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    • 39. 发明申请
    • PROCESS AND APPARATUS FOR SEPARATION OF HYDROCARBONS AND NITROGEN
    • 用于分离碳氢化合物和氮的方法和装置
    • US20120090355A1
    • 2012-04-19
    • US13259355
    • 2010-03-23
    • Grant Leigh JohnsonTerence Ronald TomlinsonLee Alan Phillips
    • Grant Leigh JohnsonTerence Ronald TomlinsonLee Alan Phillips
    • F25J3/06
    • F25J3/0209F25J3/0233F25J3/0257F25J2200/04F25J2200/06F25J2200/74F25J2200/78F25J2210/06F25J2235/60F25J2270/02
    • The invention provides a process and apparatus for the separation of nitrogen from a gaseous feed comprising a mixture of hydrocarbons and nitrogen gas, the process comprising the steps of: (i) cooling and at least partially condensing the gaseous feed; (ii) feeding the cooled and at least partially condensed feed from step (i) to a first fractionation to produce an overhead vapour stream having an enriched nitrogen content and a condensed product having a reduced nitrogen content which is subjected to a second fractionation, which comprises reboil, at a lower pressure than the first fractionation; (iii) partially condensing the overhead vapour stream, and separating to provide a liquid stream, which is used to provide reflux to the first fractionation, and a separated vapour stream, which is condensed to provide reflux to the second fractionation; and (iv) sub-cooling the condensed product of the first fractionation and dividing the resulting sub-cooled product into at least two streams: a first stream being expanded and fed to the second fractionation, and a second stream being expanded and reheated in heat exchange with the separated vapour stream from step (ii) before being fed to the second fractionation; (v) removing a hydrocarbon product stream low in nitrogen from the second fractionation; and (vi) removing a nitrogen rich stream from the second fractionation.
    • 本发明提供了一种用于从包含烃和氮气的混合物的气态进料分离氮气的方法和装置,该方法包括以下步骤:(i)冷却并至少部分地冷凝气态进料; (ii)将来自步骤(i)的冷却和至少部分冷凝的进料进料至第一分馏以产生具有富氮含量的塔顶蒸气料流和具有降低的氮含量的冷凝产物,其进行第二次分馏, 包括在比第一分馏更低的压力下再沸腾; (iii)部分冷凝顶部蒸汽流,并分离以提供用于向第一分馏提供回流的液体流,以及分离的蒸气流,其被冷凝以提供回流至第二分馏; 和(iv)次冷却第一分馏的冷凝产物并将所得的副冷却产物分成至少两股:第一流被膨胀并进料至第二分馏,第二料流在热量下膨胀和再加热 在进料到第二分馏之前与来自步骤(ii)的分离的蒸气物流交换; (v)从第二分馏中除去低氮的烃产物流; 和(vi)从第二分馏中除去富氮物流。