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31. 发明授权

US6026880A Process and apparatus for the purification of commercially available diphenyl-p-phenylenediamine (DPPD) 失效
标题翻译：用于纯化市售二苯基对苯二胺（DPPD）的方法和设备
公开(公告)号：US6026880A
公开(公告)日：2000-02-22
申请号：US301601
申请日：1999-04-29
申请人： Albert-Johannes Frings , Michael Horn , Peter Jenker , Jaroslaw Monkiewicz , Hans-Guenther Srebny , Burkhard Standke , Bertram Trautvetter
发明人： Albert-Johannes Frings , Michael Horn , Peter Jenker , Jaroslaw Monkiewicz , Hans-Guenther Srebny , Burkhard Standke , Bertram Trautvetter
IPC分类号： B01D11/02 , C07C209/84 , C07C211/54 , C07C211/55 , C07F7/18 , B60C1/00 , B60C9/02
CPC分类号： C07C211/55 , B01D11/028 , C07C209/84
摘要： A process for the purification of crude N,N'-diphenyl-p-phenylenediamine (DPPD), which comprises extracting crude DPPD with a hydrocarbon or hydrocarbon mixtures thereby forming an extract solution containing DPPD, passing the extract solution over an adsorption layer, and recovering purified DPPD from the solution.
摘要翻译：一种用于净化粗N，N'-二苯基对苯二胺（DPPD）的方法，其包括用烃或烃混合物提取粗DPPD，由此形成含有DPPD的提取溶液，使提取液超过吸附层，以及从溶液中回收纯化的DPPD。

32. 发明授权

US5932757A Mixture of oligomers of condensed alkylalkoxysilanes 失效
标题翻译：缩合的烷基烷氧基硅烷的低聚物的混合物
公开(公告)号：US5932757A
公开(公告)日：1999-08-03
申请号：US877556
申请日：1997-06-17
申请人： Burkhard Standke , Roland Edelmann , Albert Frings , Michael Horn , Peter Jenkner , Ralf Laven , Jaroslaw Monkiewicz , Lothar Elfenthal , Hans-Hermann Luginsland
发明人： Burkhard Standke , Roland Edelmann , Albert Frings , Michael Horn , Peter Jenkner , Ralf Laven , Jaroslaw Monkiewicz , Lothar Elfenthal , Hans-Hermann Luginsland
IPC分类号： C07F7/18 , B01J2/30 , C07F7/08 , C07F7/21 , C08G77/04 , C09D183/04
CPC分类号： B01J2/30 , C07F7/0859 , C07F7/21 , C08G77/045 , C09D183/04
摘要： A mixture of oligomers of alkylalkoxysilanes condensed in the chain and/or cyclic form, said mixture of oligomers containing less than 2% by weight of free alcohols and the condensed alkoxysilanes satisfying formula I: ##STR1## wherein R is an alkyl group having 3 to 18 carbon atoms, and each R' is a member (i) selected from the group consisting of methyl, ethyl or hydrogen, or is (ii) methyl or hydrogen, or is (iii) ethyl or hydrogen, the degree of oligomerization being in the range 2.ltoreq.x.ltoreq.20 and the quotient of the molar ratio �Si/alkoxy group!.gtoreq.1; and/orsatisfying formula II: ##STR2## in which R is an alkyl group having 3 to 18 carbon atoms, and each R' is a member (i) selected from the group consisting of methyl, ethyl or hydrogen, or is (ii) methyl or hydrogen or is (iii) ethyl or hydrogen, the degree of oligomerization being x.gtoreq.3 and the quotient of the molar ratio �Si/alkoxy group!.gtoreq.1.
摘要翻译：以链和/或环状缩合的烷基烷氧基硅烷的低聚物的混合物，所述含低于2重量％游离醇的低聚物混合物和满足式I的缩合烷氧基硅烷：其中R是具有3至18个碳原子的烷基，并且每个R'是选自甲基，乙基或氢的成员（i），或（ii）甲基或氢，或（iii）乙基或氢，低聚度的范围为2 = 1的商; 和/或满足式II：其中R是具有3至18个碳原子的烷基，并且每个R'是选自甲基，乙基或氢的成员（i），或者是（ⅱ）甲基或氢或是（ⅲ）乙基或氢，低聚度为x≥3，摩尔比[Si /烷氧基]> = 1的商。

33. 发明授权

US5817854A Process for the preparation of organocarbonoyloxysilanes 失效
标题翻译：制备有机碳酰氧基硅烷的方法
公开(公告)号：US5817854A
公开(公告)日：1998-10-06
申请号：US978025
申请日：1997-11-25
申请人： Michael Horn , Albert-Johannes Frings , Peter Jenkner , Jaroslaw Monkiewicz , Claus-Dietrich Seiler , Burkhard Standke , Bertram Trautvetter
发明人： Michael Horn , Albert-Johannes Frings , Peter Jenkner , Jaroslaw Monkiewicz , Claus-Dietrich Seiler , Burkhard Standke , Bertram Trautvetter
IPC分类号： B01J31/02 , C07B61/00 , C07F7/18 , C07F7/08
CPC分类号： C07F7/1896
摘要： Organocarbonoyloxysilanes are prepared by reacting an organochlorosilane with a carboxylic acid in a first step which liberates HCl, removing the HCl which is formed, reacting the reaction mixture from the first step with a carboxylic acid anhydride in a second reaction step, the first and/or second reaction steps being conducted in the presence of a catalyst, and isolating the resulting organocarbonoyloxysilane product from the reaction mixture.
摘要翻译：有机氯硅烷与羧酸反应制备，第一步是释放HCl，除去形成的HCl，使第一步的反应混合物与羧酸酐在第二反应步骤中反应，第一和/或在催化剂存在下进行第二反应步骤，并从反应混合物中分离得到的有机碳硅烷氧基硅烷产物。

34. 发明授权

US5616762A Process for the preparation of 3-halo-and pseudohalo-alkylsilane esters 失效
标题翻译： 3-卤代 - 和拟卤代烷基硅烷酯的制备方法
公开(公告)号：US5616762A
公开(公告)日：1997-04-01
申请号：US548131
申请日：1995-10-25
申请人： Frank Kropfgans , Albert Frings , Michael Horn , Hans-Joachim Koetzsch , Jaroslaw Monkiewicz , Claus-Dietrich Seiler , Hans-Guenther Srebny , Burkhard Standke
发明人： Frank Kropfgans , Albert Frings , Michael Horn , Hans-Joachim Koetzsch , Jaroslaw Monkiewicz , Claus-Dietrich Seiler , Hans-Guenther Srebny , Burkhard Standke
IPC分类号： B01J31/02 , C07B61/00 , C07F7/08 , C07F7/10 , C07F7/18
CPC分类号： B01J31/02 , C07B61/00 , C07F7/08 , C07F7/10 , C07F7/18
摘要： 3-Halo- and pseudohalo-alkylsilane esters are prepared by reacting an allyl X compound or a compound containing an allyl X structure with a hydridosilane ester in the presence of an iridium catalyst prepared under specific conditions and/or the reaction medium containing a 0.01-100 mol % excess of the allyl X compound or compound containing the allyl X unit relative to the amount of hydridosilane ester reactant.
摘要翻译： 3-卤代和假卤代烷基硅烷酯是通过烯丙基X化合物或含有烯丙基X结构的化合物与氢化硅烷酯在特定条件下制备的铱催化剂和/或含有0.01- 100摩尔％过量的烯丙基X化合物或含有烯丙基X单元的化合物相对于氢硅烷酯反应物的量。

35. 发明授权

US5527937A Process for preparing hydrogenalkoxysilanes 失效
标题翻译：制备氢烷氧基硅烷的方法
公开(公告)号：US5527937A
公开(公告)日：1996-06-18
申请号：US538636
申请日：1995-10-04
申请人： Burkhard Standke , Albert Frings , Michael Horn , Hans-Joachim Koetzsch , Frank Kropfgans , Jaroslaw Monkiewicz , Claus-Dietrich Seiler , Hans-Guenther Srebny
发明人： Burkhard Standke , Albert Frings , Michael Horn , Hans-Joachim Koetzsch , Frank Kropfgans , Jaroslaw Monkiewicz , Claus-Dietrich Seiler , Hans-Guenther Srebny
IPC分类号： B01J27/122 , C07B61/00 , C07F7/02 , C07F7/04 , C07F7/18
CPC分类号： C07F7/025
摘要： Hydrogenalkoxysilanes are prepared by direct reaction of finely divided metallic silicon with alcohols in the presence of copper-containing catalysts in a heat-transfer oil comprising tritoluenes, tetratoluenes or mixtures thereof at from 100.degree. to 350.degree. C.
摘要翻译：在含铜催化剂存在下，在100-350℃的含三木聚四烯或其混合物的传热油中，通过细分的金属硅与醇的直接反应来制备氢烷氧基硅烷。

36. 发明授权

US08795784B2 Aqueous emulsions of functional alkoxysilanes and condensed oligomers thereof, their preparation and use for surface treatment 有权
标题翻译：功能性烷氧基硅烷及其缩合低聚物的水乳液，其制备和用于表面处理
公开(公告)号：US08795784B2
公开(公告)日：2014-08-05
申请号：US11815391
申请日：2005-12-08
申请人： Burkhard Standke , Kerstin Weissenbach , Bernd Bartkowiak
发明人： Burkhard Standke , Kerstin Weissenbach , Bernd Bartkowiak
IPC分类号： C09D5/16 , B01J31/02 , C08L5/00 , C09K3/00 , B05D3/00 , C04B41/49 , C08J3/03 , C04B41/00 , C04B111/00
CPC分类号： C08J3/03 , C04B41/009 , C04B41/4961 , C04B2111/00112 , C08J2383/04 , C04B41/4922 , C04B41/502 , C04B2103/40 , C04B28/02
摘要： Aqueous oil-in-water emulsion comprising from 1 to 70% by weight, based on the total weight of the emulsion, of functional alkoxysilanes and/or condensed oligomers thereof and/or organoalkoxysiloxanes, at least one emulsifier and water, wherein the emulsion has a pH of from 5 to 9 and preferably a mean droplet size of the disperse phase of ≦0.5 μm, and the width of the droplet size distribution, expressed as the span (Formula I), is from 0.6 to 1.2. The preparation of the emulsions having the desired droplet size distribution is carried out in apparatuses having at least one pressure stage at a pressure of from 2 to 15 MPa. The emulsion can be used for hydrophobicizing porous mineral building materials.
摘要翻译：水包油包水乳液包含1至70重量％，基于乳液的总重量，官能的烷氧基硅烷和/或其缩合的低聚物和/或有机烷氧基硅氧烷，至少一种乳化剂和水，其中乳液具有 pH为5至9，优选分散相的平均液滴尺寸为＆lt; lE;0.5μm，液滴尺寸分布的宽度以跨度（式I）表示为0.6至1.2。具有所需液滴尺寸分布的乳液的制备在具有2至15MPa压力的至少一个压力级的装置中进行。该乳液可用于疏水化多孔矿物建筑材料。

37. 发明申请

US20080188617A1 High-Viscosity Aqueous Emulsions Of Functional Alkoxysilanes, Condensed Oligomers Thereof, Organopolysiloxanes, Their Preparation And Use For Surface Treatment Of Inorganic Materials 有权
公开(公告)号：US20080188617A1
公开(公告)日：2008-08-07
申请号：US11814127
申请日：2005-12-08
申请人： Burkhard Standke , Kerstin Weissenbach , Bernd Bartkowiak
发明人： Burkhard Standke , Kerstin Weissenbach , Bernd Bartkowiak
IPC分类号： C04B41/49 , C08J3/03 , C09D183/04
CPC分类号： C08J3/03 , C04B41/009 , C04B41/4961 , C08J2383/04 , Y10T428/249953 , Y10T428/249954 , Y10T428/249955 , Y10T428/249956 , C04B41/4922 , C04B41/502 , C04B2103/40 , C04B33/00 , C04B14/043 , C04B28/02
摘要： High-viscosity aqueous emulsions of functional alkoxysilanes, condensed oligomers thereof, organopolysiloxanes, their preparation and use for the surface treatment of inorganic materials High-viscosity aqueous oil-in-water emulsion which comprises from 50 to 90% by weight, based on the total weight of the emulsion, of functional alkoxysilanes and/or condensed oligomers thereof and/or organoalkoxysiloxanes, at least one emulsifier and water and has a pH of from 5 to 9 and a mean droplet size of the disperse phase of less than 5 μm, wherein the width of the droplet size distribution, expressed as the span (see formula (I)), is >1.5, preferably from 3 to 8. The preparation of the emulsions having the desired droplet size distribution is carried out in apparatuses having at least one pressure stage at a pressure of from 2 to 15 MPa. The emulsion can be used for hydrophobicizing porous mineral building materials. D   90 - D   10 D   50 ( I )

38. 发明申请

US20080233341A1 Special Aminoalkylsilane Compounds as Binders for Composite Materials 有权
公开(公告)号：US20080233341A1
公开(公告)日：2008-09-25
申请号：US11995215
申请日：2006-06-02
申请人： Peter Jenkner , Burkhard Standke , Jaroslaw Monkiewicz , Roland Edelmann , Alireza Kharazipour , Lars Kloeser
发明人： Peter Jenkner , Burkhard Standke , Jaroslaw Monkiewicz , Roland Edelmann , Alireza Kharazipour , Lars Kloeser
IPC分类号： B32B5/12 , C09K3/00 , C09K21/00
CPC分类号： C08L97/02 , C08K5/544 , Y10T428/24124 , Y10T428/249965 , Y10T428/249972 , Y10T428/253 , Y10T428/254 , Y10T428/31591 , C08L2666/44
摘要： The present invention relates to composite materials based on (a) at least one cellulose- or lignocellulose-containing material and (b) at least one aminoalkylsilane of the formula (I) R1R2N(CHR4)aSi(R3)r(OR)3-r (I), in which groups R1 and R2 are identical or different and in each case are H or a linear, branched or cyclic C1- to C20-alkyl group or an aryl group or an aminocarbyl group, it being possible for groups R1 and R2 to be optionally substituted, groups R4 are identical or different and R is H or methyl, a is from 1 to 10, R3 is H or a linear or branched C1- to C8-alkyl group, groups R are identical or different and R is H or a linear or branched C1- to C8-alkyl group and r is 0 or 1 or 2, or at least one cocondensate of at least one aminoalkylsilane of the general formula (I) and at least one further functional silane of the general formula (II) R7(CHR6)bSi(R5)p(OR)3-p (II), in which R7 is H or a vinyl group or an amino group or a glycidyloxy group or an acryloyloxy group or a methacryloyloxy group or a mercapto group or a sulfane group or a linear or branched C1- to C20-alkyl group or an aryl group, it being possible for the group R7 to be optionally substituted, groups R6 are identical or different and R6 is H or methyl, b is from 0 to 18, R5 is H or a linear or branched C1- to C8-alkyl group, groups R are identical or different and R is H or a linear or branched C1- to C8-alkyl group and p is 0 or 1 or 2, it being possible for the amino functions in the cocondensate to be partly or completely neutralized with an inorganic or organic acid, or an aqueous solution which contains at least one aminoalkylsilane of the formula (I) or at least one cocondensate based on at least one aminoalkylsilane of the general formula (I) and at least one further functional silane of the general formula (II), as a binder, such composite materials being obtainable by—treating dried or moist cellulose- or lignocellulose-containing material with—a liquid which contains at least one aminosilane compound according to the formula (I) or at least one cocondensate based on at >least one aminoalkylsilane of the general formula (I) and at least one further functional silane of the general formula (II),—bringing the cellulose or lignocellulose material thus treated into a desired form and then hot-pressing it. The present invention furthermore relates to a corresponding process for the production of composite materials and the use of aminosilane compounds according to the formula (I) or at least one cocondensate based on at least one aminoalkylsilane of the general formula (I) and at least one further functional silane of the general formula (II) as a binder for producing wood-based materials.

39. 发明申请

US20080221318A1 Cellulose- or Lignocellulose-Containing Composite Materials Based on a Silane-Based Composite as a Binder 有权
标题翻译：基于硅烷基复合材料作为粘结剂的含纤维素或木质素纤维素的复合材料
公开(公告)号：US20080221318A1
公开(公告)日：2008-09-11
申请号：US11995550
申请日：2006-06-14
申请人： Roland Edelmann , Burkhard Standke , Peter Jenkner , Alireza Kharazipour , Lars Kloeser , Jaroslaw Monkiewicz
发明人： Roland Edelmann , Burkhard Standke , Peter Jenkner , Alireza Kharazipour , Lars Kloeser , Jaroslaw Monkiewicz
IPC分类号： C08L97/02 , C08B15/00
CPC分类号： C08L83/06 , C08K5/0091 , C08L1/02 , C08L97/02 , C08L83/00 , C08L2666/58 , C08L2666/26 , C08L2666/02
摘要： The present invention relates to a composite material based on (a) a cellulose- or lignocellulose-containing material and (b) a composite as a binder, the composite resulting from the reaction of at least the components (i) a glycidyloxypropylalkoxysilane, (ii) an aqueous silica sol having a solids content of >20% by weight, (iii) an organic acid as a hydrolysis catalyst and (iv) n-propyl zirconate, butyl titanate or titanium acetylacetonate as a crosslinking agent. The present invention furthermore relates to a process for the production of said composite materials and the use of a composite (b) as a binder for the production of wood-based materials.
摘要翻译：本发明涉及一种基于（a）含纤维素或木质素纤维素材料和（b）作为粘合剂的复合材料的复合材料，所述复合材料由至少组分（i）缩水甘油氧基丙基烷氧基硅烷（ii））固体含量> 20重量％的水性硅溶胶，（iii）作为水解催化剂的有机酸和（iv）锆酸正丙酯，钛酸丁酯或乙酰丙酮钛作为交联剂。本发明还涉及生产所述复合材料的方法以及复合材料（b）作为用于生产木质材料的粘合剂的用途。

40. 发明申请

US20080206572A1 Silane-Containing Binder for Composite Materials 有权
标题翻译：含硅烷的复合材料粘合剂
公开(公告)号：US20080206572A1
公开(公告)日：2008-08-28
申请号：US11995751
申请日：2006-06-14
申请人： Roland Edelmann , Burkhard Standke , Peter Jenkner , Alireza Kharazipour , Lars Kloeser , Jaroslaw Monkiewicz
发明人： Roland Edelmann , Burkhard Standke , Peter Jenkner , Alireza Kharazipour , Lars Kloeser , Jaroslaw Monkiewicz
IPC分类号： B32B27/40 , C08L1/02 , B32B27/00 , C08J5/00 , C08L75/04
CPC分类号： C09J161/00 , C08J5/045 , C08J2361/06 , C08K5/544 , C08L61/20 , C08L97/02 , C09J161/06 , C09J161/24 , C09J161/28 , C09J189/00 , C09J193/00 , Y10T428/31591 , Y10T428/31663 , Y10T428/31848 , C08L83/00 , C08L2666/16
摘要： The present invention relates to a binder for composite materials comprising cellulose- or lignocellulose-containing materials, which is based on the components (i) at least one binder from the series consisting of organic resins, isocyanates, natural or near-natural binders and (ii) at least one composition based on an aminoalkylsilane. The invention furthermore relates to a composite material which is at least based on a cellulose- or lignocellulose-containing material and the abovementioned binder, a process for the production of such a composite material and the use of the binder system according to the invention for the production of wood-based materials.
摘要翻译：本发明涉及一种用于复合材料的粘合剂，其包含含纤维素或木质素纤维素的材料，其基于组分（i）至少一种由有机树脂，异氰酸酯，天然或近天然粘合剂组成的系列的粘合剂和（ ii）至少一种基于氨基烷基硅烷的组合物。本发明还涉及至少基于含纤维素或木质素纤维素材料和上述粘合剂的复合材料，用于生产这种复合材料的方法以及根据本发明的粘合剂体系用于生产木质材料。

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