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    • 36. 发明申请
    • Process for production of hydroxybenzoic acids
    • 羟基苯甲酸的制备方法
    • US20060183939A1
    • 2006-08-17
    • US10547763
    • 2004-03-02
    • Ryuzo UenoMasaya KitayamaRyoichi OtsukaTakeshi Shirai
    • Ryuzo UenoMasaya KitayamaRyoichi OtsukaTakeshi Shirai
    • C07C51/15
    • C07C51/15C07C65/03
    • The present invention provides A method for producing a hydroxybenzoic acid compound comprising, preparing an alkali metal salt of a phenol compound from the phenol compound, and reacting the alkali metal salt of the phenol compound with carbon dioxide, wherein the step of preparing the alkali metal salt of the phenol compound from the phenol compound comprises the steps of: a) reacting an alkali metal alkoxide with an excess amount of the phenol compound, which is in excess of the alkali metal alkoxide, to give the alkali metal salt of the phenol compound, and b) distilling away the generated alcohol from the reaction simultaneously with carrying out step a). The method of the present invention makes it possible to produce hydroxybenzoic acid compound in high yield without using aprotic polar organic solvent.
    • 本发明提供一种羟基苯甲酸化合物的制造方法,其特征在于,含有由酚化合物制备酚化合物的碱金属盐,使酚化合物的碱金属盐与二氧化碳反应,其中,制备碱金属 酚酚化合物的盐包括以下步骤:a)使碱金属醇盐与过量碱金属醇盐的过量的酚化合物反应,得到酚化合物的碱金属盐 ,和b)在进行步骤a)的同时蒸馏生成的醇与反应物。 本发明的方法使得可以在不使用非质子极性有机溶剂的情况下高产率生产羟基苯甲酸化合物。