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31. 发明授权

US4314046A Process for the stereoregular polymerization of .alpha.-olefins in the presence of a supported titanium catalyst 失效
标题翻译：在负载型钛催化剂存在下α-烯烃的立构规整聚合方法
公开(公告)号：US4314046A
公开(公告)日：1982-02-02
申请号：US172797
申请日：1980-07-28
申请人： Hiroshi Ueno , Masafumi Imai , Naomi Inaba , Makoto Yoda , Shozo Wada
发明人： Hiroshi Ueno , Masafumi Imai , Naomi Inaba , Makoto Yoda , Shozo Wada
IPC分类号： C08F4/00 , C08F4/60 , C08F4/64 , C08F10/00
CPC分类号： C08F10/00 , Y10S526/903 , Y10S526/906
摘要： A supported titanium catalyst, adaptable for use in the stereoregular polymerization of .alpha.-olefins, is produced by treating a supported titanium-containing solid, obtained by cogrinding a magnesium halide, tetravalent titanium halide and organic acid ester, with a hydrocarbon, organo halogen compound or mixture thereof with heating. The resulting supported titanium catalyst, when employed as a titanium component with an organo aluminum catalyst component for the catalyst system in a process for stereoregular polymerization of .alpha.-olefins, produces high polymerization activity and unexpectedly high stereoregular polymer yielding ratios.

32. 发明授权

US4240928A Titanium trichloride catalyst and process for the production thereof 失效
标题翻译：三氯化钛催化剂及其生产方法
公开(公告)号：US4240928A
公开(公告)日：1980-12-23
申请号：US927803
申请日：1978-07-25
申请人： Hiroshi Ueno , Naomi Inaba , Tukuo Makishima , Koh Watanabe , Shozo Wada
发明人： Hiroshi Ueno , Naomi Inaba , Tukuo Makishima , Koh Watanabe , Shozo Wada
IPC分类号： B01J27/10 , C08F4/64 , C08F10/00
CPC分类号： B01J27/10 , C08F10/00
摘要： A titanium trichloride catalytic complex is produced by reducing titanium tetrachloride with an alkylaluminum halide composition at low temperature and then treating the resulting reduced solids product by contacting it at elevated temperature with a dialkyl ether having alkyl groups of 4 to 5 carbon atoms and with hexachloroethane, the proportion of dialkyl ether being at least 1 mol per 1 mol of hexachloroethane and the proportion of hexachloroethane being at least greater than about 0.5 mol per 1 gram atom of titanium in the reduced solids product. The resulting titanium trichloride complex composition, when employed as co-catalyst with an organo-metal compound for Ziegler-type catalysts in polymerization of .alpha.-olefins, results in uniform polymer grains with unexpectedly high polymerization activity and high stereoregular polymer yielding ratios.
摘要翻译：通过在低温下用烷基卤化铝组合物还原四氯化钛，然后在升高的温度下将其与具有4至5个碳原子的烷基的二烷基醚和六氯乙烷接触来处理所得的还原固体产物，从而生产三氯化钛催化络合物，每1摩尔六氯乙烷中二烷基醚的比例至少为1摩尔，并且六氯乙烷的比例在还原固体产物中至少大于约0.5摩尔/克原子钛。所得到的三氯化钛复合物组合物当用作α-烯烃聚合中的齐格勒型催化剂的有机金属化合物作为助催化剂时，导致均匀的聚合物颗粒具有出乎预料的高聚合活性和高立体规则聚合物产率。

33. 发明授权

US4127505A Process for the production of a catalyst component for use in the polymerization of .alpha.-olefins 失效
标题翻译：制备用于聚合{60-烯烃的催化剂组分的方法
公开(公告)号：US4127505A
公开(公告)日：1978-11-28
申请号：US744236
申请日：1976-11-23
申请人： Hiroshi Ueno , Naomi Inaba , Tokyo Makishima , Shozo Wada
发明人： Hiroshi Ueno , Naomi Inaba , Tokyo Makishima , Shozo Wada
IPC分类号： C08F4/00 , C01G23/02 , C08F4/60 , C08F4/64 , C08F10/00
CPC分类号： C08F10/00
摘要： The invention relates to a process for the production of a catalyst component for use in the polymerization of .alpha.-olefins, which comprises reacting titanium tetrachloride with a dialkylaluminum monohalide and monoalkylaluminum dihalide, said dialkylaluminum monohalide being in a proportion of at least equimolar to said titanium tetrachloride, to thus obtain a violet reduced solid, then removing aluminum compounds contained in said reduced solid and further activating with a mixture or complex of titanium tetrachloride and a dialkyl ether of the general formula ROR' wherein R and R' are the same or different and are (a) alkyl groups having 1-4 carbon atoms, (b) normal alkyl groups having 5 carbon atoms or (c) alkyl groups having 6-20 carbon atoms and to a catalyst component prepared by the process of the invention.
摘要翻译：本发明涉及用于生产用于α-烯烃聚合的催化剂组分的方法，该方法包括使四氯化钛与二烷基铝一卤化物和一烷基铝二卤化物反应，所述二烷基铝一卤化物与所述钛的至少等摩尔比例从而获得紫色还原固体，然后除去所述还原固体中所含的铝化合物，并进一步用四氯化钛和通式ROR'的二烷基醚的混合物或络合物活化，其中R和R'相同或不同并且是（a）具有1-4个碳原子的烷基，（b）具有5个碳原子的正烷基或（c）具有6-20个碳原子的烷基和通过本发明的方法制备的催化剂组分。

34. 发明授权

US5061667A Catalytic component for olefin polymerization 失效
标题翻译：用于烯烃聚合的催化组分
公开(公告)号：US5061667A
公开(公告)日：1991-10-29
申请号：US576106
申请日：1990-08-29
申请人： Masahide Murata , Seizaburo Kanazawa , Hiroyuki Furuhashi , Kouji Maruyama , Masafumi Imai , Hiroshi Ueno
发明人： Masahide Murata , Seizaburo Kanazawa , Hiroyuki Furuhashi , Kouji Maruyama , Masafumi Imai , Hiroshi Ueno
IPC分类号： C08F4/60 , C08F4/64 , C08F4/654 , C08F4/658 , C08F10/00
CPC分类号： C08F10/00 , Y10S526/904
摘要： A catalytic component for olefin polymerization, produced by a process which comprises causing (A) magnesium metal, (B) a halogenated hydrocarbon represented by the general formula, RX [wherein R stands for an alkyl group, an aryl group, or a cycloalkyl group each having 1 to 20 carbon atoms and X for a halogen atom], and (C) a compound represented by the general formula, X.sub.n.sup.1 M(OR.sup.1).sub.m-n [wherein X.sup.1 stands for a hydrogen atom, a halogen atom, or a hydrocarbon group having 1 to 20 carbon atoms, M for a boron, carbon, aluminum, silicon, or phorphorus atom, R.sup.1 stands for a hydrocarbon group having 1 to 20 carbon atoms, m for the valency of M, and m>n.gtoreq.0] to contact (D) a halogen-containing alcohol and then contact (E) an electron donating compound and (F) a titanium compound thereby forming a titanium-containing solid substance, and causing said titanium-containing solid substance, in the presence of (G) an organic aluminum compound, to contact (H) an olefin thereby allowing said titanium-containing solid substance to incorporate therein a corresponding olefin polymer in a ratio in the range of 0.1 to 100 g per g of said titanium-containing solid substance.

35. 发明授权

US4814313A Method of production of catalyst carrier for polymerization of olefin 失效
标题翻译：烯烃聚合催化剂载体的生产方法
公开(公告)号：US4814313A
公开(公告)日：1989-03-21
申请号：US132752
申请日：1987-12-14
申请人： Masahide Murata , Masafumi Imai , Hiroyuki Furuhashi , Kouji Maruyama , Hiroshi Ueno
发明人： Masahide Murata , Masafumi Imai , Hiroyuki Furuhashi , Kouji Maruyama , Hiroshi Ueno
IPC分类号： C08F4/02 , C08F4/60 , C08F4/64 , C08F4/658 , C08F10/00
CPC分类号： C08F10/00
摘要： A method for the production of a catalyst carrier for use in the polymerization of an olefin, which method comprises causing a magnesium-containing solid obtained by contact of (A) magnesium metal, (B) a halogenated hydrocarbon represented by the general formula, RX wherein R stands for an alkyl, aryl, or cycloalkyl group having 1 to 20 carbon atoms and X for a halogen atom, and (C) a compound of the general formula, X.sub.n.sup.1 M(OR.sup.1).sub.m-n wherein X.sup.1 stands for a hydrogen atom, a halogen atom, or a hydrocarbon group having 1 to 20 carbon atoms, M for a boron, carbon, silicon, aluminum, or phosphorus atom, R.sup.1 for a hydrocarbon group having 1 to 20 carbon atoms, and m for the valency of said atom M, providing that m>n.gtoreq.0 is satisfied, to contact (D) a halogen-containing alcohol.

36. 发明授权

US4960743A Method for production of catalyst carrier for polymerization of olefin 失效
标题翻译：烯烃聚合催化剂载体的制备方法
公开(公告)号：US4960743A
公开(公告)日：1990-10-02
申请号：US273397
申请日：1988-11-18
申请人： Masahide Murata , Masafumi Imai , Hiroyuki Furuhashi , Kouji Maruyama , Hiroshi Ueno
发明人： Masahide Murata , Masafumi Imai , Hiroyuki Furuhashi , Kouji Maruyama , Hiroshi Ueno
IPC分类号： C08F4/02 , C08F4/64 , C08F10/00
CPC分类号： C08F10/00
摘要： A method for the production of a catalyst carrier for use in the polymerization of an olefin, which method comprises causing a magnesium-containing solid obtained by contact of (A) magnesium metal, (B) a halogenated hydrocarbon represented by the general formula, RX [wherein R stands for an alkyl, aryl, or cycloalkyl group having 1 to 20 carbon atoms and X stands for a halogen atom], and (C) a compound of the general formula, X.sub.n.sup.1 M(OR.sup.1).sub.m-n [wherein X.sup.1 stands for a hydrogen atom, a halogen atom, or a hydrocarbon group having 1 to 20 carbon atoms, M stands for a boron, carbon, aluminum, silicon, or phosphorus atom, R.sup.1 stands for a hydrocarbon group having 1 to 20 carbon atoms, and m stands for the valency of said atom M, providing that m>n.gtoreq.0 is satisfied], to contact (D) a halogen-containing alcohol.

37. 发明授权

US4814312A Method for production of catalyst component for olefin polymerization 失效
标题翻译：烯烃聚合催化剂组分的生产方法
公开(公告)号：US4814312A
公开(公告)日：1989-03-21
申请号：US132751
申请日：1987-12-14
申请人： Masahide Murata , Masafumi Imai , Hiroyuki Furuhashi , Kouji Maruyama , Hiroshi Ueno
发明人： Masahide Murata , Masafumi Imai , Hiroyuki Furuhashi , Kouji Maruyama , Hiroshi Ueno
IPC分类号： C08F4/64 , C08F10/00
CPC分类号： C08F10/00
摘要： A method for the production of a catalyst component for use in the polymerization of an olefin, which method comprises causing a magnesium-containing solid obtained by contact of (A) magnesium metal, (B) a halogenated hydrocarbon represented by the general formula, RX [wherein R stands for an alkyl, aryl, or cycloalkyl group having 1 to 20 carbon atoms and X for a halogen atom], and (C) a compound of the general formula, X.sub.n.sup.1 M(OR.sup.1).sub.m-n [wherein X.sup.1 stands for a hydrogen atom, a halogen atom, or a hydrocarbon group having 1 to 20 carbon atoms, M for a boron, carbon, silicon, aluminum, or phosphorus atom, R.sup.1 for a hydrocarbon group having 1 to 20 carbon atoms, and m for the valency of said atom M, providing that m>n.gtoreq.0 is satisfied], to contact (D) a halogen-containing alcohol and then contact (E) an electron donor type compound and (F) a titanium compound.

38. 发明授权

US4950630A Method for production of catalyst component for olefin polymerization 失效
标题翻译：烯烃聚合催化剂组分的生产方法
公开(公告)号：US4950630A
公开(公告)日：1990-08-21
申请号：US273400
申请日：1988-11-18
申请人： Masahide Murata , Masafumi Imai , Hiroyuki Furuhashi , Kouji Maruyama , Hiroshi Ueno
发明人： Masahide Murata , Masafumi Imai , Hiroyuki Furuhashi , Kouji Maruyama , Hiroshi Ueno
IPC分类号： C08F4/64 , C08F10/00
CPC分类号： C08F10/00
摘要： A method for the production of a catalyst component for use in the polymerization of an olefin, which method comprises causing a magnesium-containing solid obtained by contact of (A) magnesium metal, (B) a halogenated hydrocarbon represented by the general formula, RX [wherein R stands for an alkyl, aryl, or cycloalkyl group having 1 to 20 carbon atoms and X stands for a halogen atom], and (C) a compound of the general formula, X.sub.n.sup.1 M(OR.sup.1).sub.m-n [wherein X.sup.1 stands for a hydrogen atom, a halogen atom, or a hydrocarbon group having 1 to 20 carbon atoms, M stands for a boron, carbon, aluminum, silicon, or phosphorus atom, R.sup.1 stands for a hydrocarbon group having 1 to 20 carbon atoms, and m stands for the valency of said atom M, providing that m>n.gtoreq.0 is satisfied], to contact (d) a halogen-containing alcohol and then contact (E) an electron donor type compound and (F) a titanium compound.

39. 发明授权

US4814311A Method for production of catalyst component for olefin polymerization (P-1292) 失效
标题翻译：烯烃聚合催化剂组分的生产方法（P-1292）
公开(公告)号：US4814311A
公开(公告)日：1989-03-21
申请号：US132735
申请日：1987-12-14
申请人： Masahide Murata , Masafumi Imai , Hiroyuki Furuhashi , Kouji Maruyama , Hiroshi Ueno
发明人： Masahide Murata , Masafumi Imai , Hiroyuki Furuhashi , Kouji Maruyama , Hiroshi Ueno
IPC分类号： C08F4/60 , C08F4/64 , C08F4/658 , C08F10/00
CPC分类号： C08F10/00
摘要： A method for the production of a catalyst component for use in the polymerization of an olefin, which method comprises causing a magnesium-containing solid obtained by contact of (A) magnesium metal, (B) a halogenated hydrocarbon represented by the general formula, RX, wherein R stands for an alkyl, aryl, or cycloalkyl group having 1 to 20 carbon atoms and X for a halogen atom, and (C) a compound of the general formula, X.sub.n.sup.1 M(OR.sup.1).sub.m-n, wherein X.sup.1 stands for a hydrogen atom, a halogen atom, or a hydrocarbon group having 1 to 20 carbon atoms, M for a boron, carbon, silicon, aluminum, or phosphorus atom, R.sup.1 for a hydrocarbon group having 1 to 20 carbon atoms, and m for the valency of said atom M, providing that m>n.gtoreq.0 is satisfied, to contact (D) a halogen-containing alcohol and then contact (E) a titanium compound.

40. 发明授权

US10485853B2 Cheese and method for producing the same 有权
公开(公告)号：US10485853B2
公开(公告)日：2019-11-26
申请号：US14418224
申请日：2012-07-31
申请人： Aiko Ohmachi , Hiroaki Matsuyama , Yoshikazu Morita , Yuko Ishida , Takayuki Nara , Ken Kato , Atsushi Serizawa , Hiroshi Ueno , Hiroshi Urazono
发明人： Aiko Ohmachi , Hiroaki Matsuyama , Yoshikazu Morita , Yuko Ishida , Takayuki Nara , Ken Kato , Atsushi Serizawa , Hiroshi Ueno , Hiroshi Urazono
IPC分类号： A61K38/46 , A61K38/44 , A23C19/06 , A23C19/05 , A23C19/076 , A23C19/082
CPC分类号： A61K38/465 , A23C19/053 , A23C19/063 , A23C19/076 , A23C19/082 , A61K38/44 , A23V2002/00 , A23V2200/00 , A23V2200/306 , A23V2250/55 , C12Y111/01007 , C12Y301/27
摘要： The invention relates to a cheese includes angiogenin and/or angiogenin hydrolysate in an amount of 6.5 mg/100 g to 160 mg/100 g, and lactoperoxidase and/or lactoperoxidase hydrolysate in the mass ratio to the angiogenin and/or angiogenin hydrolysate of 0.3 to 33.

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