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31. 发明授权

US06451450B1 Method of depositing a protective layer over a biaxially textured alloy substrate and composition therefrom 失效
标题翻译：在双轴织构的合金基底上沉积保护层的方法及其组成
公开(公告)号：US06451450B1
公开(公告)日：2002-09-17
申请号：US09563665
申请日：2000-05-02
申请人： Amit Goyal , Donald M. Kroeger , Mariappan Paranthaman , Dominic F. Lee , Roeland Feenstra , David P. Norton
发明人： Amit Goyal , Donald M. Kroeger , Mariappan Paranthaman , Dominic F. Lee , Roeland Feenstra , David P. Norton
IPC分类号： B32B1504
CPC分类号： H01L39/248 , C21D8/12 , C21D2201/04 , C21D2201/05 , C23C14/028 , C30B5/00 , C30B23/02 , C30B25/02 , C30B29/16 , C30B29/22 , H01L39/2454 , H01L39/2461 , Y10S505/775 , Y10S505/779 , Y10S505/812 , Y10T428/1259 , Y10T428/12944
摘要： A laminate article consists of a substrate and a biaxially textured protective layer over the substrate. The substrate can be biaxially textured and also have reduced magnetism over the magnetism of Ni. The substrate can be selected from the group consisting of nickel, copper, iron, aluminum, silver and alloys containing any of the foregoing. The protective layer can be selected from the group consisting of gold, silver, platinum, palladium, and nickel and alloys containing any of the foregoing. The protective layer is also non-oxidizable under conditions employed to deposit a desired, subsequent oxide buffer layer. Layers of YBCO, CeO2, YSZ, LaAlO3, SrTiO3, Y2O3, RE2O3, SrRuO3, LaNiO3 and La2ZrO3 can be deposited over the protective layer. A method of forming the laminate article is also disclosed.
摘要翻译：层压制品由衬底和衬底上的双轴纹理保护层组成。衬底可以是双轴织构的，并且还具有比Ni的磁性更低的磁性。基材可以选自镍，铜，铁，铝，银和含有上述任何一种的合金。保护层可以选自金，银，铂，钯和镍以及含有上述任何一种的合金。保护层在用于沉积所需的随后的氧化物缓冲层的条件下也是不可氧化的。 YBCO，CeO2，YSZ，LaAlO3，SrTiO3，Y2O3，RE2O3，SrRuO3，LaNiO3和La2ZrO3的层可以沉积在保护层上。还公开了一种形成层压制品的方法。

32. 发明申请

US20010003117A1 Method of preparing zeolite single crystals 有权
标题翻译：沸石单晶的制备方法
公开(公告)号：US20010003117A1
公开(公告)日：2001-06-07
申请号：US09730462
申请日：2000-12-05
申请人： Haldor Topsoe A/S
发明人： Claus J. Jacobsen , Jindrich Houzvicka , Iver Schmidt , Claus Madsen , Anna Carlsson
IPC分类号： C01B039/02
CPC分类号： C30B5/00 , B01J29/041 , C01B37/005 , C01B37/02 , C01B39/04 , C01B39/48 , C30B29/34 , Y10S423/22 , Y10S423/27
摘要： Method of preparing zeolite single crystals comprising the step of applying a synthesis gel with zeolite precursor composition within pore system and on surface of a particulate matrix material having a predetermined pore structure and particle size; subjecting the precursor composition to crystallising conditions; and isolating porous single crystals of the zeolite by removing the matrix material.
摘要翻译：制备沸石单晶的方法包括以下步骤：在孔体系内和在具有预定孔结构和粒径的颗粒基质材料的表面上施加具有沸石前体组合物的合成凝胶; 使前体组合物经历结晶条件; 并通过除去基质材料来分离沸石的多孔单晶。

33. 发明授权

US6139626A Three-dimensionally patterned materials and methods for manufacturing same using nanocrystals 有权
标题翻译：使用纳米晶体的三维图案化材料及其制造方法
公开(公告)号：US6139626A
公开(公告)日：2000-10-31
申请号：US148521
申请日：1998-09-04
申请人： David J. Norris , Yurii A. Vlasov
发明人： David J. Norris , Yurii A. Vlasov
IPC分类号： B82B3/00 , C30B5/00 , G02B6/122 , H01L21/368 , C30B7/02
CPC分类号： G02B6/1225 , B82Y20/00 , C30B29/605 , C30B5/00 , Y10T428/25
摘要： A method for patterning materials according to a predetermined, three-dimensional pattern, as well as patterned materials produced by said methods, are provided. A template is prepared comprising a template material, the template having a plurality of pores therein, the plurality of pores comprising a negative of the predetermined, three-dimensional pattern. Colloidal nanocrystals sufficient to fill the pores in the template are also prepared. The pores in the template are filled with the colloidal nanocrystals. A quantum-dot solid is formed from the colloidal nanocrystals within the pores in the template, such that the colloidal nanocrystals are concentrated as close-packed nanocrystals within the pores in the template in the predetermined, three-dimensional pattern. If desired, a conventional solid may be obtained by sintering the close-packed nanocrystals within the pores of the template.
摘要翻译：提供了根据预定的三维图案来图案化材料的方法，以及通过所述方法制造的图案化材料。制备包含模板材料的模板，所述模板在其中具有多个孔，所述多个孔包含预定的三维图案的负值。还制备了足以填充模板中的孔的胶体纳米晶体。模板中的孔被胶体纳米晶体填充。量子点固体由模板中的孔内的胶体纳米晶体形成，使得胶体纳米晶体以预定的三维图案在模板的孔内作为紧密堆积的纳米晶体浓缩。如果需要，可以通过在模板的孔内烧结紧密堆积的纳米晶体来获得常规的固体。

34. 发明授权

US6123845A Crystalline colloidal arrays in solid form 有权
标题翻译：固体形式的结晶胶体阵列
公开(公告)号：US6123845A
公开(公告)日：2000-09-26
申请号：US153521
申请日：1998-09-15
申请人： Sanford A. Asher , Jay Henis
发明人： Sanford A. Asher , Jay Henis
IPC分类号： C30B5/00 , G02B5/20 , G02B6/12 , G02B6/122 , G02B6/13 , B01D69/00 , B01J13/00
CPC分类号： C30B5/00 , B82Y20/00 , C30B29/60 , G02B5/203 , G02B5/206 , G02B6/1225 , G02B6/13 , G02B2006/12109 , G02B2006/12176 , Y10S977/773 , Y10T428/2982
摘要： A method of making a solid filter material which filters a predetermined wavelength band from a broader spectrum of radiation is provided. The method includes creating a colloidal structure composed of particles dispersed within a medium, and introducing a solvent thereto. Thereafter, the solvent is evaporated and the remaining structure solidifies into a solid crystalline array. The particles can also be fused together by polymerization using one of several methods which are provided. In another embodiment, methods of filtering submicron particles have been developed which consists of establishing a gel membrane from a crystalline colloidal array with an interstice size less than or equal to the particles to be filtered are disclosed. The gel membrane may employ anisotropic interstices of submicron size and is stretchable or compressible mechanically. The method also includes stacking a plurality of gel membrane filters so that the material to be filtered sequentially flows through the interstices of the filters leaving different size submicron particles on different levels of said filters. Another embodiment of the invention has a plurality of particles having a positive or negative charge in a lattice and has oppositely charged mobile particles movable into and out of the interstices of the gel membrane. An electric field is employed to move the mobile particles to close or open the interstices of the lattice. The mobile particles can also pump material through the interstices. Decorative uses of the materials are also disclosed.
摘要翻译：提供了制造从宽范围的辐射过滤预定波段的固体过滤材料的方法。该方法包括产生由分散在介质中的颗粒构成的胶体结构，并向其中引入溶剂。此后，蒸发溶剂，剩下的结构固化成固体晶体阵列。通过使用提供的几种方法之一通过聚合也可将颗粒熔合在一起。在另一个实施方案中，已经开发了过滤亚微米颗粒的方法，其包括由晶体尺寸小于或等于待过滤颗粒的晶体胶体阵列建立凝胶膜。凝胶膜可以使用亚微米尺寸的各向异性空隙，并且是机械可拉伸的或可压缩的。该方法还包括堆叠多个凝胶膜过滤器，使得待过滤的材料依次流过过滤器的间隙，在不同级别的所述过滤器上留下不同尺寸的亚微米颗粒。本发明的另一个实施方案具有多个在晶格中具有正电荷或负电荷的颗粒，并且具有可移入和移出凝胶膜间隙的相反电荷的可移动颗粒。使用电场来移动移动颗粒以关闭或打开格子的间隙。移动颗粒还可以通过间隙泵送材料。还公开了材料的装饰用途。

35. 发明授权

US6028020A Single crystal quartz thin film and preparation thereof 失效
标题翻译：单晶石英薄膜及其制备
公开(公告)号：US6028020A
公开(公告)日：2000-02-22
申请号：US567530
申请日：1995-12-05
申请人： Motoyuki Tanaka , Takahiro Imai , Naoji Fujimori
发明人： Motoyuki Tanaka , Takahiro Imai , Naoji Fujimori
IPC分类号： C30B5/00 , H03H3/02 , H03H9/19 , C03C10/12 , B05D3/02
CPC分类号： H03H9/19 , C30B29/18 , C30B5/00
摘要： A single crystal quartz thin film having a thickness of 5 nm to 50 .mu.m can be prepared by forming the thin film on a single crystal substrate by a sol-gel process and peeling the thin film from the substrate. The present invention can provide the single crystal quartz thin film at a low price without a large and complex apparatus.
摘要翻译：通过溶胶 - 凝胶法在单晶基板上形成薄膜，并从基板剥离薄膜，可以制备厚度为5nm〜50μm的单晶石英薄膜。本发明可以以低价格提供单晶石英薄膜而不需要大而复杂的装置。

36. 发明授权

US4806198A Producing alpha-alumina whiskers 失效
标题翻译：生产α-氧化铝晶须
公开(公告)号：US4806198A
公开(公告)日：1989-02-21
申请号：US115928
申请日：1987-11-02
申请人： Sujata Jagota , Rishi Raj
发明人： Sujata Jagota , Rishi Raj
IPC分类号： C30B5/00
CPC分类号： C30B5/00 , C30B29/20 , C30B29/62
摘要： Alpha-alumina whiskers are produced by forming a film of boehmite gel seeded with alpha-alumina seed material, preferably sapphire, and heating at 900.degree. C. to 1200.degree. C. for 5 minutes to 2 hours.
摘要翻译：通过形成用α-氧化铝种子材料（优选蓝宝石）接种的勃姆石凝胶膜并在900℃至1200℃加热5分钟至2小时来制备α-氧化铝晶须。

37. 发明授权

US4696808A Procedure to prepare transparent silica gels 失效
标题翻译：制备透明硅胶的步骤
公开(公告)号：US4696808A
公开(公告)日：1987-09-29
申请号：US933961
申请日：1986-11-24
申请人： Patrick G. Barber , Norman R. Simpson
发明人： Patrick G. Barber , Norman R. Simpson
IPC分类号： C01B33/154 , C30B5/00 , C01B33/12
CPC分类号： C30B5/00 , C01B33/154 , C30B29/12 , C30B29/46
摘要： A process for the preparation of transparent silica gels which can be used as crystal growth media is disclosed. A quantity of cation exchange resin beads is placed in a solution of a soluble potassium salt and stirred for several hours to allow the potassium ions to replace the cations on the resin beads. The supernatant liquid is then decanted through a filter, and the treated resin beads are rinsed with distilled water to remove excess salts. The treated resin beads are then transferred into a sodium silicate solution. The resulting mixture is stirred to allow the potassium ions on the treated resin beads to exchange with the sodium ions in the sodium silicate solution. The treated silicate solution is then poured through a coarse filter. A volume of boiled, cooled distilled water is added to a volume of the treated silicate solution, after which a volume of acetic acid solution is added to the mixture of distilled water and treated silicate solution. This mixture is then allowed to gel at room temperature, whereby a transparent silica gel is produced. The transparent silica gel is used as a crystal growth medium to simulate the convectionless environment of space and produce structurally perfect crystals.
摘要翻译：公开了可用作晶体生长介质的透明硅胶的制备方法。将一定数量的阳离子交换树脂珠置于可溶性钾盐溶液中并搅拌数小时以使钾离子替代树脂珠上的阳离子。然后将上清液通过过滤器倾析，用蒸馏水冲洗经处理的树脂珠以除去过量的盐。然后将经处理的树脂珠转移到硅酸钠溶液中。搅拌所得混合物，使处理后的树脂珠上的钾离子与硅酸钠溶液中的钠离子交换。然后将经处理的硅酸盐溶液通过粗过滤器倒入。将一定量的煮沸的冷却的蒸馏水加入一定体积的经处理的硅酸盐溶液中，然后将一定体积的乙酸溶液加入到蒸馏水和经处理的硅酸盐溶液的混合物中。然后将该混合物在室温下凝胶化，由此制备透明硅胶。透明硅胶用作晶体生长介质，以模拟空间的无对流环境，并产生结构完美的晶体。

38. 发明授权

US09997778B2 Polycrystalline vanadium oxide nanosheets 有权
公开(公告)号：US09997778B2
公开(公告)日：2018-06-12
申请号：US14440849
申请日：2013-11-05
申请人： University of Washington through its Center for Commercialization
发明人： Guozhong Cao , Yanwei Li
IPC分类号： H01M4/485 , H01M4/62 , C01G31/02 , C30B5/02 , C30B29/16 , C30B29/60 , H01M10/0525 , C30B5/00
CPC分类号： H01M4/485 , C01G31/02 , C01P2004/20 , C01P2006/12 , C01P2006/40 , C30B5/00 , C30B5/02 , C30B29/16 , C30B29/60 , H01M4/625 , H01M10/0525 , Y02T10/7011
摘要： Improved V2O5 materials are disclosed herein in the form of 2D leaf-like nanosheets. Methods of forming the V2O5 nanosheets and batteries (e.g., lithium-ion) incorporating the V2O5 nanosheets are also provided.

39. 发明授权

US09994442B2 Method for arranging fine particles on substrate by physical pressure 有权
公开(公告)号：US09994442B2
公开(公告)日：2018-06-12
申请号：US13263689
申请日：2010-04-09
申请人： Kyung Byung Yoon , Nguyen Khanh Nguyen , Cao Thanh Tung Pham
发明人： Kyung Byung Yoon , Nguyen Khanh Nguyen , Cao Thanh Tung Pham
IPC分类号： B32B5/16 , B05D1/36 , B81C1/00 , B82Y10/00 , B82Y30/00 , B82Y40/00 , C30B5/00 , C30B29/60 , G03F7/00
CPC分类号： B81C1/00373 , B82Y10/00 , B82Y30/00 , B82Y40/00 , C30B5/00 , C30B29/60 , G03F7/0002 , Y10T156/10 , Y10T428/24851 , Y10T428/24876 , Y10T428/24893 , Y10T428/25
摘要： Provided is a method of arranging particles on a substrate, the method including: (a) preparing a substrate, a surface of which has depressions or projections capable of fixing the positions and/or orientations of one or more particles; and (b) placing the particles on the substrate and applying a physical pressure to the particles so that a portion or the whole of each particle is inserted in each of pores defined by the depressions or the projections. Provided is also a method of arranging particles on a substrate, the method including: (a) preparing a substrate, at least a surface portion of which has adhesive property; and (b) placing particles, which do not have flat facets but curved surfaces, on the substrate and applying a physical pressure to the particles so that the particles are immobilized on adhesive surface portions of the substrate.

40. 发明授权

US09989673B2 Photonic crystal microsphere 有权
公开(公告)号：US09989673B2
公开(公告)日：2018-06-05
申请号：US15053443
申请日：2016-02-25
申请人： The Procter & Gamble Company , Institute of Chemistry, Chinese Academy of Sciences
发明人： Mingzhu Li , Qiang Yang , Yanlin Song , Libin Wang , Liang Yang , Ping Wang
IPC分类号： G02B1/00 , G02B1/04 , C08F2/22 , C30B29/58 , C30B5/00 , C30B29/16 , C30B29/46 , C30B29/60 , C08F220/56 , C08F222/38
CPC分类号： G02B1/005 , C08F2/22 , C08F220/56 , C08F222/385 , C30B5/00 , C30B29/16 , C30B29/46 , C30B29/58 , C30B29/60 , G02B1/04 , C08F212/08 , C08F220/14 , C08F220/06
摘要： A photonic crystal microsphere, comprising: a plurality of mono-dispersed polymer particles in a closely-packed and regularly-ordered structure, with interstition therebetween, forming the photonic crystal microsphere; and a co-assembly material contained in the interstition. The photonic crystal microsphere provides a structure of enhanced strength and a good color effect.

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