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31. 发明授权

US4690813A Molybdenum oxide whiskers and a method of producing the same 失效
标题翻译：氧化钼晶须及其制造方法
公开(公告)号：US4690813A
公开(公告)日：1987-09-01
申请号：US775659
申请日：1985-09-13
申请人： Yoshimi Kamijyo
发明人： Yoshimi Kamijyo
IPC分类号： C01G39/02 , C08K7/08
CPC分类号： C01G39/02 , C08K7/08 , C01P2004/03 , C01P2004/10 , C01P2004/20 , C01P2004/61 , Y02P20/582
摘要： A whisker of molybdenum oxide in the form of a filament, rod or flake. Molybdenum oxide whiskers are produced by firing metallic molybdenum at a temperature of at least 400.degree. C., preferably at least 800.degree. C., in an atmosphere containing oxygen, or by firing an organic molybdenum compound in an atmosphere containing oxygen at a temperature which is at least equal to its thermal decomposition temperature. They are very strong crystals which are expected to be useful as a filler for plastics and for a variety of other applications.
摘要翻译：氧化钼晶须为细丝，棒状或片状。氧化钼晶须通过在含有氧的气氛中在至少400℃，优选至少800℃的温度下焙烧金属钼，或者通过在含有氧气的气氛中焙烧有机钼化合物，至少等于其热分解温度。它们是非常强的晶体，其预期可用作塑料和各种其它应用的填料。

32. 发明授权

US4593012A Production of hydrocarbon-soluble salts of molybdenum for epoxidation of olefins 失效
标题翻译：生产用于烯烃环氧化的钼的烃溶性盐
公开(公告)号：US4593012A
公开(公告)日：1986-06-03
申请号：US708480
申请日：1985-03-05
申请人： Masahiro Usui , Yasuhiko Higashio
发明人： Masahiro Usui , Yasuhiko Higashio
IPC分类号： B01J23/00 , B01J23/28 , B01J31/04 , C01G39/00 , C01G39/02 , C07D301/19
CPC分类号： C07D301/19 , B01J31/04 , B01J2231/72
摘要： Production of novel hydrocarbon-soluble salts, especially adapted for use as catalysts in the epoxidation of olefinic compounds with an organic hydroperoxide, by reaction of an ammonium molybdate with a carboxylic acid in the presence of an organic amine at specified elevated temperatures while removing water.
摘要翻译：通过钼酸铵与羧酸在有机胺的存在下在规定的升高温度下反应同时除去水，特别适合用作烯烃化合物与有机氢过氧化物环氧化的新型烃溶性盐的生产。

33. 发明授权

US4587109A Process for the separate recovery of molybdenum and vanadium 失效
标题翻译：分离回收钼和钒的工艺
公开(公告)号：US4587109A
公开(公告)日：1986-05-06
申请号：US512005
申请日：1983-07-08
申请人： Georges Lyaudet , Jean Vial
发明人： Georges Lyaudet , Jean Vial
IPC分类号： C01G31/00 , C01G39/00 , C22B34/22 , C22B34/34 , C01G43/00 , C01G31/02 , C01G39/02
CPC分类号： C01G39/00 , C01G31/00 , C22B34/22 , C22B34/34
摘要： The invention relates to a process for recovering and purifying the molybdenum from a solution containing more molybdenum than vanadium.The process of the invention comprises the step of contacting the solution which contains molybdenum and vanadium, originally at a pH at least equal to 11 with an excess of an ammonium salt sufficient to precipitate the greatest part of vanadium in the form of solid ammonium vanadate, this excess being yet hot higher than a value such that after precipitation of vanadium, the quantity of ammonium having not reacted with the vanadate would be over a concentration which would account for risks of precipitating also molybdenum which is contained in the liquid phase of the supernatant.The molybdenum which is obtained is of industrial grade.
摘要翻译：本发明涉及从含有比钒更多的钼的溶液中回收和纯化钼的方法。本发明的方法包括使含有钼和钒的溶液最初在至少等于11的pH下与过量的铵盐接触以使固体钒酸铵形式的最大量的钒沉淀的步骤，该过剩仍然高于使钒沉淀后的未与钒酸盐反应的铵的量将超过沉淀的风险的浓度，还含有上清液相中的钼。得到的钼是工业级的。

34. 发明授权

US4555387A Flash roasting of molybdenum sulfide concentrates in a slagging reactor 失效
标题翻译：将硫化钼精矿在造渣反应器中进行快速焙烧
公开(公告)号：US4555387A
公开(公告)日：1985-11-26
申请号：US583905
申请日：1984-02-27
申请人： Bruce J. Sabacky , Malcolm T. Hepworth
发明人： Bruce J. Sabacky , Malcolm T. Hepworth
IPC分类号： C01G39/02 , C22B1/02 , C22B34/34
CPC分类号： C01G39/02 , C22B1/02 , C22B34/34
摘要： A process and system are provided for flash-roasting molybdenum sulfide containing slag-forming constituents. The process comprises feeding a pneumatically suspended stream of particulate molybdenum sulfide and a mixture of fuel and oxidizing gases through a nozzle into a confined furnace chamber, the fuel gas-oxidizing gas mixture exiting from the nozzle being ignited to provide a flame thereof, the flame being maintained at a condition to provide a temperature in the furnace chamber sufficient to oxidize the molybdenum sulfide and form a volatile gas comprising molybdenum trioxide. The temperature is at least sufficient to melt the slag-forming constituents such that the slag formed is sufficiently liquid to separate from the gaseous mixture and collect at a selected portion of said chamber for removal therefrom. The resulting gases in the volatile molybdenum trioxide are caused to flow from the furnace chamber to and through a condensing chamber, the temperature of the condensing chamber being controlled to condense the volatilized molybdenum trioxide and separate it from the off-gases.
摘要翻译：提供了一种快速焙烧含硫化钼的成渣成分的方法和系统。该方法包括将气体悬浮的颗粒状硫化钼料流和燃料和氧化气体的混合物通过喷嘴进入限制炉室，从喷嘴排出的燃料气体 - 氧化气体混合物被点燃以提供其火焰，火焰保持在炉室中提供足以氧化硫化钼并形成包含三氧化钼的挥发性气体的温度的条件。温度至少足以熔化形成成渣的成分，使得形成的炉渣充分地液体以与气体混合物分离并收集在所述室的选定部分以从中除去。使挥发性三氧化钼中的所得气体从炉室流出并通过冷凝室，冷凝室的温度被控制以冷凝挥发的三氧化钼并将其与废气分离。

35. 发明授权

US4551312A Process for converting molybdenite to molybdenum oxide 失效
标题翻译：将辉钼矿转化为氧化钼的工艺
公开(公告)号：US4551312A
公开(公告)日：1985-11-05
申请号：US670244
申请日：1984-11-13
申请人： William A. Yuill
发明人： William A. Yuill
IPC分类号： C01G39/02 , C22B1/02 , C22B34/34
CPC分类号： C22B1/02 , C01G39/02 , C22B34/34 , C01P2006/80
摘要： A process for converting molybdenite to molybdenum oxide by a flash roasting process wherein the molybdenum calcine produced in the flash roasting process is subsequently treated with a free chlorine-containing aqueous solution.
摘要翻译：通过闪蒸焙烧方法将辉钼矿转化为氧化钼的方法，其中在闪蒸焙烧过程中产生的钼煅烧物随后用游离的含氯水溶液处理。

36. 发明授权

US4512958A Method of recovering molybdenum oxide 失效
标题翻译：回收氧化钼的方法
公开(公告)号：US4512958A
公开(公告)日：1985-04-23
申请号：US546510
申请日：1983-10-28
申请人： Gunter Bauer , Joachim Eckert
发明人： Gunter Bauer , Joachim Eckert
IPC分类号： C01G39/02
CPC分类号： C01G39/02 , C01P2004/51 , C01P2004/61 , C01P2006/80
摘要： A method of recovering molybdenum oxide as in U.S. Pat. No. 4,379,127 wherein, however, the temperature in the autoclave and the pressure therein are controlled within narrow ranges by increasing the suspension density of the molybdenum sulfide suspension fed to the autoclave upon a fall in temperature and by adding water to the slurry of molybdenum sulfide concentrate formed before introduction into the autoclave upon an increase in temperature.
摘要翻译：回收氧化钼的方法如美国专利No. 然而，高压釜中的温度和其中的压力通过增加在温度下降时供给到高压釜中的硫化钼悬浮液的悬浮密度并通过向硫化钼的浆料中加入水来控制在窄范围内在温度升高之前，在引入高压釜之前形成浓缩物。

37. 发明授权

US4379127A Method of recovering molybdenum oxide 失效
标题翻译：回收氧化钼的方法
公开(公告)号：US4379127A
公开(公告)日：1983-04-05
申请号：US308845
申请日：1981-10-05
申请人： Gunter Bauer , Joachim Eckert
发明人： Gunter Bauer , Joachim Eckert
IPC分类号： C01G39/02 , C22B34/34
CPC分类号： C01G39/02 , C22B34/34 , C01P2004/61 , C01P2006/80 , C01P2006/82
摘要： A method of recovering molybdenum oxide by oxidation of a molybdenum sulfide concentrate contaminated with impurities wherein the concentrate in an average particle size in the range of 20 to 90 microns is suspended to form an aqueous suspension which is oxidized at elevated temperature and an elevated oxygen partial pressure in an autoclave. The suspension withdrawn from the autoclave is subjected to filtration to remove the molybdenum oxide from the primary filtrate containing sulfuric acid and this filtrate is neutralized with lime to form calcium sulfate which is then removed from the suspension to provide a second filtrate. According to the invention, only this second filtrate is recirculated at a rate such that the suspension density in the oxidation stage is between 100 to 150 g of solids per liter and this suspension density is maintained in the oxidation stage by the recirculation.
摘要翻译：通过氧化由杂质污染的硫化钼浓缩物来回收氧化钼的方法，其中将平均粒度在20至90微米范围内的浓缩物悬浮以形成在升高的温度下被氧化并且升高的氧部分高压釜中的压力。将从高压釜中取出的悬浮液过滤，从含有硫酸的初级滤液中除去氧化钼，用石灰中和该滤液，形成硫酸钙，然后从悬浮液中除去，得到第二滤液。根据本发明，只有该第二滤液以使得氧化阶段中的悬浮液密度在每升100至150g固体之间的速率再循环，并且该悬浮液密度通过再循环维持在氧化阶段。

38. 发明授权

US4245017A Battery cathode and method 失效
标题翻译：电池阴极和方法
公开(公告)号：US4245017A
公开(公告)日：1981-01-13
申请号：US33718
申请日：1979-04-26
申请人： Rudolph R. Haering , James A. R. Stiles , Klaus Brandt
发明人： Rudolph R. Haering , James A. R. Stiles , Klaus Brandt
IPC分类号： C01G39/02 , H01M4/02 , H01M4/36 , H01M4/04
CPC分类号： C01G39/02 , H01M4/02 , H01M4/36 , C01P2004/80
摘要： A method for producing electrodes for use in secondary cells. A suspension in oil of fine particles of electrode material is applied as a film to a metal foil substrate which is then baked in an inert atmosphere at temperatures high enough to drive off the oil yet below the melting point of the metal foil substrate. Oxygen is introduced to the baking atmosphere at selected times to slightly oxidize or carbonize the electrode material. The preferred electrode material is molybdenum disulphide and the invention is chiefly applicable to the fabrication of molybdenum disulphide battery cathodes on aluminum foil.
摘要翻译：一种用于制造用于二次电池的电极的方法。将电极材料微粒的油中的悬浮液作为膜施加到金属箔基材上，然后在惰性气氛中在足够高的温度下烘烤但不低于金属箔基材的熔点的油。在选定的时间将氧气引入烘烤气氛中，以使电极材料稍微氧化或碳化。优选的电极材料是二硫化钼，本发明主要适用于在铝箔上制造二硫化钼电池阴极。

39. 发明授权

US4221588A Oxidation roasting of ore 失效
标题翻译：矿石氧化焙烧
公开(公告)号：US4221588A
公开(公告)日：1980-09-09
申请号：US538181
申请日：1975-01-02
申请人： George R. Grimes, deceased
发明人： George R. Grimes, deceased
IPC分类号： C01G39/02 , C22B1/02 , C22B34/34 , C22B1/10
CPC分类号： C22B34/34 , C01G39/02 , C22B1/02
摘要： The roasting temperature of ore, such as sulfide concentrate, is controlled by feeding water and air under pressure to at least one spray nozzle located relative to a roasting zone containing the ore, means being employed for selectively varying the ratio of water and air fed to the nozzle in accordance with the temperature to be desired and maintained in the roasting zone.
摘要翻译：矿石的焙烧温度，如硫化物浓缩物，通过将压力下的水和空气送入位于相对于含有矿石的焙烧区的至少一个喷嘴来控制，所述装置用于选择性地改变供给的水和空气的比例喷嘴根据要求的温度和保持在焙烧区域。

40. 发明授权

US4045216A Direct reduction of molybdenum oxide to substantially metallic molybdenum 失效
标题翻译：将氧化钼直接还原成基本上金属的钼
公开(公告)号：US4045216A
公开(公告)日：1977-08-30
申请号：US627972
申请日：1975-11-03
申请人： Harry W. Meyer, deceased , Jerry D. Baker , William H. Ceckler
发明人： Harry W. Meyer, deceased , Jerry D. Baker , William H. Ceckler
IPC分类号： C01G39/02 , C22B34/34
CPC分类号： C01G39/02 , C22B34/34 , C01P2004/32 , C01P2004/50
摘要： A continuous process for producing a substantially dense pelletized metallic molybdenum product from an agglomerated molybdenum trioxide containing feed material in which the feed material is continuously charged at a controlled rate into a reactor formed with a first reaction maintained at a controlled first temperature and containing a first hydrogen-containing atmosphere having a controlled composition for effecting the exothermic reduction of molybdenum trioxide to molybdenum dioxide, whereafter the partially reduced pelletized feed is transferred at a controlled rate into a second reaction zone at a controlled higher temperature and incorporating a second hydrogen-containing atmosphere of a controlled different composition to effect an endothermic reduction of substantially all of the molybdenum dioxide to metallic molybdenum, which upon subsequent cooling is recovered as a pelletized product suitable for use in steelmaking, other metal alloy production, melting, chemical reaction operations and the like. The invention further contemplates a continuous single-stage process for producing a pelletized molybdenum dioxide product from a pelletized molybdenum trioxide feed material and a continuous single-stage process for producing a pelletized substantially metallic molybdenum product from a pelletized molybdenum dioxide feed material.
摘要翻译：一种用于从含聚集的含三氧化钼的进料中生产基本上致密的颗粒状金属钼产物的连续方法，其中将进料以受控的速率连续加入到形成有反应器的反应器中，所述反应器保持在受控的第一温度并含有第一具有控制组合物的含氢气氛，用于将三氧化钼放热还原成二氧化钼，然后将部分还原的造粒的进料以受控的速率转移到受控较高温度的第二反应区，并加入第二含氢气氛控制不同的组合物，以实现基本上所有的二氧化钼吸收还原成金属钼，金属钼在随后的冷却作为适合用于炼钢，其他金属合金生产，熔化，化学反应的造粒产品中被回收操作等。本发明进一步考虑了一种连续的单阶段方法，用于从造粒的三氧化钼进料中生产造粒的二氧化钼产品，以及用于从造粒的二氧化钼原料生产造粒的基本上金属的钼产品的连续的单阶段方法。

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