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31. 发明授权

US08192711B2 Process for production of cathode active material for lithiun ion secondary battery 有权
标题翻译：锂离子二次电池用正极活性物质的制造方法
公开(公告)号：US08192711B2
公开(公告)日：2012-06-05
申请号：US12606224
申请日：2009-10-27
申请人： Megumi Uchida , Takeshi Kawasato , Remi Hiraki
发明人： Megumi Uchida , Takeshi Kawasato , Remi Hiraki
IPC分类号： C01G51/00
CPC分类号： H01M4/505 , H01M4/1315 , H01M4/362 , H01M4/485 , H01M4/525 , H01M10/052 , Y10T428/2991 , Y10T428/2993
摘要： To provide a process for producing a surface modified lithium-containing composite oxide, which is excellent in discharge capacity, volume capacity density, safety, durability for charge and discharge cycles and an excellent rate property, at a low production cost.The present invention is characterized in that a process for producing a surface modified lithium-containing composite oxide, wherein a lithium titanium composite oxide is contained in the surface layer of particles of a lithium-containing composite oxide represented by the formula: LipNxMyOzFa, where N is at least one element selected from the group consisting of Co, Mn and Ni, M is at least one element selected from the group consisting of Al, Sn, alkaline earth metal elements and transition metal elements other than Co, Mn and Ni, 0.9≦p≦1.3, 0.9≦x≦2.0, 0≦y≦0.1, 1.9≦z≦4.2, and 0≦a≦0.05, which comprises impregnating a solution having a lithium source and a titanium source dissolved therein, followed by heat treatment at a determined temperature, to obtain the surface modified lithium-containing composite oxide, wherein the titanium contained in the surface layer is from 0.01 to 1.95 mol %.
摘要翻译：为了提供一种生产成本低的放电容量，容量容量密度，安全性，充放电循环的耐久性和优异的速率特性的表面改性的含锂复合氧化物的方法。本发明的特征在于一种表面改性的含锂复合氧化物的制造方法，其中，在下式表示的锂复合氧化物的表面层中含有锂钛复合氧化物，式中，N表示下式：LipNxMyOzFa，其中N 是选自Co，Mn和Ni中的至少一种元素，M是选自Al，Sn，碱土金属元素和Co，Mn和Ni以外的过渡金属元素中的至少一种元素，0.9 其中包括浸渍溶解有锂源和钛源的溶液，其中包括溶解在其中的锂源和溶解有钛源的溶液，随后通过在确定的温度下进行热处理，得到表面改性的含锂复合氧化物，其中表面层中所含的钛为0.01〜1.95摩尔％。

32. 发明授权

US08101143B2 Process for producing lithium-containing composite oxide for positive electrode for lithium secondary battery 失效
标题翻译：锂二次电池用正极用锂复合氧化物的制造方法
公开(公告)号：US08101143B2
公开(公告)日：2012-01-24
申请号：US11529301
申请日：2006-09-29
申请人： Takeshi Kawasato , Megumi Uchida , Toshiaki Abe , Naoshi Saito , Manabu Suhara
发明人： Takeshi Kawasato , Megumi Uchida , Toshiaki Abe , Naoshi Saito , Manabu Suhara
IPC分类号： H01M4/58 , H01M4/50 , H01M4/52 , C01D15/00
CPC分类号： H01M4/525 , C01G45/1228 , C01G51/42 , C01G53/42 , C01P2002/52 , C01P2006/12 , C01P2006/40 , H01M4/131 , H01M4/1315 , H01M4/485 , H01M4/505 , H01M10/052
摘要： A process for producing a lithium-containing composite oxide for a positive electrode active material for use in a lithium secondary battery, the oxide having the formula LipNxMmOzFa (wherein N is at least one element selected from the group consisting of Co, Mn and Ni, M is at least one element selected from the group consisting of Al, alkaline earth metal elements and transition metal elements other than N, 0.9≦p≦1.2, 0.9≦x
摘要翻译：一种锂二次电池用正极活性物质的含锂复合氧化物的制造方法，其特征在于，具有式LiNiMMOzFa（其中，N为选自Co，Mn，Ni， M是选自Al，碱土金属元素和除N之外的过渡金属元素中的至少一种元素，0.9和nlE; p

33. 发明申请

US20100173199A1 SURFACE MODIFIED LITHIUM-CONTAINING COMPOSITE OXIDE FOR CATHODE ACTIVE MATERIAL FOR LITHIUN ION SECONDARY BATTERY AND ITS PRODUCTION PROCESS 审中-公开
标题翻译：用于锂离子二次电池的阴极活性材料的表面改性含锂复合氧化物及其制备方法
公开(公告)号：US20100173199A1
公开(公告)日：2010-07-08
申请号：US12683458
申请日：2010-01-07
申请人： Remi Hiraki , Takeshi Kawasato
发明人： Remi Hiraki , Takeshi Kawasato
IPC分类号： H01M4/58 , H01M4/88 , H01M4/525 , H01M4/505
CPC分类号： C01G23/003 , C01G45/1221 , C01G51/42 , C01G53/42 , C01P2002/52 , C01P2002/72 , C01P2004/51 , C01P2006/12 , C01P2006/40 , C04B35/01 , C04B35/62675 , C04B35/62821 , C04B35/62886 , C04B2235/3203 , C04B2235/3206 , C04B2235/3217 , C04B2235/3244 , C04B2235/3268 , C04B2235/3275 , C04B2235/3279 , C04B2235/3293 , C04B2235/442 , C04B2235/445 , C04B2235/449 , C04B2235/5409 , C04B2235/5436 , C04B2235/5481 , C04B2235/768 , H01M4/1315 , H01M4/362 , H01M4/38 , H01M10/0525 , H01M2004/028
摘要： To provide a surface modified lithium-containing composite oxide for a cathode active material for a lithium ion secondary cell, which is excellent in volume capacity density, safety, durability for charge and discharge cycles and an excellent rate property, and its production process.Particles of a lithium-containing composite oxide represented by the formula: LipNxMyOzFa, wherein N is at least one element selected from the group consisting of Co, Mn and Ni, M is at least one element selected from the group consisting of Al, Sn, alkaline earth metal elements and transition metal elements other than N, 0.9≦p≦1.3, 0.9≦x≦2.0, 0≦y≦0.1, 1.9≦z≦4.2, and 0≦a≦0.05, are impregnated with a solution containing a lanthanoid source and a titanium source, followed by heat treatment at from 550 to 1,000° C., to prepare a surface modified lithium-containing composite oxide having a highly crystalline lithium lanthanoid titanium composite oxide having a perovskite structure containing no fluorine contained in the surface layer of the particles.
摘要翻译：为了提供用于锂离子二次电池用正极活性物质的表面改性含锂复合氧化物及其制造方法，其体积容积密度，安全性，充放电循环的耐久性和优异的速率性质优异。由下式表示的含锂复合氧化物的颗粒：LipNxMyOzFa，其中N为选自Co，Mn和Ni中的至少一种元素，M为选自Al，Sn，碱土金属元素和过渡金属元素，除N，0.9和nlE之外; p＆nlE; 1.3,0.9和nlE; x和nlE; 2.0,0和nlE; y和nlE; 0.1,1.9和nlE; z和nlE; 4.2和0＆含有镧系元素源和钛源的溶液，然后在550〜1000℃下进行热处理，制备具有不含氟的钙钛矿结构的高结晶性锂镧系元素复合氧化物的表面改性含锂复合氧化物在颗粒的表面层。

34. 发明授权

US08163198B2 Process for producing lithium-containing composite oxide for positive electrode of lithium secondary battery 失效
标题翻译：锂二次电池用正极用锂复合氧化物的制造方法
公开(公告)号：US08163198B2
公开(公告)日：2012-04-24
申请号：US11940689
申请日：2007-11-15
申请人： Naoshi Saito , Takeshi Kawasato , Tokumitsu Kato , Kazushige Horichi
发明人： Naoshi Saito , Takeshi Kawasato , Tokumitsu Kato , Kazushige Horichi
IPC分类号： H01M4/88
CPC分类号： H01M4/505 , C01G3/006 , C01G45/006 , C01G45/1228 , C01G51/006 , C01G51/42 , C01G51/50 , C01G53/006 , C01G53/42 , C01G53/50 , C01P2002/52 , C01P2002/54 , C01P2002/72 , C01P2004/51 , C01P2004/61 , C01P2004/62 , C01P2006/11 , C01P2006/12 , C01P2006/40 , H01M4/485 , H01M4/525 , H01M10/052
摘要： A process for producing a lithium-containing composite oxide having a large volume capacity density, high safety, excellent durability for charge/discharge cycles, and excellent low temperature characteristics. An oxide of general formula LipNxMyOzFa (wherein N is at least one of Co, Mn or Ni, M is at least one of Al, an alkali earth metal element, a transition metal element other than N, 0.9≦p≦1.2, 0.97≦x≦1.00, 0≦y≦0.03, 1.9≦z≦2.2, x+y=1 and 0≦a≦0.02) can be produced.
摘要翻译：一种具有大容量密度，高安全性，充放电循环的优异耐久性和优异的低温特性的含锂复合氧化物的制造方法。通式为LiNiMyOzFa的氧化物（其中N为Co，Mn或Ni中的至少一种，M为Al，碱土类金属元素，N以外的过渡金属元素中的至少一种，0.9＆nlE; p＆nlE; 1.2,0.97 ＆nlE; x＆nlE; 1.00，0＆nlE; y＆nlE; 0.03，1.9＆nlE; z＆nlE; 2.2，x + y = 1和0＆nlE; a＆nlE; 0.02）。

35. 发明申请

US20070298324A1 PROCESS FOR PRODUCING LITHIUM-CONTAINING COMPOSITE OXIDE FOR POSITIVE ELECTRODE FOR LITHIUM SECONDARY BATTERY 有权
标题翻译：生产用于锂二次电池的正电极的含锂复合氧化物的方法
公开(公告)号：US20070298324A1
公开(公告)日：2007-12-27
申请号：US11838283
申请日：2007-08-14
申请人： Takeshi Kawasato , Tokumitsu Kato , Megumi Uchida , Naoshi Saito , Manabu Suhara
发明人： Takeshi Kawasato , Tokumitsu Kato , Megumi Uchida , Naoshi Saito , Manabu Suhara
IPC分类号： H01M4/58 , H01M4/50 , H01M4/52 , C01B35/06 , C01B35/10 , C01B25/45 , C01B25/455
CPC分类号： H01M4/525 , C01G3/006 , C01G51/42 , C01G53/42 , C01P2002/52 , C01P2002/54 , C01P2002/72 , C01P2002/74 , C01P2004/03 , C01P2004/32 , C01P2004/50 , C01P2004/51 , C01P2004/61 , C01P2006/11 , C01P2006/12 , C01P2006/40 , H01M4/1315 , H01M4/13915 , H01M4/505 , H01M2004/021 , H01M2004/028
摘要： To provide a cathode active material for a lithium secondary battery, which is low in gas generation and has high safety and excellent durability for charge and discharge cycles even at a high charge voltage. A process for producing a lithium-containing composite oxide represented by the formula LipLqNxMyOzFa (wherein L is at least one element selected from the group of B and P, N is at least one element selected from the group consisting of Co, Mn and Ni, M is at least one element selected from the group consisting of Al, alkaline earth metal elements and transition metal elements other than N, 0.9≦p≦1.1, 1.0≦q
摘要翻译：为了提供即使在高充电电压下，气体产生低，并具有高安全性和优异的充放电循环耐久性的锂二次电池用正极活性物质。一种制备由下式表示的含锂复合氧化物的方法：其中R 1，R 2，R 2，R 3，（其中L是选自B和P中的至少一种元素，N是选自Co，Mn中的至少一种元素） Ni，M是选自Al，碱土金属元素和N以外的过渡金属元素中的至少一种元素，0.9 <= p <= 1.1,1.0 <= q <0.03,0.97 <= x <1.00 ，0 <= y <= 0.03，1.9 <= z <= 2.1，q + x + y = 1，0 <= a <= 0.02），其中含有N元素的锂复合氧化物粉末，M元素和氟原子; 将含锂复合氧化物粉末与含有L元素源的水溶液混合; 从所得混合物中除去水性介质，然后在含氧气氛中在300〜1050℃下烧成。

36. 发明申请

US20070026314A1 Process for producing lithium-containing composite oxide for positive electrode for lithium secondary battery 失效
标题翻译：锂二次电池用正极用锂复合氧化物的制造方法
公开(公告)号：US20070026314A1
公开(公告)日：2007-02-01
申请号：US11529301
申请日：2006-09-29
申请人： Takeshi Kawasato , Megumi Uchida , Toshiaki Abe , Naoshi Saito , Manabu Suhara
发明人： Takeshi Kawasato , Megumi Uchida , Toshiaki Abe , Naoshi Saito , Manabu Suhara
IPC分类号： H01M4/58 , H01M4/50 , H01M4/52 , C01D15/00
CPC分类号： H01M4/525 , C01G45/1228 , C01G51/42 , C01G53/42 , C01P2002/52 , C01P2006/12 , C01P2006/40 , H01M4/131 , H01M4/1315 , H01M4/485 , H01M4/505 , H01M10/052
摘要： It is to provide a positive electrode active material for a lithium secondary battery, which has a large volume capacity density, high safety, excellent properties for uniform coating, excellent durability for charge and discharge cycles and low temperature characteristics even at a high charge voltage. A process for producing a lithium-containing composite oxide represented by the formula LipNxMmOzFa (wherein N is at least one element selected from the group consisting of Co, Mn and Ni, M is at least one element selected from the group consisting of Al, alkaline earth metal elements and transition metal elements other than N, 0.9≦p≦1.2, 0.9≦x
摘要翻译：本发明提供一种用于锂二次电池的正极活性物质，其即使在高充电电压下也具有体积容积密度大，安全性高，涂膜均匀性优异的充放电循环耐久性和低温特性。一种制备由下式表示的含锂复合氧化物的方法：其中R 1，R 2，R 2，R 3，（其中N是选自Co，Mn和Ni中的至少一种元素，M是选自Al，碱土金属元素和过渡金属中的至少一种元素）除了N以外的元素，0.9 <= p <= 1.2,0.9 <= x <1.00,0

37. 发明授权

US08795896B2 Lithium-containing composite oxide and its production method 有权
标题翻译：含锂复合氧化物及其制备方法
公开(公告)号：US08795896B2
公开(公告)日：2014-08-05
申请号：US12486799
申请日：2009-06-18
申请人： Takeshi Kawasato , Takuya Mihara , Koichiro Ueda , Yukimitsu Wakasugi , Nozomi Honda
发明人： Takeshi Kawasato , Takuya Mihara , Koichiro Ueda , Yukimitsu Wakasugi , Nozomi Honda
IPC分类号： H01M4/00 , H01M4/36 , H01M4/525 , H01M4/131
CPC分类号： H01M4/36 , C01G45/1228 , C01G51/50 , C01G53/50 , C01P2002/52 , C01P2004/32 , C01P2004/51 , C01P2004/53 , C01P2004/61 , C01P2006/11 , C01P2006/12 , C01P2006/40 , H01M4/02 , H01M4/131 , H01M4/485 , H01M4/505 , H01M4/525 , H01M10/052 , H01M2004/021
摘要： A lithium/nickel/cobalt/manganese-containing composite oxide powder represented by the formula LipNixCoyMnzMqO2-aFa (wherein M is at least one element selected from the group consisting of Al, Ge, Sn, alkaline earth metal elements and transition metal elements other than Co, Mn and Ni, 0.9≦p≦1.1, 0.2≦x≦0.5, 0.2≦y≦0.5, 0.1≦z≦0.4, 0≦q≦0.5, 1.9≦a≦2.1, p+x+y+z+q=2, and 0≦a≦0.02), characterized in that when the powder is classified into small particle size-classified particles with an average particle size 2 μm≦D50≦8 μm and large particle size-classified particles with an average particle size of 10 μm≦D50≦75 μm, the ratio of (% by weight of the small particle size-classified particles)/(% by weight of the large particle size-classified particles) is from 15/85 to 40/60.
摘要翻译：由式LipNixCoyMnzMqO2-aFa（其中M为选自Al，Ge，Sn，碱土金属元素和过渡金属元素中的至少一种元素的锂/镍/钴/锰复合氧化物粉末） Co，Mn和Ni，0.9＆nlE; p＆nlE; 1.1,0.2＆amp; nlE; x＆lt; lE; 0.5,0.2＆nlE; y＆nlE; 0.5,0.1＆nlE; z＆nlE; 0.4,0和nlE; q＆nlE; 0.5,1.9＆ + y + z + q = 2和0＆nlE; a＆nlE; 0.02），其特征在于，当粉末分为平均粒度为2μm＆nlE; D50＆nlE;8μm的小颗粒尺寸分级颗粒时，平均粒径为10μm＆nlE; D50＆nlE;75μm的颗粒，（小粒径分级粒子的重量％）/（重量％）是15/85 至40/60。

38. 发明授权

US07842268B2 Process for producing lithium-containing composite oxide for positive electrode for lithium secondary battery 有权
标题翻译：锂二次电池用正极用锂复合氧化物的制造方法
公开(公告)号：US07842268B2
公开(公告)日：2010-11-30
申请号：US11838283
申请日：2007-08-14
申请人： Takeshi Kawasato , Tokumitsu Kato , Megumi Uchida , Naoshi Saito , Manabu Suhara
发明人： Takeshi Kawasato , Tokumitsu Kato , Megumi Uchida , Naoshi Saito , Manabu Suhara
IPC分类号： H01M4/00
CPC分类号： H01M4/525 , C01G3/006 , C01G51/42 , C01G53/42 , C01P2002/52 , C01P2002/54 , C01P2002/72 , C01P2002/74 , C01P2004/03 , C01P2004/32 , C01P2004/50 , C01P2004/51 , C01P2004/61 , C01P2006/11 , C01P2006/12 , C01P2006/40 , H01M4/1315 , H01M4/13915 , H01M4/505 , H01M2004/021 , H01M2004/028
摘要： To provide a cathode active material for a lithium secondary battery, which is low in gas generation and has high safety and excellent durability for charge and discharge cycles even at a high charge voltage.A process for producing a lithium-containing composite oxide represented by the formula LipLqNxMyOzFa (wherein L is at least one element selected from the group of B and P, N is at least one element selected from the group consisting of Co, Mn and Ni, M is at least one element selected from the group consisting of Al, alkaline earth metal elements and transition metal elements other than N, 0.9≦p≦1.1, 1.0≦q
摘要翻译：为了提供即使在高充电电压下，气体产生低，并具有高安全性和优异的充放电循环耐久性的锂二次电池用正极活性物质。一种由式LiLqNxMyOzFa（其中L是选自B和P中的至少一种元素，N是选自Co，Mn和Ni中的至少一种元素）的由式LiLqNxMyOzFa表示的含锂复合氧化物的方法， M是选自Al，碱土金属元素和除N之外的过渡金属元素中的至少一种元素，0.9＆nlE; p＆nlE; 1.1,1.0＆amp; nlE; q <0.03,0.97＆amp; nlE; x <1.00,0和nlE; y＆ ;其中含有N元素，如果需要的话，含有M元素和氟的含锂复合氧化物粉末是预先形成的，其中，0.03，1.9和nlE; z和nlE; 2.1，q + x + y = 1和0＆准备将含锂复合氧化物粉末与含有L元素源的水溶液混合; 从所得混合物中除去水性介质，然后在含氧气氛中在300〜1050℃下烧成。

39. 发明授权

US07709148B2 Lithium-containing composite oxide and its production process 有权
标题翻译：含锂复合氧化物及其生产工艺
公开(公告)号：US07709148B2
公开(公告)日：2010-05-04
申请号：US11952185
申请日：2007-12-07
申请人： Takeshi Kawasato , Tokumitsu Kato , Naoshi Saito , Koji Tatsumi , Megumi Uchida , Remi Hiraki
发明人： Takeshi Kawasato , Tokumitsu Kato , Naoshi Saito , Koji Tatsumi , Megumi Uchida , Remi Hiraki
IPC分类号： H01M4/00
CPC分类号： C01G53/42 , C01G45/1221 , C01G51/42 , C01P2002/52 , C01P2004/51 , C01P2004/61 , C01P2006/40 , H01M4/131 , H01M4/1315 , H01M4/485 , H01M4/505 , H01M4/525 , H01M10/052
摘要： To provide a process for producing a lithium-containing composite oxide for a positive electrode of a lithium secondary battery, which has a large volume capacity density, high safety, excellent durability for charge and discharge cycles and excellent low temperature characteristics.
摘要翻译：本发明提供一种锂二次电池正极用含锂复合氧化物的制造方法，其具有容量密度大，安全性高，充放电循环耐久性优异，低温特性优良的特征。

40. 发明申请

US20090258296A1 LITHIUM-CONTAINING COMPOSITE OXIDE AND ITS PRODUCTION METHOD 有权
标题翻译：含锂的复合氧化物及其生产方法
公开(公告)号：US20090258296A1
公开(公告)日：2009-10-15
申请号：US12486799
申请日：2009-06-18
申请人： Takeshi Kawasato , Takuya Mihara , Koichiro Ueda , Yukimitsu Wakasugi , Nozomi Honda
发明人： Takeshi Kawasato , Takuya Mihara , Koichiro Ueda , Yukimitsu Wakasugi , Nozomi Honda
IPC分类号： H01M4/32 , H01M4/52
CPC分类号： H01M4/36 , C01G45/1228 , C01G51/50 , C01G53/50 , C01P2002/52 , C01P2004/32 , C01P2004/51 , C01P2004/53 , C01P2004/61 , C01P2006/11 , C01P2006/12 , C01P2006/40 , H01M4/02 , H01M4/131 , H01M4/485 , H01M4/505 , H01M4/525 , H01M10/052 , H01M2004/021
摘要： To provide a lithium/nickel/cobalt/manganese-containing composite oxide powder which has a high weight capacity density, a high packing property, an excellent cycle property, an excellent discharge rate property and an excellent safety, and which has little content of free alkalis and is free from gelation at a time of producing a slurry.A lithium/nickel/cobalt/manganese-containing composite oxide powder represented by the formula LipNixCoyMnzMqO2-aFa (wherein M is at least one element selected from the group consisting of Al, Ge, Sn, alkaline earth metal elements and transition metal elements other than Co, Mn and Ni, 0.9≦p≦1.1, 0.2≦x≦0.5, 0.2≦y≦0.5, 0.1≦z≦0.4, 0≦q≦0.05, 1.9≦2-a≦2.1, p+x+y+z+q=2, and 0≦a≦0.02), characterized in that when the powder is classified into small particle size-classified particles with an average particle size of 2 μm≦D50≦8 μm and large particle size-classified particles with an average particle size of 10 μm≦D50≦25 μm, the ratio of (% by weight of the small particle size-classified particles)/(% by weight of the large particle size-classified particles) is from 15/85 to 40/60, the molar ratio (ps) of lithium to the total of nickel, cobalt, manganese and the M element contained in the small particle size-classified particles is smaller than the molar ratio (pl) of lithium to the total of nickel, cobalt, manganese and the M element contained in the large particle size-classified particles.
摘要翻译：为了提供具有高重量容量密度，高包装性，优异的循环性能，优异的排出速率特性和优异的安全性的锂/镍/钴/锰复合氧化物粉末，并且几乎没有游离的含量碱，并且在制备浆料时不凝胶化。由式LipNixCoyMnzMqO2-aFa（其中M为选自Al，Ge，Sn，碱土金属元素和过渡金属元素中的至少一种元素的锂/镍/钴/锰复合氧化物粉末） Co，Mn和Ni，0.9 <= p <= 1.1,0.2 <= x <= 0.5,0.2 <= y <= 0.5,0.1 <= z <= 0.4,0 <= q <= 0.05,1.9 <= 2 -a <= 2.1，p + x + y + z + q = 2，0 <= a <= 0.02），其特征在于，当粉末分为平均粒度为2的小颗粒尺寸分类颗粒 mum <= D50 <=8μm，平均粒径为10μm

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