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31. 发明授权

US5030618A Alkyl-substituted tetra- or hexahydrobenzopyran derivatives, organoleptic uses thereof and process for preparing same 失效
标题翻译：烷基取代的四或六氢苯并吡喃衍生物，其感官用途及其制备方法
公开(公告)号：US5030618A
公开(公告)日：1991-07-09
申请号：US545625
申请日：1990-06-29
申请人： Mark A. Sprecker , Robert P. Belko , Marie R. Hanna , Charles E. J. Beck , Salvatore M. Brucato
发明人： Mark A. Sprecker , Robert P. Belko , Marie R. Hanna , Charles E. J. Beck , Salvatore M. Brucato
IPC分类号： C07D311/74 , C07D311/94 , C11B9/00 , C11D3/50
CPC分类号： C11D3/50 , C07D311/74 , C07D311/94 , C11B9/008
摘要： Described are alkyl-substituted tetra- or hexahydrobenzopyran derivatives defined according to one of the generic structures: ##STR1## wherein Z is a moiety in the alternative either ##STR2## wherein in the moiety having the structure: ##STR3## R' is methyl or ethyl and in the moiety having the structure: ##STR4## one of the dashed lines is a carbon-carbon double bond and each of the other of the dashed lines represent carbon-carbon single bonds; wherein R.sub.1 and R.sub.2 taken separately represent hydrogen or C.sub.1 -C.sub.3 lower alkyl (with the proviso that R.sub.1 and R.sub.2 are not both hydrogen) or R.sub.1 and R.sub.2 taken together complete a C.sub.5 or C.sub.6 cycloalkyl moiety; and uses thereof in augmenting or enhancing the aroma of perfume compositions, colognes and perfumed articles including but not limited to solid or liquid anionic, cationic, nonionic or zwitterionic detergents, fabric softener compositions, fabric softener articles, hair preparations, cosmetic powders and perfumed polymers. Also described are synthesis processes for preparing such alkyl-substituted tetra- or hexahydrobenzopyran derivatives by means of reacting isopulegol or an isomer thereof with an acetal or ketal.
摘要翻译：描述了根据以下通用结构之一定义的烷基取代的四或六氢苯并吡喃衍生物：其中Z是可选择的部分或其中的“IMAGE”或“IMAGE”，其中在具有以下结构的部分中： R'是甲基或乙基，并且在具有以下结构的部分中：虚线之一是碳 - 碳双键，虚线中的每一个代表碳 - 碳单键; 其中R1和R2分别代表氢或C1-C3低级烷基（前提是R1和R2不同时为氢）或R1和R2一起形成C5或C6环烷基部分; 包括但不限于固体或液体阴离子，阳离子，非离子或两性离子洗涤剂，织物柔软剂组合物，织物柔软剂制品，毛发制品，化妆粉和加香聚合物的香料组合物，古龙水和香料制品的香气。。还描述了通过异丙醇或其异构体与缩醛或缩酮反应制备这种烷基取代的四或六氢苯并吡喃衍生物的合成方法。

32. 发明授权

US4902840A Substituted tetrahydroindane derivatives and organoleptic uses of substituted tetrahydroindanes 失效
标题翻译：取代的四氢茚满衍生物和取代的四氢茚满的感官用途
公开(公告)号：US4902840A
公开(公告)日：1990-02-20
申请号：US345014
申请日：1989-04-28
申请人： Mark A. Sprecker , Robert P. Belko , Charles E. J. Beck
发明人： Mark A. Sprecker , Robert P. Belko , Charles E. J. Beck
IPC分类号： C07D303/04 , A61K8/00 , A61K8/37 , A61K8/49 , A61Q13/00 , C07C17/16 , C07C23/34 , C07C51/38 , C07C57/26 , C07C67/08 , C07C67/10 , C07C69/02 , C07C69/58 , C07C69/593 , C07C69/608 , C07D301/14 , C11B9/00
CPC分类号： C07C23/34 , C11B9/0049 , C07C2102/24
摘要： Described are substituted tetrahydroindanes defined according to the generic structure: ##STR1## wherein Z is a moiety selected from the group consisting of: ##STR2## wherein X represents chloro or bromo; wherein R.sub.1 represents:--OR.sub.3 or --O.sup..sym. M.sup..crclbar. ;wherein R.sub.3 represents hydrogen, methyl or ethyl; wherein M represents alkali metal, sodium potassium or lithium; wherein R.sub.2 represents hydrogen or the moiety: ##STR3## as well as uses of substituted tetrahydroindanes defined according to the structure: ##STR4## wherein Z' represents a moiety selected from the group consisting of: ##STR5## wherein R.sub.2 is hydrogen and wherein R.sub.1 is the moiety:OR.sub.3 'wherein R.sub.3 ' is methyl or ethyl in augmenting or enhancing the aroma of perfume compositions, colognes and perfumed articles including but not limited to perfumed polymers, solid or liquid anionic, cationic, nonionic or zwitterionic detergents, fabric softener compositions, fabric softener articles, hair preparations and cosmetic powders.

33. 发明授权

US4756840A Beta-alkylidene phenethyl alcohols, organoleptic uses thereof and processes for preparing same 失效
标题翻译： β-亚烷基苯乙醇，其感官用途及其制备方法
公开(公告)号：US4756840A
公开(公告)日：1988-07-12
申请号：US92756
申请日：1987-09-03
申请人： Mark A. Sprecker , Robert P. Belko
发明人： Mark A. Sprecker , Robert P. Belko
IPC分类号： C11B9/00 , A61K7/46
CPC分类号： C11B9/0061
摘要： Described is the novel compound genus, the beta-alkylidene phenethyl alcohols of our invention, defined according to the generic structure: ##STR1## (wherein R.sub.1 represents hydrogen or methyl, useful in augmenting or enhancing the aroma of consumable materials including perfumes, colognes and perfumed articles including solid or liquid anionic, cationic, nonionic or zwitterionic detergents, fabric softener articles, fabric softener compositions, cosmetic powders and hair preparations).
摘要翻译：描述了本发明的新型化合物，根据通用结构定义的本发明的β-亚烷基苯乙醇：其中R1表示氢或甲基，可用于增强或增强消耗材料的香气，包括香料，古龙水和包括固体或液体阴离子，阳离子，非离子或两性离子洗涤剂，织物柔软剂制品，织物柔软剂组合物，化妆粉和头发制剂的加香制品）。

34. 发明授权

US4614831A Process for preparing alkyl substituted para-carboalkoxy cyclohexanones 失效
标题翻译：制备烷基取代的对 - 烷氧基环己酮的方法
公开(公告)号：US4614831A
公开(公告)日：1986-09-30
申请号：US771820
申请日：1985-09-03
申请人： Mark A. Sprecker , Wilhelmus J. Wiegers , Robert P. Belko , Richard M. Boden
发明人： Mark A. Sprecker , Wilhelmus J. Wiegers , Robert P. Belko , Richard M. Boden
IPC分类号： C08K5/101 , C11B9/00 , C11D3/50 , C07C67/30 , C07C67/303 , C07C69/757
CPC分类号： C08K5/101 , C11B9/0034 , C11D3/50
摘要： Described are para-carboalkoxy cyclohexanones defined according to the structure: ##STR1## wherein R.sub.1 represents hydrogen or C.sub.1 -C.sub.7 alkyl and R.sub.2 represents methyl or ethyl and uses thereof in augmenting or enhancing the aroma of consumable materials including foodstuffs, chewing gums, toothpastes, medicinal products, chewing tobaccos, perfume compositions, colognes and perfumed articles (e.g., solid or liquid anionic, cationic, nonionic or zwitterionic detergents, cosmetic compositions, fabric softener compositions, fabric softener articles, hair preparations and perfumed polymers. The compounds defined according to the structure: ##STR2## wherein R.sub.1 ' represents C.sub.4 -C.sub.7 alkyl and R.sub.2 represents methyl or ethyl are novel compounds.
摘要翻译：描述了根据以下结构定义的对 - 烷氧基环己酮：其中R 1表示氢或C 1 -C 7烷基，R 2表示甲基或乙基，并且其用于增强或增强消耗材料的香气，包括食品，口香糖，牙膏，药用产品，咀嚼烟草，香水组合物，古龙水和香料制品（例如固体或液体阴离子，阳离子，非离子或两性离子洗涤剂，化妆品组合物，织物柔软剂组合物，织物柔软剂制品，毛发制剂和加香聚合物。结构：其中R 1'表示C 4 -C 7烷基，R 2表示甲基或乙基是新化合物。

35. 发明授权

US4448984A Mono-oxomethyl substituted polyhydrodimethanonaphthalene derivatives 失效
公开(公告)号：US4448984A
公开(公告)日：1984-05-15
申请号：US458890
申请日：1983-01-18
申请人： Mark A. Sprecker , Marie R. Hanna , Richard J. Tokarzewski , Robert P. Belko , Hugh Watkins , Manfred H. Vock
发明人： Mark A. Sprecker , Marie R. Hanna , Richard J. Tokarzewski , Robert P. Belko , Hugh Watkins , Manfred H. Vock
IPC分类号： A24B15/34 , C07C47/347 , C07C47/445 , C07C43/162 , C07C35/28 , C07C67/035 , C07C67/04
CPC分类号： A24B15/345 , C07C47/347 , C07C47/445
摘要： Described are mono-oxomethyl substituted polyhydrodimethanonaphthalene derivatives having the generic structure: ##STR1## wherein the dashed line represents a carbon-carbon single bond or a carbon-carbon double bond; wherein R.sub.1, R.sub.1 ', R.sub.1 ", R.sub.1 '", R.sub.1 "", R.sub.3, R.sub.5, R.sub.5 ', R.sub.5 ", R.sub.5 '", R.sub.5 "" and R.sub.6 represent hydrogen or methyl with the provisos:(i) at least four of R.sub.1, R.sub.1 ', R.sub.1 ", R.sub.1 '" and R.sub.1 "" are hydrogen; and (ii) at least four of R.sub.5, R.sub.5 ', R.sub.5 ", R.sub.5 '" and R.sub.5 "" represent hydrogen;and wherein Z represents one of the moieties:(i) carboxaldehyde having the structure: ##STR2## (ii) alkylene dioxy or dialkoxy methyl having the structure: ##STR3## (iii) hydroxy methyl having the structure: ##STR4## (iv) acetoxymethyl having the structure: ##STR5## and wherein R.sub.7 and R.sub.8 taken separately represent C.sub.1 -C.sub.4 lower alkyl or R.sub.7 and R.sub.8 taken together represent C.sub.2 -C.sub.4 alkylene; wherein the line represented by:[++++] is either (i) a carbon-carbon single bond when R.sub.7 and R.sub.8 taken together are C.sub.2 -C.sub.4 alkylene or (ii) no bond at all when R.sub.7 and R.sub.8 taken separately represent C.sub.1 -C.sub.4 lower alkyl. Also described are processes for preparing such mono-oxomethyl substituted polyhydrodimethanonaphthalene derivatives, and processes for using the above defined mono-oxomethyl substituted polyhydrodimethanonaphthalene derivatives for their organoleptic properties and compositions containing said mono-oxomethyl substituted polyhydrodimethanonaphthalene derivatives including perfumes, perfumed articles (such as solid or liquid anionic, cationic, nonionic or zwitterionic detergents, perfumed polymers, fabric softeners and cosmetic powders), foodstuffs, chewing gums, toothpastes, medicinal products, chewing tobaccos, smoking tobaccos and smoking tobacco articles.

36. 发明授权

US4391284A Use in modifying smoking tobacco aroma and flavor or mono-oxomethyl substituted polyhydrodimethanonaphthalene derivatives 失效
标题翻译：用于改变吸烟烟草香气和风味或单氧甲基取代的多羟基甲基萘衍生物
公开(公告)号：US4391284A
公开(公告)日：1983-07-05
申请号：US354387
申请日：1982-03-02
申请人： Mark A. Sprecker , Marie R. Hanna , Richard J. Tokarzewski , Robert P. Belko , Hugh Watkins , Manfred H. Vock
发明人： Mark A. Sprecker , Marie R. Hanna , Richard J. Tokarzewski , Robert P. Belko , Hugh Watkins , Manfred H. Vock
IPC分类号： A24B15/34 , C07C47/347 , C07C47/445 , A24B3/12 , A24B15/30
CPC分类号： A24B15/345 , C07C47/347 , C07C47/445
摘要： Described is the use in modifying, augmenting or enhancing the aroma or taste of smoking tobacco products of mono-oxomethyl substituted polyhydrodimethanonaphthalene derivatives having the generic structure: ##STR1## wherein the dashed line represents a carbon-carbon single bond or a carbon-carbon double bond; wherein R.sub.1, R.sub.1 ', R.sub.1 ", R.sub.1 '", R.sub.1 "", R.sub.3, R.sub.5, R.sub.5 ', R.sub.5 ", R.sub.5 '", R.sub.5 "" and R.sub.6 represent hydrogen or methyl with the provisos:(i) at least four of R.sub.1, R.sub.1 ', R.sub.1 ", R.sub.1 '" and R.sub.1 "" are hydrogen; and (ii) at least four of R.sub.5, R.sub.5 ', R.sub.5 ", R.sub.5 '" and R.sub.5 "" represent hydrogen;and wherein Z represents one of the moieties:(i) carboxaldehyde having the structure: ##STR2## (ii) alkylene dioxy or dialkoxy methyl having the structure: ##STR3## (iii) hydroxy methyl having the structure: ##STR4## (iv) acetoxymethyl having the structure: ##STR5## and wherein R.sub.7 and R.sub.8 taken separately represent C.sub.1 -C.sub.4 lower alkyl or R.sub.7 and R.sub.8 taken together represent C.sub.2 -C.sub.4 alkylene; wherein the line represented by:[++++]is either (i) a carbon-carbon single bond when R.sub.7 and R.sub.8 taken together are C.sub.2 -C.sub.4 alkylene or (ii) no bond at all when R.sub.7 and R.sub.8 taken separately represent C.sub.1 -C.sub.4 lower alkyl.
摘要翻译：描述了用于改变，增强或增强具有以下通用结构的单氧代甲基取代的多羟基甲基萘衍生物的烟草产品的香气或味道：其中虚线表示碳 - 碳单键或碳 - 碳双键; 其中R1，R1'，R1“，R1”，R1“，R3，R5，R5'，R5”，R5“，R5”和R6表示氢或甲基，条件：（i）R1，R1'，R1“，R1”和R1“”中的至少四个为氢; 和（ii）R5，R5'，R5“，R5”和R5“中的至少四个表示氢; （ⅰ）具有以下结构的甲醛：（ⅱ）具有以下结构的亚烷基二氧基或二烷氧基甲基：（ⅲ）具有以下结构的羟基甲基：（ⅳ）具有以下结构的乙酰氧基甲基：其中R7和R8分别代表C1-C4低级烷基或R7和R8一起代表C2-C4亚烷基; 其中由以下各项表示的线：[++++]是（i）当R 7和R 8一起为C 2 -C 4亚烷基时的碳 - 碳单键或（ii）当R7和R8分别表示C1 -C4低级烷基。

37. 发明授权

US5378685A Process for preparing mixture of trimethyl and dimethylmethylene propyl polyhydropyrans, products produced thereby perfumery uses of such product 失效
标题翻译：制备三甲基和二甲基亚甲基丙基多羟基吡喃的混合物的方法，由此产生的产品由此产生香料的用途
公开(公告)号：US5378685A
公开(公告)日：1995-01-03
申请号：US214185
申请日：1994-03-17
申请人： Mark A. Sprecker , Robert P. Belko , Marie R. Hanna
发明人： Mark A. Sprecker , Robert P. Belko , Marie R. Hanna
IPC分类号： C07D309/04 , C07D309/12 , C11B9/00 , A61K7/46
CPC分类号： C07D309/12 , C07D309/04 , C11B9/008
摘要： Described is a process for preparing trimethyl and dimethylmethylene propyl polyhydropyran derivatives including compounds defined according to the structure: ##STR1## which defines a mixture wherein in the mixture, in each of the compounds one of the dashed lines is a carbon-carbon double bond and each of the other of the dashed lines represents a carbon-carbon single bond as well as the compound having the structure: ##STR2## products produced thereby; perfumery uses of such products; process intermediates of such process including compounds defined according to the structures: ##STR3## wherein X represents chloro or bromo.
摘要翻译：描述了一种制备三甲基和二甲基亚甲基丙基多氢吡喃衍生物的方法，其包括根据以下结构定义的化合物：其定义为混合物，其中在每种化合物中，虚线中的一个为碳 - 碳双键，虚线中的每一个代表碳 - 碳单键，以及具有以下结构的化合物：由此产生的产物; 这种产品的香水用途; 该方法的加工中间体包括根据以下结构定义的化合物：其中X表示氯或溴。

38. 发明授权

US4933488A Triisobutylene alcohols and esters, uses thereof in perfumery and halogenated intermediates useful for preparing same 失效
标题翻译：三异丁烯醇和酯，其用于可用于制备它的香料和卤代中间体中
公开(公告)号：US4933488A
公开(公告)日：1990-06-12
申请号：US456744
申请日：1989-12-26
申请人： Mark A. Sprecker , Robert P. Belko , Marie R. Hanna
发明人： Mark A. Sprecker , Robert P. Belko , Marie R. Hanna
IPC分类号： C07C33/025 , C11B9/00 , C11D3/50
CPC分类号： C11D3/50 , C07C33/025 , C07C67/11 , C11B9/0015
摘要： Described are triisobutylene alcohols and esters and halogenated intermediates for preparing same defined according to the generic structure: ##STR1## wherein one of the dashed lines represents a carbon-carbon single bond and the other of the dashed lines represents a carbon-carbon double bond; wherein R.sub.1 " and R.sub.2 " are the same or different and each represents hydrogen, chloro, bromo, hydroxyl or a C.sub.1 -C.sub.3 acyloxy with the provisos that when the dashed line in the 4--4' position is a carbon-carbon double bond then R.sub.1 " is hydrogen and R.sub.2 " is not hydrogen; and R.sub.1 " and R.sub.2 " are not both hydrogen.Also described are the uses of the triisobutylene alcohols and esters in augmenting or enhancing the aroma of perfume compositions, colognes and perfumed articles including but not limited to perfumed polymers solid or liquid anionic, cationic, nonionic or zwitterionic detergents, fabric softener compositions, fabric softener articles, cosmetic powders and hair preparations.
摘要翻译：描述了根据一般结构定义的三异丁烯醇和酯和卤代中间体，其中虚线中的一个代表碳 - 碳单键，虚线中的另一个代表碳 - 碳双键; 其中R 1“和R 2”相同或不同，各自表示氢，氯，溴，羟基或C 1 -C 3酰氧基，条件是当4-4'位的虚线是碳 - 碳双键，则R1“是氢，R2”不是氢; 并且R1“和R2”不都是氢。还描述了三异丁烯醇和酯在增强或增强香料组合物，古龙水和加香制品的香气中的用途，包括但不限于：固体或液体阴离子，阳离子，非离子或两性离子洗涤剂，织物柔软剂组合物，织物柔软剂制品，化妆粉和头发制剂。

39. 发明授权

US4933321A Triisobutylene alcohols and esters, uses thereof in perfumery and halogenated intermediates useful for preparing same 失效
标题翻译：三异丁烯醇和酯，其用于可用于制备它的香料和卤代中间体中
公开(公告)号：US4933321A
公开(公告)日：1990-06-12
申请号：US457174
申请日：1989-12-26
申请人： Mark A. Sprecker , Robert P. Belko , Marie R. Hanna
发明人： Mark A. Sprecker , Robert P. Belko , Marie R. Hanna
IPC分类号： C07C33/025 , C11B9/00 , C11D3/50
CPC分类号： C07C33/025 , C07C67/11 , C11B9/0015 , C11D3/50
摘要： Described are triisobutylene alcohols and esters and halogenated intermediates for preparing same defined according to the generic structure: ##STR1## wherein one of the dashed lines represents a carbon-carbon single bond and the other of the dashed lines represents a carbon-carbon double bond; wherein R.sub.1 " and R.sub.2 " are the same or different and each represents hydrogen, chloro, bromo, hydroxyl or a C.sub.1 -C.sub.3 acyloxy with the provisos that when the dashed line in the 4-4' position is a carbon-carbon double bond then R.sub.1 " is hydrogen and R.sub.2 " is not hydrogen; and R.sub.1 " and R.sub.2 " are not both hydrogen.Also described are the uses of the triisobutylene alcohols and esters in augmenting or enhancing the aroma of perfume composition, colognes and perfumed articles including but not limited to perfumed polymers solid or liquid anionic, cationic, nonionic or switterionic detergents, fabric softener compositions, fabric softener articles, cosmetic powders and hair preparations.
摘要翻译：描述了根据一般结构定义的三异丁烯醇和酯和卤代中间体，其中虚线中的一个代表碳 - 碳单键，虚线中的另一个代表碳 - 碳双键; 其中R 1“和R 2”相同或不同，各自表示氢，氯，溴，羟基或C 1 -C 3酰氧基，条件是当4-4'位的虚线是碳 - 碳双键，则R1“是氢，R2”不是氢; 并且R1“和R2”不都是氢。还描述了三异丁烯醇和酯在增强或增强香料组合物，古龙水和加香制品的香气中的用途，包括但不限于：固体或液体阴离子，阳离子，非离子或转换洗涤剂，织物柔软剂组合物，织物柔软剂制品，化妆粉和头发制剂。

40. 发明授权

US4933319A Substituted tetrahydroindane derivatives and organoleptic uses of substituted tetrahydroindanes 失效
标题翻译：取代的四氢茚满衍生物和取代的四氢茚满的感官用途
公开(公告)号：US4933319A
公开(公告)日：1990-06-12
申请号：US424718
申请日：1989-10-20
申请人： Mark A. Sprecker , Robert P. Belko , Charles E. J. Beck
发明人： Mark A. Sprecker , Robert P. Belko , Charles E. J. Beck
IPC分类号： C07C23/34 , C11B9/00
CPC分类号： C07C23/34 , C11B9/0049 , C07C2102/24
摘要： Described are substituted tetrahydroindanes defined according to the generic structure: ##STR1## wherein Z is a moiety selected from the group consisting of: ##STR2## wherein X represents chloro or bromo; wherein R.sub.1 represents:--OR.sub.3 or --O.sup..crclbar. M.sup..sym. ;wherein R.sub.3 represents hydrogen, methyl or ethyl; wherein M represents alkali metal, sodium potassium or lithium; wherein R.sub.2 represents hydrogen or the moiety: ##STR3## as well as uses of substituted tetrahydroindanes defined according to the structure: ##STR4## wherein Z' represents a moiety selected from the group consisting of: ##STR5## wherein R.sub.2 is hydrogen and wherein R.sub.1 is the moiety:--OR.sub.3 'wherein R.sub.3 ' is methyl or ethyl in augmenting or enhancing the aroma of perfume compositions, colognes and perfumed articles including but not limited to perfumed polymers, solid or liquid anionic, cationic, nonionic or zwitterionic detergents, fabric softener compositions, fabric softener articles, hair preparations and cosmetic powders.
摘要翻译：描述的是根据以下通用结构定义的取代的四氢茚基：其中Z是选自下列的部分：其中X代表氯或溴; 其中R1表示：-OR3或-O（ - ）M（+）; 其中R 3表示氢，甲基或乙基; 其中M表示碱金属，钠或钾; 其中R 2表示氢或其部分：以及根据以下结构定义的取代的四氢茚基的用途：其中Z'表示选自以下的部分：其中R 2为氢，并且其中R 1是部分：-OR 3'，其中R 3'是甲基或乙基，以增强或增强香料组合物，古龙水和香料制品的香气，包括但不限于加香聚合物，固体或液体阴离子，阳离子，非离子或两性离子洗涤剂，织物柔软剂组合物，织物柔软剂制品，头发制剂和化妆粉末。

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