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41. 发明授权

US08795784B2 Aqueous emulsions of functional alkoxysilanes and condensed oligomers thereof, their preparation and use for surface treatment 有权
标题翻译：功能性烷氧基硅烷及其缩合低聚物的水乳液，其制备和用于表面处理
公开(公告)号：US08795784B2
公开(公告)日：2014-08-05
申请号：US11815391
申请日：2005-12-08
申请人： Burkhard Standke , Kerstin Weissenbach , Bernd Bartkowiak
发明人： Burkhard Standke , Kerstin Weissenbach , Bernd Bartkowiak
IPC分类号： C09D5/16 , B01J31/02 , C08L5/00 , C09K3/00 , B05D3/00 , C04B41/49 , C08J3/03 , C04B41/00 , C04B111/00
CPC分类号： C08J3/03 , C04B41/009 , C04B41/4961 , C04B2111/00112 , C08J2383/04 , C04B41/4922 , C04B41/502 , C04B2103/40 , C04B28/02
摘要： Aqueous oil-in-water emulsion comprising from 1 to 70% by weight, based on the total weight of the emulsion, of functional alkoxysilanes and/or condensed oligomers thereof and/or organoalkoxysiloxanes, at least one emulsifier and water, wherein the emulsion has a pH of from 5 to 9 and preferably a mean droplet size of the disperse phase of ≦0.5 μm, and the width of the droplet size distribution, expressed as the span (Formula I), is from 0.6 to 1.2. The preparation of the emulsions having the desired droplet size distribution is carried out in apparatuses having at least one pressure stage at a pressure of from 2 to 15 MPa. The emulsion can be used for hydrophobicizing porous mineral building materials.
摘要翻译：水包油包水乳液包含1至70重量％，基于乳液的总重量，官能的烷氧基硅烷和/或其缩合的低聚物和/或有机烷氧基硅氧烷，至少一种乳化剂和水，其中乳液具有 pH为5至9，优选分散相的平均液滴尺寸为＆lt; lE;0.5μm，液滴尺寸分布的宽度以跨度（式I）表示为0.6至1.2。具有所需液滴尺寸分布的乳液的制备在具有2至15MPa压力的至少一个压力级的装置中进行。该乳液可用于疏水化多孔矿物建筑材料。

42. 发明授权

US08481654B2 Aqueous silane nanocomposites 有权
标题翻译：水性硅烷纳米复合材料
公开(公告)号：US08481654B2
公开(公告)日：2013-07-09
申请号：US11572691
申请日：2004-11-08
申请人： Roland Edelmann , Bjoern Borup , Jaroslaw Monkiewicz , Christian Wassmer , Kerstin Bibbo , Burkhard Standke
发明人： Roland Edelmann , Bjoern Borup , Jaroslaw Monkiewicz , Christian Wassmer , Kerstin Bibbo , Burkhard Standke
IPC分类号： C08G77/38 , C08G77/382 , C08L83/06
CPC分类号： C08G77/58 , B22C1/183 , C01P2004/62 , C01P2004/64 , C09C1/3054 , C09C1/3081 , C09C1/309 , C09D183/14 , Y10T428/31663
摘要： The present invention provides a composition based on the reaction at least of the following components: (i) a glycidyloxypropylalkoxysilane, (ii) an aqueous silica sol having an SiO2 content of >20% by weight, (iii) an organic acid hydrolysis catalyst, and (iv) n-propyl zirconate, butyl titanate or titanium acetylacetonate as crosslinker, a process for its preparation, and the use thereof, particularly as a composition for scratch resistant coatings, and also provides articles thus coated.
摘要翻译：本发明提供了至少以下组分的基于该反应的组合物：（i）缩水甘油氧基丙基烷氧基硅烷，（ii）SiO 2含量> 20重量％的水性硅溶胶，（iii）有机酸水解催化剂，和（iv）锆酸正丙酯，钛酸丁酯或乙酰丙酮钛作为交联剂，其制备方法及其用途，特别是作为耐划伤涂料的组合物，并且还提供如此涂覆的制品。

43. 发明申请

US20130040078A1 METHODS FOR PRODUCING A DISPERSION CONTAINING SILICON DIOXIDE PARTICLES AND CATIONIZATION AGENT 有权
标题翻译：生产含二氧化硅颗粒和起泡剂的分散体的方法
公开(公告)号：US20130040078A1
公开(公告)日：2013-02-14
申请号：US13642862
申请日：2011-05-23
申请人： Stefan Scharfe , Andrea Heuschen , Christoph Batz-Sohn , Burkhard Standke , Christian Wassmer , Heinz Lach
发明人： Stefan Scharfe , Andrea Heuschen , Christoph Batz-Sohn , Burkhard Standke , Christian Wassmer , Heinz Lach
IPC分类号： C09D5/00 , B41M5/50 , C09D129/04
CPC分类号： B41M5/5218 , B41M5/426 , C01B33/141 , D21H19/40
摘要： Process for preparing a dispersion comprising silicon dioxide particles and cationizing agents, by dispersing 50 to 75 parts by weight of water, 25 to 50 parts by weight of silicon dioxide particles having a BET surface area of 30 to 500 m2/g and 100 to 300 μg of cationizing agent per square metre of the BET surface area of the silicon dioxide particles, wherein the cationizing agent is obtainable by reacting at least one haloalkyl-functional alkoxysilane, its hydrolysis products or condensation products and/or a mixture thereof with at least one aminoalcohol and a defined amount of water and optionally removing the resulting hydrolysis alcohol at least partly from the reaction mixture.Process for preparing a dispersion comprising silicon dioxide particles and cationizing agents, by dispersing 50 to 75 parts by weight of water, 25 to 50 parts by weight of silicon dioxide particles having a BET surface area of 30 to 500 m2/g and 100 to 300 μg of a cationizing agent per square metre of the BET surface area of the silicon dioxide particles, wherein the cationizing agent comprises one or more quaternary, aminoalcohol-functional, organosilicon compounds of the general formula III and/or condensation products thereof, wherein Ru and Rv are each independently of each other an alkyl group having 2 to 4 carbon atoms, m is 2 to 5 and n is 2 to 5.
摘要翻译：制备包含二氧化硅颗粒和阳离子化剂的分散体的方法，通过分散50至75重量份的水，25至50重量份的BET表面积为30至500m 2 / g的二氧化硅颗粒和100至300 微米的阳离子化剂每平方米的二氧化硅颗粒的BET表面积，其中阳离子化剂可通过使至少一种卤代烷基官能的烷氧基硅烷，其水解产物或缩合产物和/或其混合物与至少一种氨基醇和限定量的水，并任选地从反应混合物中部分地除去所得的水解醇。制备包含二氧化硅颗粒和阳离子化剂的分散体的方法，通过分散50至75重量份的水，25至50重量份的BET表面积为30至500m 2 / g的二氧化硅颗粒和100至300 微米的阳离子化剂每平方米的二氧化硅颗粒的BET表面积，其中阳离子化剂包含一种或多种通式III的季铵，氨基醇官能的有机硅化合物和/或其缩合产物，其中Ru和 Rv各自独立地为具有2至4个碳原子的烷基，m为2至5，n为2至5。

44. 发明授权

US08298679B2 Aqueous silane systems based on bis(trialkoxysilylalkyl)amines 有权
标题翻译：基于双（三烷氧基甲硅烷基烷基）胺的水性硅烷体系
公开(公告)号：US08298679B2
公开(公告)日：2012-10-30
申请号：US12674271
申请日：2008-07-02
申请人： Philipp Albert , Eckhard Just , Christian Wassmer , Burkhard Standke
发明人： Philipp Albert , Eckhard Just , Christian Wassmer , Burkhard Standke
IPC分类号： B32B9/04
CPC分类号： C04B41/64 , C03C17/30 , C04B41/009 , C04B41/4961 , C08L83/08 , C09D4/00 , C09D183/08 , C23C2222/20 , Y10T428/1317 , Y10T428/31663 , Y10T428/31667 , C04B28/02 , C08L2666/34 , C08G77/26 , C08G77/00
摘要： The invention relates to an aqueous composition of bis-amino-functional silicon compounds which is essentially free of organic solvents and releases essentially no further alcohol in the course of crosslinking, and to processes for preparing it and to the use thereof, for example for hydrophobization of metal or glass surfaces.
摘要翻译：本发明涉及双官能硅化合物的水性组合物，其基本上不含有机溶剂，并且在交联过程中基本上不释放其它醇，以及其制备方法及其用途，例如疏水化的金属或玻璃表面。

45. 发明授权

US08147918B2 Water-dilutable sol-gel composition 有权
标题翻译：水可稀释溶胶 - 凝胶组合物
公开(公告)号：US08147918B2
公开(公告)日：2012-04-03
申请号：US12159785
申请日：2006-12-06
申请人： Burkhard Standke , Christian Wassmer , Peter Jenkner
发明人： Burkhard Standke , Christian Wassmer , Peter Jenkner
IPC分类号： B05D1/00 , B05D3/00
CPC分类号： C09D4/00 , C09D5/08 , C09D183/14 , C23C2222/20 , Y10T428/31663 , C08G77/04
摘要： The present invention provides a sol-gel composition which is dilutable with water in any proportion and is based on the reaction of at least the following components: (i) a glycidyloxypropylalkoxysilane, (ii) an aqueous silica sol having a solids content of >1% by weight, (iii) an organic acid as hydrolysis catalyst, and (iv) n-propyl zirconate, butyl titanate or titanium acetylacetonate as crosslinker, starting from a mass ratio of the solids mass of component (ii) to component (i) 0.75, a process for preparing it and its use, in particular as a sol-gel composition for corrosion control coatings, a corresponding corrosion control coat or primer coat, and articles equipped with such a coating.
摘要翻译：本发明提供一种溶胶 - 凝胶组合物，其可以以任何比例用水稀释，并且基于至少以下组分的反应：（i）缩水甘油氧基丙基烷氧基硅烷，（ii）固体含量> 1的水性硅溶胶（iii）作为水解催化剂的有机酸，和（iv）锆酸正丙酯，钛酸丁酯或乙酰丙酮钛作为交联剂，从组分（ii）与组分（i）的固体质量的质量比开始， 0.75，其制备方法及其用途，特别是作为腐蚀控制涂料的溶胶 - 凝胶组合物，相应的腐蚀控制涂层或底漆涂层以及配备有这种涂层的制品。

46. 发明申请

US20120037040A1 COMPOSITION CONTAINING QUATERNARY AMINO-FUNCTIONAL ORGANOSILICON COMPOUNDS AND PRODUCTION AND USE THEREOF 有权
标题翻译：含有四元氨基官能有机硅化合物的组合物及其生产和使用
公开(公告)号：US20120037040A1
公开(公告)日：2012-02-16
申请号：US13257488
申请日：2010-03-19
申请人： Burkhard Standke , Christian Wassmer , Tim Voegtlin , Irene Lippert , Stefan Scharfe , Heinz Lach , Christoph Batz-Sohn , Steffen Hasenzahl
发明人： Burkhard Standke , Christian Wassmer , Tim Voegtlin , Irene Lippert , Stefan Scharfe , Heinz Lach , Christoph Batz-Sohn , Steffen Hasenzahl
IPC分类号： C09D7/12
CPC分类号： C09C1/3081 , C01P2006/11 , C07F7/1892
摘要： The invention relates to a composition and to a method for the production thereof, comprising quaternary amino-functional organosilicon compounds, in particular in the form of oligomers and polymers, which can be present ranging from partially hydrolyzed form to completely hydrolyzed form, and which are in particular soluble in water, have a low VOC content, and to the use thereof.
摘要翻译：本发明涉及一种组合物及其制备方法，其包括季铵氨基官能的有机硅化合物，特别是低聚物和聚合物的形式，其可以从部分水解形式到完全水解形式存在，并且其是特别是可溶于水，具有低VOC含量及其用途。

47. 发明申请

US20080188617A1 High-Viscosity Aqueous Emulsions Of Functional Alkoxysilanes, Condensed Oligomers Thereof, Organopolysiloxanes, Their Preparation And Use For Surface Treatment Of Inorganic Materials 有权
公开(公告)号：US20080188617A1
公开(公告)日：2008-08-07
申请号：US11814127
申请日：2005-12-08
申请人： Burkhard Standke , Kerstin Weissenbach , Bernd Bartkowiak
发明人： Burkhard Standke , Kerstin Weissenbach , Bernd Bartkowiak
IPC分类号： C04B41/49 , C08J3/03 , C09D183/04
CPC分类号： C08J3/03 , C04B41/009 , C04B41/4961 , C08J2383/04 , Y10T428/249953 , Y10T428/249954 , Y10T428/249955 , Y10T428/249956 , C04B41/4922 , C04B41/502 , C04B2103/40 , C04B33/00 , C04B14/043 , C04B28/02
摘要： High-viscosity aqueous emulsions of functional alkoxysilanes, condensed oligomers thereof, organopolysiloxanes, their preparation and use for the surface treatment of inorganic materials High-viscosity aqueous oil-in-water emulsion which comprises from 50 to 90% by weight, based on the total weight of the emulsion, of functional alkoxysilanes and/or condensed oligomers thereof and/or organoalkoxysiloxanes, at least one emulsifier and water and has a pH of from 5 to 9 and a mean droplet size of the disperse phase of less than 5 μm, wherein the width of the droplet size distribution, expressed as the span (see formula (I)), is >1.5, preferably from 3 to 8. The preparation of the emulsions having the desired droplet size distribution is carried out in apparatuses having at least one pressure stage at a pressure of from 2 to 15 MPa. The emulsion can be used for hydrophobicizing porous mineral building materials. D   90 - D   10 D   50 ( I )

48. 发明授权

US06727375B2 Apparatus and process for preparing substantially halogen-free trialkoxysilanes 有权
标题翻译：用于制备基本上无卤素的三烷氧基硅烷的装置和方法
公开(公告)号：US06727375B2
公开(公告)日：2004-04-27
申请号：US10108474
申请日：2002-03-29
申请人： Frank Steding , Gerda Grund , Burkhard Standke , Frank Kropfgans , Michael Horn , Albert-Johannes Frings , Jaroslaw Monkiewicz , Hans-Günther Srebny , Claus-Dietrich Seiler , Hans-Joachim Kötzsch
发明人： Frank Steding , Gerda Grund , Burkhard Standke , Frank Kropfgans , Michael Horn , Albert-Johannes Frings , Jaroslaw Monkiewicz , Hans-Günther Srebny , Claus-Dietrich Seiler , Hans-Joachim Kötzsch
IPC分类号： C07F704
CPC分类号： C07F7/025
摘要： An apparatus for continuously preparing substantially halogen-free, in particular chlorine-free, trialkoxysilanes of the general formula I (RO)3SiH (I) in which R is an alkyl group having from 1 to 6 carbon atoms, has a main reactor unit (1), at least one metering unit (2, 3, 4) for liquids and/or suspensions, located upstream of the main reactor, and at least one metering unit (5) for gaseous and/or vaporous substances, and also a product workup unit (6) located downstream of the main reactor. A process for preparing substantially halogen-free trialkoxysilanes of the general formula I in which silicon is reacted with alcohols in an inert solvent utilizes at least one organocopper compound catalyst.
摘要翻译：用于连续制备具有1-6个碳原子的烷基的通式Iin基本上无卤素，特别是无氯的三烷氧基硅烷的设备具有主反应器单元（1），至少一个计量单元（2,3,4），用于位于主反应器上游的液体和/或悬浮液，以及用于气体和/或气态物质的至少一个计量单元（5），以及位于主反应器下游的产品后处理单元（6）主反应堆。制备基本上无卤素的通式I的三烷氧基硅烷的方法，其中硅与醇在惰性溶剂中反应，使用至少一种有机铜化合物催化剂。

49. 发明授权

US06685766B2 Corrosion inhibitor for steel-reinforced concrete 有权
标题翻译：钢筋混凝土防腐剂
公开(公告)号：US06685766B2
公开(公告)日：2004-02-03
申请号：US10287511
申请日：2002-11-05
申请人： Burkhard Standke , Edward McGettigan
发明人： Burkhard Standke , Edward McGettigan
IPC分类号： C07F702
CPC分类号： C04B41/009 , C04B24/42 , C04B41/4922 , C04B41/4961 , C04B41/64 , C04B2111/26 , C23C2222/20 , C23F11/10 , C04B2103/61 , C04B41/46 , C04B41/463 , C04B41/4944 , C04B28/02
摘要： An organosilane- and/or organosiloxane-containing composition reduces active corrosion of steel reinforcement in concrete.
摘要翻译：含有机硅烷和/或有机硅氧烷的组合物减少混凝土中钢筋的活性腐蚀。

50. 发明授权

US06528585B1 Cross-linkable polymers, method for the production thereof, and shaped bodies made of cross-linked polymers 失效
标题翻译：可交联聚合物，其制备方法和由交联聚合物制成的成型体
公开(公告)号：US06528585B1
公开(公告)日：2003-03-04
申请号：US09830157
申请日：2001-07-19
申请人： Burkhard Standke , Jaroslaw Monkiewicz , Albert-Johannes Frings , Ralf Laven , Roland Edelmann , Peter Jenkner , Helmut Mack , Michael Horn
发明人： Burkhard Standke , Jaroslaw Monkiewicz , Albert-Johannes Frings , Ralf Laven , Roland Edelmann , Peter Jenkner , Helmut Mack , Michael Horn
IPC分类号： C08F800
CPC分类号： C08F255/02 , C08F291/00
摘要： The invention relates to a process for preparing crosslinkable polymers containing silane groups having at least one hydrolyzable radical by free-radical-initiated grafting of the base polymers with an olefinically unsaturated silane having at least one hydrolyzable radical, wherein the grafting is carried out in the presence of (a) an alkylsilane of the formula I, R1(SiR2nX3−n)m, (I) where R1 is a monovalent hydrocarbon radical having from 1 to 33 carbon atoms or a divalent hydrocarbon radical having from 4 to 24 carbon atoms, R2 is a hydrocarbon radical having from 1 to 10 carbon atoms, X are identical or different hydrolyzable radicals, n is 0, 1 or 2 and m is 1 or 2 and/or (b) a fluoroalkylsilane of the formula R3xSiR4yXz, (II) where R3 is a fluoroalkyl radical, R4 is an alkyl radical and X is a hydrolyzable radical, x is an integer from 1 to 3, y is 0, 1 or 2 and z is an integer from 1 to 3, with the proviso that the sum x+y+z=4.
摘要翻译：本发明涉及制备具有至少一个可水解基团的可交联聚合物的交联聚合物的方法，所述硅烷基团具有至少一个可水解基团的烯属不饱和硅烷通过自由基引发接枝基础聚合物，其中接枝在存在（a）式I的烷基硅烷，其中R 1是具有1至33个碳原子的一价烃基或具有4至24个碳原子的二价烃基，R 2是具有1至10个碳原子的烃基 X为相同或不同的可水解基团，n为0,1或2，m为1或2，和/或（b）下式的氟代烷基硅烷，其中R 3为氟代烷基，R 4为烷基，X为可水解基团，x为是1至3的整数，y是0,1或2，z是1至3的整数，条件是和x + y + z = 4。

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