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    • 33. 发明授权
    • Method of manufacturing aggregated particles
    • 聚集颗粒的制造方法
    • US07833446B2
    • 2010-11-16
    • US11882372
    • 2007-08-01
    • Nobuhiro MaezawaKatsuru MatsumotoKeiichi Kikawa
    • Nobuhiro MaezawaKatsuru MatsumotoKeiichi Kikawa
    • G03G9/08
    • B29C67/06
    • The aggregated particles are manufactured through a method of manufacturing aggregated particles, which includes an aggregating step, a depressurizing step, and a cooling step. In the aggregating step, a slurry is prepared which contains aggregated particles obtained by flowing an aqueous slurry of resin fine particles having a volume average particle diameter in the range of 0.4 μm to 3 μm through a coiled piping in a heated and pressurized state and thereby aggregating the resin fine particles. In the depressurizing step, the slurry containing the aggregated particles is depressurized, and a particle size control is conducted by disintegrating coarse particles so as to homogenize particle diameters of the aggregated particles. In the cooling step, the slurry containing the aggregated particles of which particle diameters have been homogenized is cooled.
    • 聚集颗粒通过制造凝集颗粒的方法制造,其包括聚集步骤,减压步骤和冷却步骤。 在聚集步骤中,制备含有凝集颗粒的浆料,该凝集颗粒通过在加热和加压状态下通过卷取管道使体积平均粒径在0.4μm至3μm范围内的树脂细颗粒的水性浆液流动而获得, 聚集树脂细颗粒。 在减压步骤中,将含有凝集颗粒的浆料减压,并通过粉碎粗颗粒进行粒径控制,使凝聚颗粒的粒径均匀化。 在冷却步骤中,将含有粒径均匀化的凝集粒子的浆料冷却。
    • 35. 发明申请
    • Developing agent and process for producing the same
    • 开发代理和生产过程
    • US20060183045A1
    • 2006-08-17
    • US10544455
    • 2004-01-23
    • Shinichi NakanoYasuhiro ShibaiKeiichi Kikawa
    • Shinichi NakanoYasuhiro ShibaiKeiichi Kikawa
    • G03G9/08
    • G03G9/0804G03G9/0802
    • A method for manufacturing a developing agent comprising dissolving a binder resin component in a supercritical fluid or a subcritical fluid, mixing it with a colorant component, reducing the solubility of the binder resin component in the supercritical fluid or subcritical fluid, and causing the binder resin component to be deposited in the form of particles while the colorant component is dispersed within the binder resin component. After the pressure within a reaction vessel is decreased from A (MPa) to B (MPa) (where A>B>critical pressure) following the manufacture of a developing agent, the method proceeds back to a developing agent manufacturing step again when at least a developing agent material and a supercritical fluid or a subcritical fluid are injected into the reaction vessel under high pressure. The method allows the dispersibility of the colorant component in the developing agent to be increased up to a primary particle level, whereby a developing agent with an even particle shape and a narrow particle size distribution can be obtained. The method also makes continuous production possible without the need to open and close the reaction vessel, leading to a high production efficiency.
    • 一种制造显影剂的方法,包括将粘合剂树脂组分溶解在超临界流体或亚临界流体中,将其与着色剂组分混合,降低粘合剂树脂组分在超临界流体或亚临界流体中的溶解度,并使粘合剂树脂 组分以颗粒的形式沉积,而着色剂组分分散在粘合剂树脂组分中。 在制造显影剂之后,在反应容器中的压力从A(MPa)降低到B(MPa)(其中A> B>临界压力)之后,该方法至少再次返回到显影剂制造步骤 将显影剂材料和超临界流体或亚临界流体在高压下注入反应容器中。 该方法允许着色剂组分在显影剂中的分散性增加到初级颗粒水平,由此可以获得具有均匀颗粒形状和窄粒度分布的显影剂。 该方法也使连续生产成为可能,而不需要打开和关闭反应容器,从而导致高生产效率。
    • 36. 发明授权
    • Method of manufacturing toner, toner, two-component developer, developing device, and image forming apparatus
    • 调色剂,调色剂,双组分显影剂,显影装置和图像形成装置的制造方法
    • US08163458B2
    • 2012-04-24
    • US12167519
    • 2008-07-03
    • Keiichi KikawaKatsuru Matsumoto
    • Keiichi KikawaKatsuru Matsumoto
    • G03G9/08
    • G03G9/081G03G9/0815G03G9/0819
    • A toner capable of forming high quality images of excellent image reproducibility at high definition and high resolution, being decreased for the bleed-out of a wax ingredient to the surface, causing less filming to a photoreceptor and offset phenomenon in a high temperature region, is provided. The toner is manufactured by a method including a preliminary pulverizing step of pulverizing a melt-kneaded product of toner raw materials in a liquid to obtain a coarse powder slurry containing a coarse toner powder, a finely pulverizing step of passing the coarse powder slurry through a pressure resistant nozzle under heating and pressurization thereby further pulverizing the coarse toner powder to obtain a fine powder slurry containing a fine toner powder and in a heated and pressurized state, a cooling step of cooling the fine powder slurry, and a depressurizing step of depressurizing the fine powder slurry.
    • 能够以高分辨率和高分辨率形成高质量图像的高质量图像的调色剂,以降低蜡组分向表面的渗出,对高温区域的感光体和偏移现象造成较少的成膜。 提供。 该调色剂是通过以下方法制造的,所述方法包括将液体中的调色剂原料的熔融捏合产物粉碎以获得含有粗调色剂粉末的粗粉末浆料的初步粉碎步骤,使粗粉末浆料通过 耐压喷嘴,从而进一步粉碎粗调色剂粉末,得到含有细调色剂粉末的细粉末浆料,并且在加热和加压状态下,冷却细粉浆料的冷却步骤和减压步骤 细粉浆。
    • 37. 发明授权
    • Toner, method of manufacturing toner, developer, two-component developer, developing device, and image forming apparatus
    • 调色剂,调色剂的制造方法,显影剂,双组分显影剂,显影装置和图像形成装置
    • US08092968B2
    • 2012-01-10
    • US12403591
    • 2009-03-13
    • Keiichi KikawaAyae NagaokaKatsuru Matsumoto
    • Keiichi KikawaAyae NagaokaKatsuru Matsumoto
    • G03G9/08
    • G03G9/0819G03G9/0821G03G9/0827
    • The toner includes a plurality of toner particles containing a binder resin and a colorant. In toner particles, according to measurement by a flow particle image analyzer, the content of small size particles having a circle-equivalent diameter of 0.5 to 2.0 μm is 5% by number or less based on the entire toner particles, the content of medium size particles having a circle-equivalent diameter of more than 2.0 μm and 4.0 μm or less is 20% by number or more and 30% by number or less based on the entire toner particles, and the content of large size particles having a circle-equivalent diameter of more than 4.0 μm and 6.0 μm or less is 50% by number or more and 70% by number or less based on the entire toner particles, and the shape factor of the toner particles SF1 is 130 or more and 140 or less.
    • 调色剂包括含有粘合剂树脂和着色剂的多个调色剂颗粒。 在调色剂颗粒中,根据流动颗粒图像分析仪的测定,圆当量直径为0.5〜2.0μm的小粒子的含量相对于整个调色剂颗粒为5个数量%以下,中等尺寸的含量 圆当量直径大于2.0μm和4.0μm以下的颗粒相对于整个调色剂颗粒为20数量级以上且30数量%以下,并且具有圆当量的大尺寸颗粒的含量 大于4.0μm和6.0μm或更小的直径基于整个调色剂颗粒为50数量级以上且70数量%以下,调色剂颗粒SF1的形状因子为130以上且140以下。
    • 38. 发明授权
    • Method of manufacturing resin particles
    • 树脂颗粒的制造方法
    • US07770828B2
    • 2010-08-10
    • US11937547
    • 2007-11-09
    • Katsuru MatsumotoKeiichi KikawaAyae Nagaoka
    • Katsuru MatsumotoKeiichi KikawaAyae Nagaoka
    • B02C23/00
    • G03G9/0804C08J3/12C08J2300/00C08J2367/02G03G9/081G03G9/0815
    • Method of manufacturing resin particles capable of manufacturing resin particles of controlled particle size stably and efficiently by removing bubbles from the surface of a molten kneaded product as the raw material for resin particles thereby sufficiently ensuring action sites for a surfactant on the surface of the molten kneaded product, is provided. The method includes a coarsely-pulverizing step of pressurizing a mixture of a molten kneaded product containing a synthetic resin and an aqueous medium containing a surfactant to 15 MPa to 120 MPa thereby removing bubbles attached to the molten kneaded product containing the synthetic resin, and a finely-granulating step of finely granulating, by a high pressure homogenizer method, an aqueous slurry containing coarse particles of a molten kneaded product passing through a pressure proof nozzle in the coarsely-pulverizing step and in a state where bubbles attached to the surface are removed.
    • 通过从作为树脂颗粒的原料的熔融混炼物的表面除去气泡,从而充分确保熔融混炼的表面上的表面活性剂的作用部位,能够稳定有效地制造具有受控粒径的树脂颗粒的树脂颗粒的制造方法 产品。 该方法包括将含有合成树脂的熔融混炼物和含有表面活性剂的水性介质的混合物加压至15MPa〜120MPa的粗粉碎工序,除去附着在含有合成树脂的熔融混炼物上的气泡, 通过高压均化器细碎造粒,在粗粉碎工序中通过耐压喷嘴的熔融混炼物的粗粒子和附着在表面上的气泡被除去的状态下, 。