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    • 41. 发明申请
    • METHOD FOR REACTIVELY CRUSHING JATROPHA SEEDS
    • 用于反复破碎JATROPHA种子的方法
    • US20130052328A1
    • 2013-02-28
    • US13575415
    • 2011-01-26
    • Jean-Luc DuboisJulien MagneAntoine Piccirilli
    • Jean-Luc DuboisJulien MagneAntoine Piccirilli
    • C11B1/10A23K1/14
    • C11C3/003A23K10/37C11B1/10Y02E50/13Y02P60/877
    • The present invention relates to a method for reactively crushing jatropha seeds, said method making it possible, starting with specifically conditioned jatropha seeds in the presence of light alcohol and a basic catalyst, to carry out, in a single step, the crushing as well as the reaction for transesterifying the triglycerides present in the jatropha oil, thus causing an oil cake, glycerol, and fatty acid esters to be simultaneously produced. The method for processing the jatropha seeds, according to the invention, makes it possible to inactivate, in a simple, low-cost manner, the phorbol esters in addition to the curcine, thus enabling humans to handle the seeds without risk and moreover use the castor oil cake in animal feed. Characteristically, the seeds are conditioned by a series of operations that include a step of pressing the seeds and a step of drying same.
    • 本发明涉及一种用于对麻风树种子进行反应性破碎的方法,所述方法使得可以在轻质醇和碱性催化剂存在下,用专门条件的麻风树种子开始,在单一步骤中进行破碎,以及 用于酯交换麻风树油中存在的甘油三酯的反应,从而同时产生油饼,甘油和脂肪酸酯。 根据本发明的用于加工麻疯树种子的方法使得可以以简单的低成本方式灭活除了姜渣之外的佛波酯,从而使人类能够无风险地处理种子,并且还使用 蓖麻油饼在动物饲料。 特征地,通过包括挤压种子的步骤和干燥步骤的一系列操作对种子进行调理。
    • 44. 发明申请
    • METHOD FOR EXTRACTING UNSAPONIFIABLES FROM RENEWABLE RAW MATERIALS
    • 从可再生原料中提取不可替代物的方法
    • US20120209018A1
    • 2012-08-16
    • US13503509
    • 2010-10-21
    • Antoine Piccirilli
    • Antoine Piccirilli
    • C11B1/10
    • C11B3/006C11B3/04C11B3/06
    • A method for extracting an unsaponifiable fraction from a renewable raw material selected among oilfruits, oleaginous seeds, oleoproteaginous seeds, seed husks, oil-yielding almonds, sprouts, stones and cuticles of fruits, high-fat raw materials from animals, algae, fungus or yeast, includes the following steps: a) dehydrating and packaging the renewable raw material, not resulting in any extraction of the fat; b) reactive crushing of the fatty packaged raw material in the presence of a light alcohol and a catalyst; c) evaporating the light alcohol; d) concentrating the liquid phase such as to obtain a concentrate including the unsaponifiable fraction diluted in fatty acid alkyl esters; e) saponifying the unsaponifiable concentrate; f) extracting the unsaponifiable fraction from the saponified mixture. The use of an unsaponifiable fraction or co-products obtained by implementing the method for preparing a composition such as a cosmetic, drug, food, or food additive or supplement is also described.
    • 从可可原料中提取不可皂化部分的方法,该可再生原料选自油果,油质种子,油蛋白质种子,种子壳,产油杏仁,芽果,果实的石头和角质层,动物,藻类,真菌等的高脂肪原料 酵母,包括以下步骤:a)脱水和包装可再生原料,不会导致任何脂肪的提取; b)在轻质醇和催化剂存在下对脂肪包装原料的反应性破碎; c)蒸发轻酒精; d)浓缩液相,以获得包含稀释在脂肪酸烷基酯中的不皂化的级分的浓缩物; e)皂化不皂化的浓缩液; f)从皂化混合物中提取不皂化的部分。 还描述了通过实施用于制备组合物如化妆品,药​​物,食品或食品添加剂或补充剂的方法获得的不皂化部分或共同产品的用途。
    • 45. 发明申请
    • Method For Obtaining A Fraction Enriched With Functionalized Fatty Acid Esters From Seeds of Oleaginous Plants
    • 获取含有油酸植物种子的官能化脂肪酸酯的分数的方法
    • US20120077999A1
    • 2012-03-29
    • US13145507
    • 2010-01-13
    • Antoine PiccirilliJacques BarbierJulien MagneJean-Luc Dubois
    • Antoine PiccirilliJacques BarbierJulien MagneJean-Luc Dubois
    • C11B1/10
    • C11C3/003C10G2300/1014C10L1/026C11C1/007C11C1/08Y02E50/13Y02P30/20
    • The invention relates to a method for the selective extraction of functionalised fatty acid esters from seeds of oleaginous plants, wherein said method includes: a) at least one step of extracting fatty acid esters that comprises simultaneously feeding into a reactor containing said seeds a light anhydrous alcohol, a basic catalyst and an extraction solvent non-miscible with said light alcohol and in which said functionalised fatty ester is not soluble in order to obtain a mixture of esters and glycerol; b) and at least one step of selectively extracting hydroxylated fatty acid esters by feeding into the reactor said extraction solvent in a backflush direction relative to the light alcohol in order to obtain an alcohol phase enriched with fatty acid esters, a glycerol phase and a cake. The invention can be used for obtaining a fraction having a high concentration of hydroxylated or epoxydised functionalised fatty acid esters, and a solvent phase containing the other non-functionalised fatty acid esters directly from the seeds of oleaginous plants.
    • 本发明涉及从含油植物的种子中选择性提取官能化脂肪酸酯的方法,其中所述方法包括:a)至少一步提取脂肪酸酯,其包括同时向包含所述种子的反应器中加入轻质无水 醇,碱性催化剂和与所述轻质醇不混溶的萃取溶剂,并且其中所述官能化脂肪酯不溶于水以获得酯和甘油的混合物; b)和至少一个步骤,通过以相对于轻质醇的反吹方向进入反应器中的所述萃取溶剂来选择性提取羟基化脂肪酸酯,以获得富含脂肪酸酯,甘油相和蛋糕的醇相 。 本发明可用于获得具有高浓度羟基化或环氧化官能化脂肪酸酯的级分,以及直接从含油植物种子中含有其它非官能化脂肪酸酯的溶剂相。