会员体验
专利管家(专利管理)
工作空间(专利管理)
风险监控(情报监控)
数据分析(专利分析)
侵权分析(诉讼无效)
联系我们
交流群
官方交流:
QQ群: 891211   
微信请扫码    >>>
现在联系顾问~
热词
    • 32. 发明申请
    • METHOD FOR PRODUCING HYDRIDOSILANES
    • 生产水合物的方法
    • US20120214005A1
    • 2012-08-23
    • US13504331
    • 2010-11-08
    • Stephan WieberMatthias PatzMartin TrochaHartwig RaulederEkkehard MuehHarald StuegerChristoph Walkner
    • Stephan WieberMatthias PatzMartin TrochaHartwig RaulederEkkehard MuehHarald StuegerChristoph Walkner
    • B32B9/04C01B33/04
    • C01B33/04C01B33/043C01B33/10773Y10T428/31663
    • The invention relates to a method for producing hydridosilanes from halosilanes by a) reacting i) at least one halosilane of the generic formula SinX2n+2 (with n≧3 and X═F, Cl, Br and/or I) with ii) at least one catalyst of the generic formula NRR'aR″bYc with a=0 or 1, b=0 or 1, and c=0 or 1, and formula (I), wherein aa) R, R′ and/or R″ are —C1-C12 alkyl, —C1-C12 aryl, —C1-C12 aralkyl, —C1-C12 aminoalkyl, —C1-C12 aminoaryl, —C1-C12 aminoaralkyl, and/or two or three groups R, R′ and R″ (if c=0) together form a cyclic or bicyclic, heteroaliphatic or heteroaromatic system including N, with the proviso that at least one group R, R′ or R″ is unequal —CH3 and/or wherein bb) R and R′ and/or R″' (if c=1) are —C1-C12 alkylene, —C1-C12 arylene, —C1-C12 aralkylene, —C1-C12 heteroalkylene, —C1-C12 heteroarylene, —C1-C12 heteroaralkylene and/or —N═, or cc) (if a=b=c=0) R═≡C-R′″ (with R′″═—C1-C10 alkyl, —C1-C10 aryl and/or —C1-C10 aralkyl), while forming a mixture comprising at least one halosilane of the generic formula SimX2m+2 (with m>n and X═F, Cl, Br and/or I) and SiX4 (with X═F, Cl, Br and/or I), and b) hydrogenating the at least one halosilane of the generic formula SimH2m+2 while forming a hydridosilane of the generic formula SimH2m+2. The invention also relates to the hydridosilanes producible according to said method and to their use
    • 本发明涉及一种由卤代硅烷生产氢硅烷的方法,其通过以下步骤:a)使i)至少一种通式为SinX2n + 2(n≥3,X = F,Cl,Br和/或I)的卤代硅烷与ii) a = 0或1,b = 0或1,c = 0或1和式(I)的通式NRR'aR“bYc的至少一种催化剂,其中aa)R,R'和/或R” 是-C 1 -C 12烷基,-C 1 -C 12芳基,-C 1 -C 12芳烷基,-C 1 -C 12氨基烷基,-C 1 -C 12氨基芳基,-C 1 -C 12氨基烷基和/或两个或三个基团R,R'和R “(如果c = 0)一起形成包括N的环状或双环,杂脂族或杂芳族体系,条件是至少一个基团R,R'或R”不等于-CH 3和/或其中bb)R和R' 和/或R“'(如果c = 1)是-C 1 -C 12亚烷基,-C 1 -C 12亚芳基,-C 1 -C 12亚芳基,-C 1 -C 12杂亚烷基,-C 1 -C 12亚杂芳基,-C 1 -C 12杂亚烷基和/ 或-N =或cc)(如果a = b = c = 0)R≡≡CR'“(其中R'”= C 1 -C 10烷基,-C 1 -C 10芳基和/或-C 1 -C 10芳烷基),同时形成包含通式SimX2m + 2(具有m> n和X = F,Cl,Br和/或I)的至少一种卤代硅烷和SiX 4(具有X = F,Cl,Br和 /或I),和b)在形成通式SimH 2 m + 2的氢硅烷的同时使通式SimH 2 m + 2的至少一种卤代硅烷氢化。 本发明还涉及根据所述方法可生产的氢硅石及其用途
    • 34. 发明申请
    • REMOVAL OF EXTRANEOUS METALS FROM SILICON COMPOUNDS BY ADSORPTION AND/OR FILTRATION
    • 通过吸附和/或过滤从硅化合物中去除非常金属
    • US20110184205A1
    • 2011-07-28
    • US13121702
    • 2009-10-13
    • Hartwig RaulederEkkehard Mueh
    • Hartwig RaulederEkkehard Mueh
    • C07F7/02
    • C07F7/20
    • The invention relates to a process for treating a composition containing silicon compounds, especially organosilanes and/or inorganic silanes, and at least one extraneous metal and/or a compound containing extraneous metal, wherein the composition is contacted with at least one adsorbent and/or a first filter and then a composition in which the content of the extraneous metal and/or of the compound containing extraneous metal has been reduced is obtained. The invention further relates to the use of organic resins, activated carbon, silicates and/or zeolites and/or else of at least one filter with small pore sizes to reduce the level of the compounds mentioned.
    • 本发明涉及一种处理包含硅化合物,特别是有机硅烷和/或无机硅烷的组合物和至少一种外来金属和/或含有外来金属的化合物的方法,其中所述组合物与至少一种吸附剂和/或 然后获得第一过滤器,然后获得其中外来金属和/或含有外来金属的化合物的含量已经被还原的组合物。 本发明还涉及使用有机树脂,活性炭,硅酸盐和/或沸石和/或至少一种具有小孔径的过滤器以降低所述化合物的含量。
    • 36. 发明申请
    • Process and apparatus for purifying silicon tetrachloride or germanium tetrachloride containing hydrogen compounds
    • 用于纯化含有氢化合物的四氯化硅或四氯化锗的方法和装置
    • US20090020413A1
    • 2009-01-22
    • US11659084
    • 2005-06-10
    • Hanns-Peter PoppRainer NicolaiHartwig RaulederJuergen Lang
    • Hanns-Peter PoppRainer NicolaiHartwig RaulederJuergen Lang
    • B01D3/00
    • C01B33/10778B01J19/088B01J2219/00853B01J2219/0093B01J2219/0809B01J2219/0815B01J2219/083B01J2219/0841B01J2219/0847B01J2219/0849B01J2219/0896C01G17/04
    • The invention relates to a process for the purification's of silicon tetrachloride or germanium tetrachloride contaminated with at least one hydrogen-containing compound, in which the silicon tetrachloride or germanium tetrachloride to be purified is treated in a targeted manner by means of a cold plasma and purified silicon tetrachloride or germanium tetrachloride is isolated from the phase which has been treated in this way. The present invention further relates to an apparatus for carrying out the process of the invention, which comprises a stock and vaporization unit for silicon or germanium tetrachloride (4.1 or 5.1) which is connected via a connecting line with the inlet of the reactor (4.3 or 5.3) with control unit (4.4 or 5.4) for producing the dielectrically hindered discharges whose outlet leads via a pipe either directly or indirectly via at least one further reactor (5.5) to a condensation unit (4.5 or 5.11) with downstream collection vessel (4.6 or 5.12) which is connected via an offtake line (4.6.2 or 5.12.1) to a distillation unit (4.8 or 5.13) and, if appropriate, is equipped with a feed line (4.6.1) to the unit (4.1).
    • 本发明涉及一种用至少一种含氢化合物污染的四氯化硅或四氯化锗的净化方法,其中待冷却的四氯化硅或四氯化锗将以冷等离子体的方式以目标方式进行处理 从已经以这种方式处理的相中分离出四氯化硅或四氯化锗。 本发明还涉及一种用于实施本发明方法的装置,其包括用于硅或四氯化锗(4.1或5.1)的原料和蒸发单元,其通过连接管线与反应器的入口(4.3或 控制单元(4.4或5.4)用于产生介电阻碍排放物,其出口通过管道直接或间接地通过至少一个另外的反应器(5.5)引导到具有下游收集容器(4.6)的冷凝单元(4.5或5.11) 或5.12),其通过出口管线(4.6.2或5.12.1)连接到蒸馏单元(4.8或5.13),并且如果合适的话,配备有到该单元(4.1)的进料管线(4.6.1) 。
    • 39. 发明授权
    • Cleavage of cyclic organosilanes in the preparation of aminofunctional organoalkoxysilanes
    • 在制备氨基官能有机烷氧基硅烷时循环有机硅烷的裂解
    • US06750361B2
    • 2004-06-15
    • US10159122
    • 2002-06-03
    • Frank KropfgansHartwig Rauleder
    • Frank KropfgansHartwig Rauleder
    • C07F700
    • C07F7/1892
    • An aminofunctional organoalkoxysilane of formula I R2N—(CH2)y—Si(OR1)3−nR2n  (I), wherein the R groups bonded to nitrogen are identical or different and each individual R group is hydrogen, an alkyl radical having from 1 to 4 carbon atoms, an aryl radical or an arylalkyl radical, R1 is an alkyl radical having from 1 to 8 carbon atoms or an aryl radical, R2 is an alkyl radical having from 1 to 8 carbon atoms or an aryl radical, y is 2, 3 or 4 and n is 0, 1 or 2, is prepared by a process comprising: reacting a chlorofunctional organoalkoxysilane of formula II Cl—(CH2)y—Si(OR1)3−nR2n  (II), wherein R1, R2, y and n are as defined above, with ammonia or an organic amine of formula III HNR2  (III), wherein the two R groups are identical or different and each is defined as described above; separating organic amine hydrochloride or ammonium chloride by-product which is formed in the reaction; distilling the resulting crude product, thereby preparing an aminofunctional organoalkoxysilane or the product fraction of an aminofunctional organoalkoxysilane; and treating the aminofunctional organoalkoxysilane or the product fraction of an aminofunctional organoalkoxysilane with an alcohol.
    • 在与氮键合的R基团中的式I的氨基官能有机烷氧基硅烷是相同或不同的,每个单独的R基团是氢,具有1至4个碳原子的烷基,芳基或芳基烷基,R 1是烷基 具有1至8个碳原子的基团或芳基,R 2是具有1至8个碳原子的烷基或芳基,y为2,3或4,n为0,1或2,为 通过以下方法制备,该方法包括:使式II的氯官能有机烷氧基硅烷,其中R 1,R 2,y和n如上定义,与氨或式III的有机胺反应,其中两个R基团相同或不同, 定义如上所述;分离在反应中形成的有机胺盐酸盐或氯化铵副产物;蒸馏所得粗产物,从而制备氨基官能有机烷氧基硅烷或氨基官能有机烷氧基硅烷的产物级分; 用醇将氨基官能的有机烷氧基硅烷或氨基官能的有机烷氧基硅烷的产物级分加成。
    • 40. 发明授权
    • Process for preparing vinyl chlorosilanes
    • 制备乙烯基氯硅烷的方法
    • US06291698B1
    • 2001-09-18
    • US09556403
    • 2000-04-24
    • Stefan BadeBernt KesperRobert KoellHartwig RaulederUwe Schoen
    • Stefan BadeBernt KesperRobert KoellHartwig RaulederUwe Schoen
    • C07F708
    • C07F7/122
    • The invention relates to a process for preparing vinyl chlorosilanes, that includes thermally and non-catalytically reacting chlorosilane with vinyl chloride at a temperature of 550 to 700° C. by flowing the chlorosilane and vinyl chloride through a ring-gap space in a ring-gap reactor to produce a reaction gas; the ring-gap space having a cross-sectional area and a volume; and, after the flowing, further reacting, adiabatically, the reaction gas in a second zone to produce a hot reaction gas that contains vinylchiorosilane; wherein the second zone has a cross-sectional area that is greater than the cross-sectional area of the ring-gap space; and wherein the second zone has a volume that is in a ratio to the volume of the ring-gap space of 0.15:1 to 1.5:1. The invention also provides an apparatus for carrying out the above process.
    • 本发明涉及一种制备乙烯基氯硅烷的方法,其包括在550-700℃的温度下使氯代硅烷与氯乙烯进行热和非催化反应,通过使氯代硅烷和氯乙烯通过环 - 间隙反应器产生反应气体; 所述环间隙具有横截面积和体积; 并且在流动之后,绝热地将第二区中的反应气体进行反应,以产生含有乙烯基氯硅烷的热反应气体; 其中所述第二区域具有大于所述环形间隙的横截面面积的横截面面积; 并且其中所述第二区域具有与所述环隙空间的体积的比率为0.15:1至1.5:1的体积。 本发明还提供一种用于执行上述过程的装置。