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31. 发明授权

US07407928B2 Solid phase benzopyran composition, process for preparing same and organoleptic uses thereof 有权
标题翻译：固相苯并吡喃组合物，其制备方法及其感官用途
公开(公告)号：US07407928B2
公开(公告)日：2008-08-05
申请号：US10361748
申请日：2003-02-10
申请人： Mark A. Sprecker , Robert P. Belko , Bruce Mechanic
发明人： Mark A. Sprecker , Robert P. Belko , Bruce Mechanic
IPC分类号： A61K8/18 , C07C15/00
CPC分类号： A61K8/498 , A61Q13/00
摘要： Described is a solid phase benzopyran composition comprising predominately 1,3,4,6,7,8-hexahydro-4,6,6,7,8,8-hexamethylcyclopenta[G]-2-benzopyran and at least one other benzopyran compound. The novel compositions are used in augmenting, enhancing and/or imparting aromas in to consumable materials such as perfume compositions, perfumed articles including soaps, detergents, fabric softener compositions, fabric softener articles, fragranced candles, cosmetics, hair preparations, perfumed polymers and colognes. Also described is a process for producing the solid phase benzopyran compositions.
摘要翻译：描述了主要的苯并吡喃组合物，其主要包含1,3,4,6,7,8-六氢-4,6,6,7,8,8-六甲基环戊并[G] -2-苯并吡喃和至少一种其它苯并吡喃化合物。新型组合物用于增强，增强和/或赋予消耗材料如香料组合物，香料制品，包括肥皂，洗涤剂，织物柔软剂组合物，织物柔软剂制品，芳香蜡烛，化妆品，毛发制品，加香聚合物和古龙香。还描述了制备固相苯并吡喃组合物的方法。

32. 发明授权

US07115553B2 Acetonide fragrance compound 有权
标题翻译：丙酮酸香精化合物
公开(公告)号：US07115553B2
公开(公告)日：2006-10-03
申请号：US10618363
申请日：2003-07-10
申请人： Michael G. Monteleone , Robert P. Belko , Manfred Pawlak , Catherine Marie Smith , Mark A. Sprecker
发明人： Michael G. Monteleone , Robert P. Belko , Manfred Pawlak , Catherine Marie Smith , Mark A. Sprecker
IPC分类号： C11B9/00
CPC分类号： C07D317/70 , C11C5/002 , C11D3/50
摘要： A novel compound 4H-indeno[4,5-D]-1,3-dioxole, 3A,5,6,7,8,8B-hexahydro-2,2,6,6,7,8,8-heptamethyl is dislosed as well as the use of the compound as a fragrance chemical. The fragrance compound is suitable for use in creating fragrances, and scents in items such as perfumes, colognes and personal care products.
摘要翻译：新化合物4H-茚并[4,5-D] -1,3-二氧杂环戊烯，3A，5,6,7,8,8-六氢-2,2,6,6,7,8,8-七甲基是松香以及化合物作为香料的使用。芳香化合物适用于制造香料，香料，香水，古龙水和个人护理用品等。

33. 发明授权

US06362141B1 Indanyl derivatives 有权
标题翻译：茚基衍生物
公开(公告)号：US06362141B1
公开(公告)日：2002-03-26
申请号：US09948511
申请日：2001-09-06
申请人： Mark A. Sprecker , Richard A. Weiss , Robert P. Belko , Ellen Ann Molner
发明人： Mark A. Sprecker , Richard A. Weiss , Robert P. Belko , Ellen Ann Molner
IPC分类号： C11D320
CPC分类号： C07C47/235 , C07C43/168 , C07C2602/08 , C07D317/12 , C11B9/0049 , C11B9/0076
摘要： The present invention is directed to indanyl derivatives and the use of the indanyl derivatives in creating fragrances, and scents in items such as perfumes, colognes and personal care products.
摘要翻译：本发明涉及茚满基衍生物和茚满基衍生物在制备香料中的用途，以及香料，古龙水和个人护理产品中的香料。

34. 发明授权

US4999439A Alkyl-substituted tetra- or hexahydrobenzopyran derivatives, organoleptic uses thereof and process for preparing same 失效
标题翻译：烷基取代的四或六氢苯并吡喃衍生物，其感官用途及其制备方法
公开(公告)号：US4999439A
公开(公告)日：1991-03-12
申请号：US497693
申请日：1990-03-22
申请人： Mark A. Sprecker , Robert P. Belko , Marie R. Hanna , Charles E. J. Beck , Salvatore M. Brucato
发明人： Mark A. Sprecker , Robert P. Belko , Marie R. Hanna , Charles E. J. Beck , Salvatore M. Brucato
IPC分类号： C07D311/74 , C07D311/94 , C11B9/00 , C11D3/50
CPC分类号： C07D311/94 , C07D311/74 , C11B9/008 , C11D3/50
摘要： Described are alkyl-substituted tetra- or hexahydrobenzopyran derivatives defined according to one of the generic structures: ##STR1## wherein Z is a moiety in the alternative either ##STR2## wherein in the moiety having the structure: ##STR3## R' is methyl or ethyl and in the moiety having the structure: ##STR4## one of the dashed lines is a carbon-carbon double bond and each of the other of the dashed lines represent carbon-carbon single bonds; wherein R.sub.1 and R.sub.2 taken separately represent hydrogen or C.sub.1 -C.sub.3 lower alkyl (with the proviso that R.sub.1 and R.sub.2 are not both hydrogen) or R.sub.1 and R.sub.2 taken together complete a C.sub.5 or C.sub.6 cycloalkyl moiety; and uses thereof in augmenting or enhancing the aroma of perfume compositions, colognes and perfumed articles including but not limited to solid or liquid anionic, cationic, nonionic or zwitterionic detergents, fabric softener compositions, fabric softener articles, hair preparations, cosmetic powders and perfumed polymers. Also described are synthesis processes for preparing such alkyl-substituted tetra- or hexahydrobenzopyran derivatives by means of reacting isopulegol or an isomer thereof with an acetal or ketal.
摘要翻译：描述了根据以下通用结构之一定义的烷基取代的四或六氢苯并吡喃衍生物：其中Z是可选择的部分或其中的“IMAGE”或“IMAGE”，其中在具有以下结构的部分中： R'是甲基或乙基，并且在具有以下结构的部分中：虚线之一是碳 - 碳双键，虚线中的每一个代表碳 - 碳单键; 其中R1和R2分别代表氢或C1-C3低级烷基（条件是R1和R2不同时为氢）或R1和R2一起形成C5或C6环烷基部分; 包括但不限于固体或液体阴离子，阳离子，非离子或两性离子洗涤剂，织物柔软剂组合物，织物柔软剂制品，毛发制品，化妆粉和加香聚合物的香料组合物，古龙水和香料制品的香气。。还描述了通过异丙醇或其异构体与缩醛或缩酮反应制备这种烷基取代的四或六氢苯并吡喃衍生物的合成方法。

35. 发明授权

US4962090A 2,4-disubstituted and 2,2,4-trisubstituted tetrahydropyranyl-4-ethers, process for preparing same and perfumery uses thereof 失效
标题翻译： 2,4-二取代和2,2,4-三取代的四氢吡喃基-4-醚，其制备方法和香料用途
公开(公告)号：US4962090A
公开(公告)日：1990-10-09
申请号：US497593
申请日：1990-03-22
申请人： Mark A. Sprecker , Robert P. Belko , Salvatore M. Brucato , Charles E. J. Beck , Marie R. Hanna
发明人： Mark A. Sprecker , Robert P. Belko , Salvatore M. Brucato , Charles E. J. Beck , Marie R. Hanna
IPC分类号： C07D309/10 , C07D311/96 , C11B9/00
CPC分类号： C07D311/96 , C07D309/10 , C11B9/008
摘要： Described are 2,4-disubstituted and 2,2,4-trisubstituted tetrahydropyranyl-4-ethers defined according to the generic structure: ##STR1## wherein R' represents methyl or ethyl; R.sub.1 and R.sub.2 taken alone are the same or different hydrogen, phenyl, C.sub.1 -C.sub.8 alkyl or C.sub.2 -C.sub.8 alkenyl (with the proviso that R.sub.1 and R.sub.2 are not both hydrogen) and R.sub.1 and R.sub.2 taken together represent C.sub.5 -C.sub.12 cycloalkyl or alkyl cycloalkyl, and reaction products containing said 2,4-disubstituted and 2,2,4-trisubstituted tetrahydropyranyl-4-ethers taken alone or taken further together in admixture with compounds defined according to the generic structure: ##STR2## wherein in the compounds defined according to the structure: ##STR3## one of the dashed lines in the moiety: ##STR4## represents a carbon-carbon double bond and each of the other dashed lines represent carbon-carbon single bonds; and R.sub.1 ' and R.sub.2 ' taken alone or taken together are defined in the same manner that R.sub.1 and R.sub.2 are defined, supra; and organoleptic uses thereof in augmenting or enhancing the aroma of perfume compositions, colognes and perfumed articles including but not limited to bleach compositions, solid or liquid anionic, cationic, nonionic or zwitterionic detergents, perfume polymers, fabric softener compositions, fabric softener articles, cosmetic powders and hair preparations.
摘要翻译：描述根据通用结构定义的2,4-二取代的和2,2,4-三取代的四氢吡喃基-4-醚：其中R'表示甲基或乙基; 单独使用的R1和R2是相同或不同的氢，苯基，C1-C8烷基或C2-C8烯基（前提是R1和R2不同时为氢），R1和R2一起代表C5-C12环烷基或烷基环烷基，以及含有所述2,4-二取代的和2,2,4-三取代的四氢吡喃基-4-醚的反应产物，其独立地取代或进一步进一步与根据一般结构定义的化合物混合：其中在根据结构：部分中的虚线之一：表示碳 - 碳双键，并且每个其它虚线表示碳 - 碳单键; 单独或一起取代的R 1'和R 2'以与上述定义R 1和R 2相同的方式定义; 包括但不限于漂白组合物，固体或液体阴离子型，阳离子型，非离子型或两性离子型洗涤剂，香料聚合物，织物柔软剂组合物，织物柔软剂制品，化妆品的香料，以及增强或增强香水组合物，古龙水和香料制品的香气的感官用途粉末和头发制剂。

36. 发明授权

US4924026A Triisobutylene alcohols and esters, uses thereof in perfumery and halogenated intermediates useful for preparing same 失效
标题翻译：三异丁烯醇和酯，其用于可用于制备它的香料和卤代中间体中
公开(公告)号：US4924026A
公开(公告)日：1990-05-08
申请号：US392423
申请日：1989-08-11
申请人： Mark A. Sprecker , Robert P. Belko , Marie R. Hanna
发明人： Mark A. Sprecker , Robert P. Belko , Marie R. Hanna
IPC分类号： C07C33/025 , C11B9/00 , C11D3/50
CPC分类号： C11B9/0015 , C07C33/025 , C07C67/11 , C11D3/50
摘要： Described are triisobutylene alcohols and esters and halogenated intermediates for preparing same defined according to the generic structure: ##STR1## wherein one of the dashed lines represents a carbon-carbon single bond and the other of the dashed lines represents a carbon-carbon double bond; wherein R.sub.1 " and R.sub.2 " are the same or different and each represents hydrogen, chloro, bromo, hydroxyl or a C.sub.1 -C.sub.3 acyloxy with the provisos that when the dashed line in the 4--4' position is a carbon-carbon double bond then R.sub.1 " is hydrogen and R.sub.2 " is not hydrogen, and R.sub.1 " and R.sub.2 " are not both hydrogen.Also described are the uses of the triisobutylene alcohols and esters in augmenting or enhancing the aroma of perfume compositions, colognes and perfumed articles including but not limited to perfumed polymers solid or liquid anionic, cationic, nonionic or zwitterionic detergents, fabric softener compositions, fabric softener articles, cosmetic powders and hair preparations.
摘要翻译：描述了根据一般结构定义的三异丁烯醇和酯和卤代中间体，其中虚线中的一个代表碳 - 碳单键，虚线中的另一个代表碳 - 碳双键; 其中R 1“和R 2”相同或不同，各自表示氢，氯，溴，羟基或C 1 -C 3酰氧基，条件是当4-4'位的虚线是碳 - 碳双键，则R1“是氢，R2”不是氢，R1“和R2”不是氢。还描述了三异丁烯醇和酯在增强或增强香料组合物，古龙水和加香制品的香气中的用途，包括但不限于：固体或液体阴离子，阳离子，非离子或两性离子洗涤剂，织物柔软剂组合物，织物柔软剂制品，化妆粉和头发制剂。

37. 发明授权

US4668817A Alkyl substituted para-carboalkoxy cyclohexanones 失效
标题翻译：烷基取代的对 - 烷氧基环己酮
公开(公告)号：US4668817A
公开(公告)日：1987-05-26
申请号：US842836
申请日：1986-03-21
申请人： Mark A. Sprecker , Wilhelmus J. Wiegers , Robert P. Belko , Richard M. Boden
发明人： Mark A. Sprecker , Wilhelmus J. Wiegers , Robert P. Belko , Richard M. Boden
IPC分类号： C08K5/101 , C11B9/00 , C11D3/50 , C07C69/757
CPC分类号： A61Q13/00 , A61K8/37 , C08K5/101 , C11B9/0034 , C11D3/50
摘要： Described are para-carboalkoxy cyclohexanones defined according to the structure: ##STR1## wherein R.sub.1 represents hydrogen or C.sub.1 -C.sub.7 alkyl and R.sub.2 represents methyl or ethyl and uses thereof in augmenting or enhancing the aroma of consumable materials including foodstuffs, chewing gums, toothpastes, medicinal products, chewing tobaccos, perfume compositions, colognes and perfumed articles (e.g., solid or liquid anionic, cationic, nonionic or zwitterionic detergents, cosmetic compositions, fabric softener compositions, fabric softener articles, hair preparations and perfumed polymers. The compounds defined according to the structure: ##STR2## wherein R.sub.1 ' represents C.sub.4 -C.sub.7 alkyl and R.sub.2 represents methyl or ethyl are novel compounds.
摘要翻译：描述了根据以下结构定义的对 - 烷氧基环己酮：其中R 1表示氢或C 1 -C 7烷基，R 2表示甲基或乙基，并且其用于增强或增强消耗材料的香气，包括食品，口香糖，牙膏，药用产品，咀嚼烟草，香水组合物，古龙水和香料制品（例如固体或液体阴离子，阳离子，非离子或两性离子洗涤剂，化妆品组合物，织物柔软剂组合物，织物柔软剂制品，毛发制剂和加香聚合物。结构：其中R 1'表示C 4 -C 7烷基，R 2表示甲基或乙基是新化合物。

38. 发明授权

US4548743A Ketal and use in perfumery 失效
标题翻译：金属和用于香料
公开(公告)号：US4548743A
公开(公告)日：1985-10-22
申请号：US602646
申请日：1984-04-20
申请人： Mark A. Sprecker , Robert P. Belko , William L. Schreiber , Michael Licciardello
发明人： Mark A. Sprecker , Robert P. Belko , William L. Schreiber , Michael Licciardello
IPC分类号： A61K8/00 , A61K8/35 , A61Q13/00 , C07C43/30 , C07C43/305 , C07C45/00 , C07C45/51 , C07C49/20 , C07C49/203 , C07C49/217 , C07C49/557 , C07C67/00 , C07C401/00 , C07C403/00 , C07C403/14 , C07C403/16 , C11B9/00 , A61K7/46 , C07C43/32
CPC分类号： C07C403/16 , C07C43/305 , C07C45/515 , C07C49/203 , C07C49/217 , C07C49/557 , C11B9/0015 , C11B9/0034 , C11B9/0061 , C07C2101/14 , C07C2101/16
摘要： Described is the compound having the structure ##STR1## useful in perfumery.
摘要翻译：描述了具有用于香料的结构的化合物。

39. 发明授权

US4492645A Organoleptic use of cyclohexenyl-alpha-alkyl acrolein derivatives 失效
标题翻译：感官使用环己烯基-α-烷基丙烯醛衍生物
公开(公告)号：US4492645A
公开(公告)日：1985-01-08
申请号：US505423
申请日：1983-06-16
申请人： Mark A. Sprecker , Philip T. Klemarczyk , Robert P. Belko
发明人： Mark A. Sprecker , Philip T. Klemarczyk , Robert P. Belko
IPC分类号： A24B15/34 , C07C45/74 , C07C45/82 , C07C47/225 , C11B9/00
CPC分类号： C11B9/0034 , A24B15/34 , C07C403/14 , C07C45/74 , C07C45/82 , C07C47/225 , C07C2101/16
摘要： Described are cyclohexenyl-alpha-alkyl acrolein derivatives defined according to the generic structure: ##STR1## wherein R.sub.1, R.sub.2, R.sub.3 and R.sub.4 represent hydrogen or methyl with the proviso that one, two or three of R.sub.1, R.sub.2, R.sub.3 and R.sub.4 represent methyl; wherein R.sub.5 represents methyl or ethyl; wherein one of the dashed lines represents a carbon-carbon double bond and the other of the dashed lines represents a carbon-carbon single bond; wherein the wavy lines represent the "cis" or "trans" juxtaposition of the moieties hydrogen, R.sub.5, cyclohexenyl and carboxaldehyde about the carbon-carbon double bond; or represented by the structures: ##STR2## and processes and compositions for augmenting or enhancing the flavor and/or aroma of consumable materials including foodstuffs, chewing gums, medicinal products, toothpastes, chewing tobaccos, perfumes, perfumed articles, colognes, smoking tobaccos and smoking tobacco articles using as the essential ingredient at least one of said cyclohexenyl-alpha-alkyl acrolein derivatives.
摘要翻译：描述了根据通用结构定义的环己烯基-α-烷基丙烯醛衍生物：其中R 1，R 2，R 3和R 4表示氢或甲基，条件是R 1，R 2，R 3和R 4中的一个，两个或三个表示甲基 ; 其中R 5表示甲基或乙基; 其中一条虚线表示碳 - 碳双键，另一条虚线表示碳 - 碳单键; 其中波浪线表示碳 - 碳双键周围部分氢，R5，环己烯基和甲醛的“顺式”或“反式”并置; 或由以下结构表示：＆lt; IMAGE＆gt;图像＆gt;以及用于增强或增强消费材料的风味和/或香气的方法和组合物，包括食品，口香糖，药用产品，牙膏，咀嚼烟草，香水，香料制品，古龙水，烟草烟草和烟草制品，其中使用至少一种所述环己烯基-α-烷基丙烯醛衍生物作为必需成分。

40. 发明授权

US4470963A Flavoring with mono-oxomethyl substituted polyhydrodimethanonaphthalene derivatives 失效
公开(公告)号：US4470963A
公开(公告)日：1984-09-11
申请号：US546383
申请日：1983-10-28
申请人： Mark A. Sprecker , Marie R. Hanna , Richard J. Tokarzewski , Robert P. Belko , Hugh Watkins , Manfred H. Vock
发明人： Mark A. Sprecker , Marie R. Hanna , Richard J. Tokarzewski , Robert P. Belko , Hugh Watkins , Manfred H. Vock
IPC分类号： A24B15/34 , C07C47/347 , C07C47/445 , A23L1/226 , A23L1/235
CPC分类号： C07C47/347 , A24B15/345 , C07C47/445
摘要： Described are mono-oxomethyl substituted polyhydrodimethanonaphthalene derivatives having the generic structure: ##STR1## wherein the dashed line represents a carbon-carbon single bond or a carbon-carbon double bond; wherein R.sub.1, R.sub.1 ', R.sub.1 ", R.sub.1 '", R.sub.1 "", R.sub.3, R.sub.5, R.sub.5 ', R.sub.5 ", R.sub.5 '", R.sub.5 "" and R.sub.6 represent hydrogen or methyl with the provisos:(i) at least four of R.sub.1, R.sub.1 ', R.sub.1 ", R.sub.1 '" and R.sub.1 "" are hydrogen; and (ii) at least four of R.sub.5, R.sub.5 ', R.sub.5 ", R.sub.5 '" and R.sub.5 "" represent hydrogen;and wherein Z represents one of the moieties:(i) carboxaldehyde having the structure: ##STR2## (ii) alkylene dioxy or dialkoxy methyl having the structure: ##STR3## (iii) hydroxy methyl having the structure: ##STR4## (iv) acetoxymethyl having the structure: ##STR5## and wherein R.sub.7 and R.sub.8 taken separately represent C.sub.1 -C.sub.4 lower alkyl or R.sub.7 and R.sub.8 taken together represent C.sub.2 -C.sub.4 alkylene; wherein the line represented by:[++++]is either (i) a carbon-carbon single bond when R.sub.7 and R.sub.8 taken together are C.sub.2 -C.sub.4 alkylene or (ii) no bond at all when R.sub.7 and R.sub.8 taken separately represent C.sub.1 -C.sub.4 lower alkyl. Also described are processes for preparing such mono-oxomethyl substituted polyhydrodimethanonaphthalene derivatives, and processes for using the above defined mono-oxomethyl substituted polyhydrodimethanonaphthalene derivatives for their organoleptic properties and compositions containing said mono-oxomethyl substituted polyhydrodimethanonaphthalene derivatives including perfumes, perfumed articles (such as solid or liquid anionic, cationic, nonionic or zwitterionic detergents, perfumed polymers, fabric softeners and cosmetic powders), foodstuffs, chewing gums, toothpastes, medicinal products, chewing tobaccos, smoking tobaccos and smoking tobacco articles.

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