sr, Ba, Cu, Zn, Cd, Pb, Cr, Au, Al, Fe, Co, Ni and/or Mo, a is from 0.3 to 1.9 and b is from 0 to 0.5, with the proviso that the difference (a-b) and c is from 0 to 20 and x is a number determined by the valence and amount of elements different from oxygen in the formula I, which has a crystal structure giving an X-ray powder diffraction pattern which displays reflections at the lattice spacings d of 15.23±0.6, 12.16±0.4, 10.68±0.3, 3.41±0.04, 3.09±0.04, 3.02±0.04, 2.36±0.04 and 1.80±0.04 Å. Precatalysts and catalysts produced therefrom for the partial oxidation of aromatic hydrocarbons are also provided.
摘要翻译：式I Aga-bMbV2Ox * cH2O，I的多金属氧化物，其中M是选自Li，Na，K，Rb，Cs，Tl，Mg，Ca，Sr，Ba，Cu，Zn，Cd ，Pb，Cr，Au，Al，Fe，Co，Ni和/或Mo，a为0.3〜1.9，b为0〜0.5，条件是差（ab）和c为0〜20， x是由式I中与氧不同的元素的化合价和数量决定的数字，其具有给出X晶粉末衍射图的晶体结构，其显示晶格间距d为15.23±0.6,12.16±0.4的反射， 10.68±0.3,3.41±0.04,3.09±0.04,3.02±0.04,2.36±0.04和1.80±0.04。还提供了预催化剂和由其制备的用于芳族烃的部分氧化的催化剂。

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