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31. 发明授权

US06576100B2 Fluorinated ionomers 有权
标题翻译：氟化离聚物
公开(公告)号：US06576100B2
公开(公告)日：2003-06-10
申请号：US09885921
申请日：2001-06-22
申请人： Vincenzo Arcella , Alessandro Ghielmi , Marco Apostolo , Julio Abusleme
发明人： Vincenzo Arcella , Alessandro Ghielmi , Marco Apostolo , Julio Abusleme
IPC分类号： C25B1300
CPC分类号： C08J5/225 , B01D71/32 , B01D71/82 , C08F214/262 , C08J2327/16 , H01M8/1023 , H01M8/1039 , H01M8/1046 , H01M8/1072 , Y02P70/56
摘要： Crosslinked sulphonic fluorinated ionomers having an equivalent weight 380-1300 g/eq, comprising: (A) monomeric units deriving from one or more fluorinated monomers containing at least one ethylene unsaturation; (B) fluorinated monomeric units containing sulphonyl groups —SO2F in an amount such as to give the above indicated equivalent weight.
摘要翻译：具有当量重量为380-1300g / eq的交联磺化氟化离聚物，其包含：（A）衍生自一种或多种含至少一种乙烯不饱和度的氟化单体的单体单元;（B）含有磺酰基-SO 2 F的氟化单体单元，例如给出上述等效重量。

32. 发明授权

US06555639B2 Polymerization process of sulphonic monomers 有权
标题翻译：磺酸单体的聚合方法
公开(公告)号：US06555639B2
公开(公告)日：2003-04-29
申请号：US09886106
申请日：2001-06-22
申请人： Marco Apostolo , Vincenzo Arcella
发明人： Marco Apostolo , Vincenzo Arcella
IPC分类号： C08F224
CPC分类号： C08F214/184 , C08F216/1466
摘要： A polymerization process in microemulsion of: (I) one or more fluorinated monomers containing at least one ethylene unsaturation; (II) one or more fluorinated monomers containing sulphonyl groups —SO2F; said process comprising: a) preparation of an aqueous microemulsion, having a pH in the range 4-7, of perfluoropolyethers (PFPEs); b) feeding of the microemulsion to the polymerization reactor, in an amount higher than 18 ml per liter of reaction medium; c) introduction of the monomer (II) in liquid form into the reactor, reactor pressurization with the gaseous monomers (I); d) addition of the initiator, and feeding of the monomers (I) during the polymerization so as to maintain constant the reactor pressure.
摘要翻译：微乳液中的聚合方法：（I）含有至少一个乙烯不饱和度的一种或多种氟化单体;（II）含有磺酰基-SO 2 F的一种或多种含氟单体; 所述方法包括：a）制备全氟聚醚（PFPE）具有4-7范围内pH值的水性微乳液; b）将微乳液以高于18ml /升反应的量加入到聚合反应器中介质; c）将液体形式的单体（II）引入反应器，用气体单体（I）进行反应器加压; d）加入引发剂和在聚合过程中进料单体（I）以保持恒定反应堆压力。

33. 发明授权

US06395834B1 Fluoroelastomer compositions 有权
公开(公告)号：US06395834B1
公开(公告)日：2002-05-28
申请号：US09511949
申请日：2000-02-23
申请人： Margherita Albano , Marco Apostolo , Vincenzo Arcella , Enrico Marchese
发明人： Margherita Albano , Marco Apostolo , Vincenzo Arcella , Enrico Marchese
IPC分类号： C08L2718
CPC分类号： C08L27/12 , C08L27/18 , C08L29/10 , C08L2205/02 , C08L2666/04
摘要： Fluoropolymers comprising a fluoroelastomer matrix incorporating therein particles of a semicrystalline fluoropolymer formed of tetrafluoroethylene (TFE) homopolymers or copolymers, wherein the average particle sizes of the semicrystalline fluoropolymer latex range from 10 to 100 nm.

34. 发明申请

US20130197163A1 Fluoroelastomers 审中-公开
标题翻译：氟弹性体
公开(公告)号：US20130197163A1
公开(公告)日：2013-08-01
申请号：US13877822
申请日：2011-10-07
申请人： Marco Apostolo , Liubov Chernysheva
发明人： Marco Apostolo , Liubov Chernysheva
IPC分类号： C08F214/28
摘要： The invention pertains to peroxide-curable fluoroelastomers for the oil and gas industry, including explosive decompression, and which can be easily processed to yield cured parts in standard machineries at reasonable throughput rates, said fluoroelastomers comprising: recurring units derived from vinylidene fluoride (VDF); recurring units derived from hexafluoropropylene (HFP); recurring units derived from at least one bis-olefin [bis-olefin (OF)] having general formula: wherein R1, R2, R3, R4, R5 and R6, equal or different from each other, are H, a halogen, or a C1-C5 optionally halogenated group, possibly comprising one or more oxygen group; Z is a linear or branched C1-C18 optionally halogenated alkylene or cycloalkylene radical, optionally containing oxygen atoms, or a (per)fluoropolyoxyalkylene radical; and iodine or bromine cure-sites; said fluoroelastomers further possessing a Mooney viscosity (ML) of at least 85 MU (1+10@121° C.), when measured according to ASTM D1646.
摘要翻译：本发明涉及用于石油和天然气工业的过氧化物可固化的含氟弹性体，包括爆炸减压，并且其可以容易地加工以在合理的产率下在标准机械中产生固化部分，所述含氟弹性体包含：衍生自偏二氟乙烯（VDF）的重复单元， ; 衍生自六氟丙烯（HFP）的重复单元; 衍生自具有以下通式的至少一种双烯烃[双烯烃（OF）]的重复单元：其中R 1，R 2，R 3，R 4，R 5和R 6彼此相同或不同，为H，卤素或可能包含一个或多个氧基团的C 1 -C 5任选卤代基团; Z是任选含有氧原子的直链或支链C1-C18任选卤代亚烷基或亚环烷基，或（全）氟聚氧亚烷基; 碘或溴固化点; 当根据ASTM D1646测量时，所述含氟弹性体还具有至少85MU（1 + 10 @ 121℃）的门尼粘度（ML）。

35. 发明申请

US20130123412A1 Fluoroelastomer composition 审中-公开
标题翻译：氟弹性体组合物
公开(公告)号：US20130123412A1
公开(公告)日：2013-05-16
申请号：US13810918
申请日：2011-07-14
申请人： Matteo Fantoni , Marco Apostolo , Giovanni Comino
发明人： Matteo Fantoni , Marco Apostolo , Giovanni Comino
IPC分类号： C08L29/10 , C08K7/00
CPC分类号： C08L29/10 , C08K7/00 , C08K9/02 , C08L27/12
摘要： A (per)fluoroelastomer composition having improved plasma resistance comprising at least one (per)fluoroelastomer [fluoroelastomer (A)] and from 0.1 to 50 weight parts per 100 parts by weight of said fluoroelastomer (A) of alkaline-earth metal carbonate particles [particles (P)]. Each particle comprises a core consisting essentially of at least one alkaline-earth metal carbonate and a shell consisting essentially of at least one Group IV transition metal compound.
摘要翻译：含有至少一种（全）含氟弹性体[含氟弹性体（A）]和0.1至50重量份/ 100重量份的所述含氟弹性体（A）的碱土金属碳酸盐颗粒的（全）含氟弹性体组合物[ 颗粒（P）]。每个颗粒包含基本上由至少一种碱土金属碳酸盐和基本上由至少一种IV族过渡金属化合物组成的壳组成的核。

36. 发明申请

US20130109797A1 Fluoroelastomer composition 有权
标题翻译：氟弹性体组合物
公开(公告)号：US20130109797A1
公开(公告)日：2013-05-02
申请号：US13809421
申请日：2011-07-08
申请人： Matteo Fantoni , Marco Apostolo , Marco Avataneo , Giuseppe Marchionni
发明人： Matteo Fantoni , Marco Apostolo , Marco Avataneo , Giuseppe Marchionni
IPC分类号： C08K5/06
CPC分类号： C08K5/06 , C08L27/18 , C08L51/08 , C08L53/00
摘要： The invention pertains to a (per)fluoroelastomer composition comprising: at least one (per)fluoroelastomer [fluoroelastomer (A)]; and from 0.1 to 30 weight parts, per hundred parts of fluoroelastomer (A), of at least one perfluoropolyether block copolymer [polymer (E)] comprising: A) one or more (per)fluoropolyoxyalkylene segment (chain Rt), that is to say a segment comprising recurring units having at least one catenary ether bond and at least one fluorocarbon moiety, and B) one or more polyalkylene segment (chain Ra) comprising recurring units of formula: —(CR1R2—CR3R4)— wherein R1, R2, R3, R4, equal to or different from each other, are selected from the group consisting of H, halogens (preferably F, Cl); C1-C6 (hydro)carbon groups, optionally containing fluorine or other heteroatoms, preferably perfluoroalkyl or (per)fluorooxyalkyl.
摘要翻译：本发明涉及一种（全）含氟弹性体组合物，其包含：至少一种（全）含氟弹性体[含氟弹性体（A）]; 和每100份含氟弹性体（A）0.1至30重量份的至少一种全氟聚醚嵌段共聚物[聚合物（E）]，其包含：A）一个或多个（全）氟聚氧亚烷基链段（链Rt），即例如包括具有至少一个链烯键和至少一个氟碳部分的重复单元的链段，以及B）包含式： - （CR 1 R 2 -CR 3 R 4） - 的重复单元的一个或多个聚亚烷基链段（链Ra） - 其中R1，R2， R 3，R 4彼此相同或不同，选自H，卤素（优选F，Cl）; 任选地含有氟或其它杂原子的C 1 -C 6（氢）碳基团，优选全氟烷基或（全）氟氧基烷基。

37. 发明授权

US07645845B2 Polymerization process 失效
标题翻译：聚合过程
公开(公告)号：US07645845B2
公开(公告)日：2010-01-12
申请号：US11476560
申请日：2006-06-29
申请人： Marco Apostolo , Valeri Kapeliouchko , Alessandro Galia , Onofrio Scialdone , Giuseppe Filardo
发明人： Marco Apostolo , Valeri Kapeliouchko , Alessandro Galia , Onofrio Scialdone , Giuseppe Filardo
IPC分类号： C08F12/20
CPC分类号： C08F14/18 , C08F2/04 , C08F2/08
摘要： A process for producing a polymer by polymerizing at least one fluorinated monomer in the presence of a radical initiator and a surfactant in a polymerization medium containing essentially only carbon dioxide. The surfactant is a functional (per)fluoropolyether having recurring units (R1) and at least one functional group containing a heteroatom other than fluorine, the recurring units containing at least one ether linkage in the main chain and at least one fluorine atom. Molded article containing the polymer obtained from the process.
摘要翻译：在基本上仅含有二氧化碳的聚合介质中，在自由基引发剂和表面活性剂的存在下使至少一种氟化单体聚合来制造聚合物的方法。表面活性剂是具有重复单元（R1）和至少一个含有除氟以外的杂原子的官能团的官能（全）氟聚醚，该重复单元在主链中含有至少一个醚键和至少一个氟原子。含有从该方法获得的聚合物的模制品。

38. 发明授权

US07408006B2 Perfluoroelastomeric compositions 有权
标题翻译：全氟弹性组合物
公开(公告)号：US07408006B2
公开(公告)日：2008-08-05
申请号：US11155890
申请日：2005-06-20
申请人： Giovanni Comino , Margherita Albano , Marco Apostolo
发明人： Giovanni Comino , Margherita Albano , Marco Apostolo
IPC分类号： C08F259/00
CPC分类号： C08K5/02 , C08F14/18 , C08K5/0025 , C08K5/14 , C08F2/02 , C08L27/12
摘要： A crosslinking system of perfuoroelastomers curable by peroxidic way comprising: as crosslinking agent, a bis-olefin having general formula: wherein: R1, R2, R3, R4, R5, R6, equal to or different from each other, are H or C1-C5 alkyls; Z is a C1-C18 linear or branched alkylene or cycloalkylene radical, optionally containing oxygen atoms, or a (per)fluoropolyoxyalkylene radical; the bis-olefin amount, expressed in per cent by weight on the total of polymer, being from 0.6% to 1.8%; peroxides for the peroxidic curing, capable to generate radicals by heating, in an amount from 0.2% to 1.3% by weight on the polymer.
摘要翻译：一种通过过氧化物可固化的增塑弹性体的交联体系，包括：作为交联剂，具有以下通式的双烯烃：其中：R 1，R 2，R 3 H或C 1，R 3，R 5，R 6，R 6，R 6，R 6和R 6彼此相同或不同， C 1 -C 5烷基; Z是任选含有氧原子的直链或支链亚烷基或亚环烷基，或（全）氟聚氧亚烷基; 以聚合物总量计的重量百分比表示的双烯烃含量为0.6％至1.8％; 能够通过加热产生自由基的过氧化物，其量为聚合物重量的0.2％至1.3％。

39. 发明申请

US20050282969A1 Perfluoroelastomeric compositions 有权
标题翻译：全氟弹性组合物
公开(公告)号：US20050282969A1
公开(公告)日：2005-12-22
申请号：US11155890
申请日：2005-06-20
申请人： Giovanni Comino , Margherita Albano , Marco Apostolo
发明人： Giovanni Comino , Margherita Albano , Marco Apostolo
IPC分类号： C08F14/18 , C08K5/00 , C08K5/02 , C08K5/14 , C08L27/12
CPC分类号： C08K5/02 , C08F14/18 , C08K5/0025 , C08K5/14 , C08F2/02 , C08L27/12
摘要： A crosslinking system of perfuoroelastomers curable by peroxidic way comprising: as crosslinking agent, a bis-olefin having general formula: wherein: R1, R2, R3, R4, R5, R6, equal to or different from each other, are H or C1-C5 alkyls; Z is a C1-C18 linear or branched alkylene or cycloalkylene radical, optionally containing oxygen atoms, or a (per)fluoropolyoxyalkylene radical; the bis-olefin amount, expressed in per cent by weight on the total of polymer, being from 0.6% to 1.8%; peroxides for the peroxidic curing, capable to generate radicals by heating, in an amount from 0.2% to 1.3% by weight on the polymer.
摘要翻译：一种通过过氧化物可固化的增塑弹性体的交联体系，包括：作为交联剂，具有以下通式的双烯烃：其中：R 1，R 2，R 3 H或C 1，R 3，R 5，R 6，R 6，R 6，R 6和R 6彼此相同或不同， C 1 -C 5烷基; Z是任选含有氧原子的直链或支链亚烷基或亚环烷基，或（全）氟聚氧亚烷基; 以聚合物总量计的重量百分比表示的双烯烃含量为0.6％至1.8％; 能够通过加热产生自由基的过氧化物，其量为聚合物重量的0.2％至1.3％。

40. 发明授权

US09458272B2 Low viscosity fluoroelastomers 有权
标题翻译：低粘度含氟弹性体
公开(公告)号：US09458272B2
公开(公告)日：2016-10-04
申请号：US13993782
申请日：2011-12-13
申请人： Marco Apostolo , Giovanni Comino , Marco Cristini
发明人： Marco Apostolo , Giovanni Comino , Marco Cristini
IPC分类号： C09D129/10 , C08F216/14 , C08F14/18 , C08F2/38 , C08F214/18 , C08F214/22
CPC分类号： C08F216/1408 , C08F2/38 , C08F14/18 , C08F214/18 , C08F214/184 , C08F214/222 , C09D129/10
摘要： The invention pertains to a low viscosity curable (per)fluoroelastomer [fluoroelastomer (A)] having a number-averaged molecular weight of 3 000 to 45 000, said (per)fluoroelastomer comprising at least 1% moles, with respect to the total moles of recurring units, of recurring units derived from at least one (per)fluoromethoxyalkylvinylether of formula (I): CFX′═CX″OCF2ORf formula (I) wherein X′ and X″, equal to or different from each other, are independently H or F; and Rf is selected from the group consisting of C1-C6 (per)fluoroalkyls, linear or branched; C5-C6 cyclic (per)fluoroalkyls; and C2-C6 (per)fluorooxyalkyls, linear or branched, comprising from 1 to 3 catenary ethereal oxygen atoms [monomer (M)].

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