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31. 发明授权

US3539573A 11-basic substituted dibenzodiazepines and dibenzothiazepines 失效
标题翻译： 11-碱性替代二苯并二苯并二苯并噻吩
公开(公告)号：US3539573A
公开(公告)日：1970-11-10
申请号：US3539573D
申请日：1968-10-21
申请人： SCHMUTZ JEAN , HUNZIKER FRITZ
发明人： SCHMUTZ JEAN , HUNZIKER FRITZ
IPC分类号： C07C37/045 , C07D267/20 , C07D403/04 , C07D413/04 , C07D417/04 , C07D93/42 , C07D53/06
CPC分类号： C07D417/04 , C07D267/20 , C07D403/04 , C07D413/04

32. 发明授权

US3534092A Dispiropyran compounds having photochromic properties 失效
标题翻译：具有光致变色特性的吡咯烷酮化合物
公开(公告)号：US3534092A
公开(公告)日：1970-10-13
申请号：US3534092D
申请日：1966-06-07
申请人： SAINT GOBAIN
发明人： GAUTRON RENE LUCIEN
IPC分类号： C07C37/045 , C07C45/42 , C07C45/43 , C07C205/22 , C07D209/08 , C07D493/22 , G03C1/685 , C07D27/38
CPC分类号： G03C1/685 , C07C37/045 , C07C45/42 , C07C45/43 , C07C205/22 , C07D209/08 , C07C47/57 , C07C47/565 , C07C39/08

33. 发明授权

US3440277A Fluoroaromatic compounds 失效
标题翻译：氟化合物
公开(公告)号：US3440277A
公开(公告)日：1969-04-22
申请号：US3440277D
申请日：1965-12-13
申请人： US AIR FORCE
发明人： HOLLAND DEWEY G , TAMBORSKI CHRIST
IPC分类号： C07C17/00 , C07C17/12 , C07C37/045 , C07C63/33 , C07C63/72 , C07D209/48 , C07F1/02 , C07C63/00
CPC分类号： C07D209/48 , C07C17/00 , C07C17/12 , C07C37/045 , C07C63/72 , C07C243/00 , C07F1/02 , C07C25/18 , C07C39/367

34. 发明授权

US2464207A Crystalline dihydroxy phenols 失效
标题翻译：结晶二羟基酚
公开(公告)号：US2464207A
公开(公告)日：1949-03-15
申请号：US52798844
申请日：1944-03-24
申请人： BAMELITE CORP
发明人： BENDER HOWARD L , FARNHAM ALFORD G , GUYER JOHN W
IPC分类号： C07C37/00 , C07C37/045 , C07C37/20 , C07C39/16
CPC分类号： C07C37/20 , C07C37/002 , C07C37/045 , C07C39/16

35. 发明授权

US2267155A Diphenylphenol 失效
标题翻译：二苯基苯酚
公开(公告)号：US2267155A
公开(公告)日：1941-12-23
申请号：US36090240
申请日：1940-10-12
申请人： MONSANTO CHEMICALS
发明人： JENKINS RUSSELL L
IPC分类号： C07C37/045 , C07C37/66 , C07C39/15 , C07C39/235 , C08K5/13
CPC分类号： C07C37/66 , C07C37/045 , C07C39/15 , C07C39/235 , C08K5/13

36. 发明授权

US1910679A Production of hydroxylic compounds 失效
标题翻译：羟基化合物的生产
公开(公告)号：US1910679A
公开(公告)日：1933-05-23
申请号：US18389627
申请日：1927-04-14
申请人： MONSANTO CHEMICAL WORKS
发明人： CROOM CRAWFORD JOHN WILLIAM , GEORGE WILLSON FRANCIS
IPC分类号： C07C37/045 , C07C45/64
CPC分类号： C07C37/045 , C07C45/64 , C07C39/04 , C07C39/07 , C07C39/28

37. 发明授权

US11760709B2 Method for preparing resorcinol through micro-channel reaction 有权
公开(公告)号：US11760709B2
公开(公告)日：2023-09-19
申请号：US17329650
申请日：2021-05-25
申请人： Inner Mongolia Sheng Tang International Mongolian Medicine Research Institute Co., Ltd.
发明人： Weidong Liu , Yantao Hao , Guodong Liang , Qinqin Gao , Pengshuai Li , Ting Zhang
IPC分类号： C07C37/045 , C07C245/20 , C07C37/05
CPC分类号： C07C37/045 , C07C37/05 , C07C245/20 , C07C2601/16 , C07C37/045 , C07C39/08
摘要： The present disclosure provides a method for preparing resorcinol through micro-channel reaction. In the method, resorcinol is prepared through micro-channel reaction using m-aminophenol as a raw material, a diazo salt is synthesized at 0° C. or more, hydrolysis of the diazo salt is performed at 90° C. or less, and then reaction conditions are reduced; the reaction time is decreased from traditional 10 hours to less than 2 minutes, and therefore the reaction time is significantly shortened; the purity of a product is 75% or more, which is significantly improved. The method provided by the present disclosure has high heat exchange efficiency and high mass transfer rate; the efficiency of reaction is improved by hundreds of times; the reaction system is precisely controlled in the temperature and pressure, and safe and reliable in process, and meanwhile is capable of stably controlling hazard processes such as diazotization, so as to promote safe industry production, reduce energy consumption and greatly reduce industrial hazard waste emission and realize green ecology development.

38. 发明申请

US20200223784A1 PROCESS FOR CATALYTIC HYDROGENATION OF HALONITROAROMATICS 审中-公开
公开(公告)号：US20200223784A1
公开(公告)日：2020-07-16
申请号：US16744323
申请日：2020-01-16
申请人： Monsanto Technology LLC
发明人： John H. Ahn , Kam-To Wan
IPC分类号： C07C209/36 , B01J21/18 , B01J23/42 , B01J23/89 , C07C37/045 , B01J35/00 , C07C245/20 , C07C231/02
摘要： The present invention generally relates to processes for the catalytic hydrogenation of halonitroaromatics. In particular, the present invention includes processes for the catalytic hydrogenation of halonitroaromatics such as 2,5-dicloronitrobenzene to 2,5-dichloroaniline over a platinum-containing catalyst. The present invention also relates to processes for producing 3,6-dichloro-2-methoxybenzoic acid.

39. 发明申请

US20170342022A1 PROCESSES FOR THE DIAZOTIZATION OF 2,5-DICHLOROANILINES 有权
公开(公告)号：US20170342022A1
公开(公告)日：2017-11-30
申请号：US15619711
申请日：2017-06-12
申请人： Monsanto Technology LLC
发明人： Bruno De Kort , Matthew D. McReynolds , John J. Parlow , Rhonda S. Woerndle
IPC分类号： C07C245/20 , C07C51/09 , C07C37/045 , C07C209/36 , A01N37/40
CPC分类号： C07C245/20 , A01N37/40 , C07C37/045 , C07C51/09 , C07C209/365
摘要： The present disclosure relates, in general, to processes for converting 2,5-dichloroaniline compounds to the corresponding 2,5-dichlorobenzenediazonium compounds, and further relates to processes for the preparation of 2,5-dichlorophenol which is a key intermediate used in the manufacture of dicamba.

40. 发明授权

US09527789B2 Method for the preparation of phenols 有权
标题翻译：苯酚的制备方法
公开(公告)号：US09527789B2
公开(公告)日：2016-12-27
申请号：US14907671
申请日：2014-07-25
申请人： WEYLCHEM FRANKFURT GMBH
发明人： Klaus Forstinger , Reinhard Schwesinger , Andreas Maier
IPC分类号： C07C37/00 , C07C37/045 , C07C51/367 , C07C51/00
CPC分类号： C07C37/00 , C07C37/045 , C07C51/00 , C07C51/367 , C07C39/28 , C07C39/07 , C07C65/10
摘要： The present invention relates to a method for the preparation of phenols, in which an aryldiazonium salt, which is prepared by the diazotisation of a corresponding aromatic, primary amine, is decomposed by heating in a mixture containing hot water, a mineral acid and an organic solvent, wherein the organic solvent contains a ketone of formula (I) R1C(O)R2 in which R1 and R2 independently stand for (C1-C5)-alkyl and R1 and R2 together have at least four carbon atoms, wherein the aromatic primary amine is aniline or a substituted aniline, which contains at least one further substituent which is selected from: alkyl, alkenyl, alkynyl, halogen, haloalkyl, cycloalkyl, heteroaryl, carboxyl, cyan, alkoxyl and ester, and wherein substantially no copper salts are contained in the mixture.
摘要翻译：本发明涉及一种制备苯酚的方法，其中通过相应的芳族伯胺的重氮化制备的芳基重氮盐通过在含有热水，无机酸和有机物的混合物中加热而分解溶剂，其中有机溶剂含有式（I）R 1 C（O）R 2的酮，其中R 1和R 2独立地代表（C 1 -C 5） - 烷基，R 1和R 2一起具有至少4个碳原子，其中芳族伯胺是苯胺或取代的苯胺，其含有至少一个选自烷基，烯基，炔基，卤素，卤代烷基，环烷基，杂芳基，羧基，氰基，烷氧基和酯的另外的取代基，其中基本上不含铜盐在混合物中。

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