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31. 发明授权

US07179311B2 Stable olefinic, low sulfur diesel fuels 有权
标题翻译：稳定的烯烃，低硫柴油燃料
公开(公告)号：US07179311B2
公开(公告)日：2007-02-20
申请号：US10355284
申请日：2003-01-31
申请人： Dennis J. O'Rear , John E. Sundberg
发明人： Dennis J. O'Rear , John E. Sundberg
IPC分类号： C10L1/18 , C10L1/22
CPC分类号： C10L1/08 , C10L1/14 , C10L1/1824 , C10L1/1832 , C10L1/1881 , C10L1/19 , C10L1/2222 , C10L1/223
摘要： The present invention relates to a stable blended diesel fuel comprising an olefinic diesel fuel blending stock. The olefinic diesel fuel blending stock of the invention comprises olefins in an amount of 2 to 80 weight percent, non-olefins in an amount of 20 to 98 weight percent wherein the non-olefins are substantially comprised of paraffins, oxygenates in an amount of at least 0.012 weight percent and sulfur in an amount of less than 1 ppm. To provide acceptable stability, the blended diesel fuel comprising the olefinic diesel fuel blending stock comprises a sulfur-free antioxidant. The blended diesel fuel comprising the olefinic diesel fuel blending stock and sulfur-free antioxidant added has a peroxide content of less than 5 ppm when stored at 60° C. for 4 weeks. The present invention also relates to processes for making the stable blended diesel fuel and olefinic diesel fuel blending stocks as defined above.
摘要翻译：本发明涉及包含烯烃柴油混合原料的稳定混合柴油燃料。本发明的烯烃柴油混合原料包含2至80重量％的烯烃，其量为20至98重量％的非烯烃，其中非烯烃基本上由链烷烃组成，含氧化合物的量为至少0.012重量％和小于1ppm的硫。为了提供可接受的稳定性，包含烯烃柴油混合原料的混合柴油包含无硫抗氧化剂。包含烯烃柴油混合原料和无硫氧化物的混合柴油燃料在60℃下储存4周时的过氧化物含量小于5ppm。本发明还涉及如上定义的制备稳定的混合柴油和烯烃柴油混合原料的方法。

32. 发明授权

US07033552B2 Upgrading Fischer-Tropsch and petroleum-derived naphthas and distillates 失效
公开(公告)号：US07033552B2
公开(公告)日：2006-04-25
申请号：US10059224
申请日：2002-01-31
申请人： Dennis J. O'Rear , Lawrence W. Jossens
发明人： Dennis J. O'Rear , Lawrence W. Jossens
IPC分类号： F28D21/00 , B01J8/00
CPC分类号： C10G2/32 , B01J23/888 , C10G65/00 , C10G65/16 , C10G69/08
摘要： A process for upgrading at least one of a Fischer-Tropsch naphtha and a Fischer-Tropsch distillate to produce at least one of a gasoline component, a distillate fuel or a lube base feedstock component. The process includes reforming a Fischer-Tropsch naphtha to produce hydrogen by-product and a gasoline component with a research octane rating of at least about 80. The process further includes upgrading a Fischer-Tropsch distillate using the hydrogen by-product to produce a distillate fuel and/or a lube base feedstock component.

33. 发明授权

US06824574B2 Process for improving production of Fischer-Tropsch distillate fuels 有权
标题翻译：改进费 - 托馏分燃料生产的方法
公开(公告)号：US06824574B2
公开(公告)日：2004-11-30
申请号：US10267444
申请日：2002-10-09
申请人： Dennis J. O'Rear , Thomas Van Harris , Cong-Yan Chen
发明人： Dennis J. O'Rear , Thomas Van Harris , Cong-Yan Chen
IPC分类号： C10L118
CPC分类号： C10L1/026
摘要： Olefins and alcohols present in Fischer-Tropsch light naphthas are converted to dialkyl ethers of the formula: R—O—R′ where R and R′ are each primarily non-tertiary alkyl groups of more than four carbon atoms, via hydration of the olefins to alcohols followed by dehydration of the alcohols. Ethers may also form by direct reaction of olefins and alcohols. The ethers are separated from the remaining paraffins in the naphtha by distillation and added in an amount of 1-25 wt. % to paraffinic mid-distillate fuel components obtained by hydrotreating a Fischer-Tropsch product. The properties of the distillate fuel components such as lubricity and seal swell are improved by the dialkyl ethers. The removal of olefins and alcohols from the naphthas reduces refining and lead to a more salable product.
摘要翻译：存在于费 - 托轻石脑油中的烯烃和醇转化为下式的二烷基醚：ROR'，其中R和R'各自主要是具有四个以上碳原子的非叔烷基，通过将烯烃水合成醇，醇的脱水。醚也可以通过烯烃和醇的直接反应形成。通过蒸馏将醚与石脑油中的剩余链烷烃分离，并以1-25重量％的量加入。％对通过加氢处理费 - 托产物而获得的链烷烃中间馏分燃料组分。通过二烷基醚改善馏出物燃料组分的性质，如润滑性和密封膨胀。从石脑油中除去烯烃和醇可以减少精炼并导致更可销售的产品。

34. 发明授权

US06822006B1 Methods of controlling the temperature of an exothermic reaction 有权
标题翻译：控制放热反应温度的方法
公开(公告)号：US06822006B1
公开(公告)日：2004-11-23
申请号：US10613594
申请日：2003-07-02
申请人： Dennis J. O'Rear , Charles L. Kibby
发明人： Dennis J. O'Rear , Charles L. Kibby
IPC分类号： C07C2700
CPC分类号： C10G2/342 , B01J8/22 , B01J2208/00061 , B01J2208/00256 , B01J2208/00274
摘要： Novel methods of controlling the temperature of an exothermic reaction are disclosed. Such methods are particularly applicable to a Fischer-Tropsch synthesis reaction, and comprise removing a vapor phase product from the Fischer-Tropsch reactor, condensing at least a portion of the vapor phase product to form a volatilizable liquid, and injecting at least a portion of the volatilizable liquid into the reactor, wherein the volatilizable liquid comprises hydrocarbons that are in the highest boiling point range of the vapor phase product that is removed from the reactor.
摘要翻译：公开了控制放热反应温度的新方法。这种方法特别适用于费 - 托合成反应，并且包括从费 - 托反应器中除去气相产物，将至少一部分气相产物冷凝以形成可挥发液体，并注入至少一部分可挥发的液体进入反应器，其中可挥发液体包括处于从反应器中除去的气相产物的最高沸点范围内的烃。

35. 发明授权

US06806237B2 Lube base oils with improved stability 有权
标题翻译：润滑油基础油具有改进的稳定性
公开(公告)号：US06806237B2
公开(公告)日：2004-10-19
申请号：US09966298
申请日：2001-09-27
申请人： Dennis J. O'Rear
发明人： Dennis J. O'Rear
IPC分类号： C10M11100
CPC分类号： C10G2/30 , C10M101/02 , C10M107/00 , C10M111/02 , C10M2203/1006 , C10M2205/173 , C10N2230/10 , C10N2230/43 , C10N2240/10
摘要： A lube base oil comprising a synthetic lube base oil, such as a Fischer Tropsch-derived component, and a non-synthetic lube base oil is defined that has improved stability to oxidation both during storage and during use in engines or other applications, even in the substantial absence of anti-oxidant additives and oxidation promoters.
摘要翻译：定义了包含合成润滑油基础油如费 - 托衍生组分和非合成润滑油基础油的润滑油基础油，在储存和使用期间在发动机或其他应用中具有改善的氧化稳定性，即使在基本上没有抗氧化添加剂和氧化促进剂。

36. 发明授权

US06806087B2 Use of microchannel reactors in combinatorial chemistry 有权
标题翻译：在组合化学中使用微通道反应器
公开(公告)号：US06806087B2
公开(公告)日：2004-10-19
申请号：US10156164
申请日：2002-05-28
申请人： Charles L. Kibby , Dennis J. O'Rear , Georgieanna L. Scheuerman
发明人： Charles L. Kibby , Dennis J. O'Rear , Georgieanna L. Scheuerman
IPC分类号： G01N3110
CPC分类号： G01N31/10 , B01J19/0046 , B01J19/0093 , B01J2219/00279 , B01J2219/00585 , B01J2219/00698 , B01J2219/00702 , B01J2219/00745 , B01J2219/00747 , B01J2219/00835 , B01J2219/00858 , B01J2219/0086 , B01J2219/00891 , B01J2219/00952 , C40B30/08 , C40B40/18 , C40B60/14
摘要： Methods for discovering optimum catalysts and/or reaction conditions for performing endo-or exothermic reactions, in particular gas-to-liquid reactions, are disclosed. A combinatorial approach is used to identify optimum catalysts and/or reaction conditions for performing the reactions. The reactions are performed in the channels of a microchannel reactor. These results can be used directly to optimize large scale reactions performed in a plurality of microchannel reactors, or can be correlated to useful catalysts and reaction conditions for use in large scale reactors by taking into consideration the heat transfer effects in the microchannel reactor and the large scale reactor. The method can advantageously be used to generate a database of combinations of catalyst systems and/or reaction conditions which provide various product streams, such that as market conditions vary and/or product requirements change, conditions suitable for forming desired products can be identified with little or no downtime. The catalysts can be evaluated using varied reaction conditions, which can provide a) a combinatorial library of product streams and a database including the combination of catalysts and reaction conditions to provide each product stream and/or b) the optimum combination of catalysts and reaction conditions for obtaining a desired product stream.
摘要翻译：公开了用于发现用于进行内反应或放热反应，特别是气 - 液反应的最佳催化剂和/或反应条件的方法。组合方法用于鉴定用于进行反应的最佳催化剂和/或反应条件。反应在微通道反应器的通道中进行。这些结果可以直接用于优化在多个微通道反应器中进行的大规模反应，或者可以通过考虑到在微通道反应器中的传热效应和大型反应器中的大量反应器中的热传递效应而与用于大规模反应器的有用的催化剂和反应条件相关联规模反应堆。该方法可以有利地用于产生提供各种产物流的催化剂体系和/或反应条件的组合的数据库，使得随着市场条件变化和/或产品需求的变化，可以很少地识别适合于形成所需产品的条件或不停机。可以使用不同的反应条件来评估催化剂，其可以提供a）产物流的组合文库和包括催化剂和反应条件的组合的数据库，以提供每种产物流和/或b）催化剂和反应条件的最佳组合以获得所需的产品流。

37. 发明授权

US06541524B2 Method for transporting Fischer-Tropsch products 有权
公开(公告)号：US06541524B2
公开(公告)日：2003-04-01
申请号：US10011501
申请日：2001-11-13
申请人： Dennis J. O'Rear , March R. Buetzow
发明人： Dennis J. O'Rear , March R. Buetzow
IPC分类号： C07C2700
CPC分类号： C10G2/32 , C10G73/00 , C10L1/04
摘要： Facilities to convert natural gas into syncrude often are located at remote sites. At these sites and in their surrounding communities there exists demand for salable products: gasoline, distillate fuels, solvents, lubricants, etc. While it would be possible to produce these products from syncrude, the construction of such production facilities would be very expensive, and their operation would be difficult at the remote site. Fischer-Tropsch syncrude will be waxy and will also contain volatile components, complicating the shipping of both Fischer-Tropsch products from remote production sites to developed sites and salable products from developed sites to remote sites. This invention describes a safe process to both transport Fischer-Tropsch syncrude from the remote site to the developed site and supply salable products from the developed site to the remote site.

38. 发明授权

US06359018B1 Process for upflow fixed-bed hydroprocessing of fischer-tropsch wax 有权
标题翻译：费托蜡的上流固定床加氢处理工艺
公开(公告)号：US06359018B1
公开(公告)日：2002-03-19
申请号：US09698392
申请日：2000-10-27
申请人： Dennis J. O'Rear , Krishniah Parimi , Richard O. Moore, Jr.
发明人： Dennis J. O'Rear , Krishniah Parimi , Richard O. Moore, Jr.
IPC分类号： C07C2700
CPC分类号： C10G49/00
摘要： An integrated process for producing a liquid hydrocarbon stream from Fischer-Tropsch hydrocarbon product without having to remove particulate contaminants such as catalyst fines from hot Fischer-Tropsch wax is disclosed. The process involves performing Fischer-Tropsch synthesis, preferably under conditions which favor formation of wax and heavy products (i.e., using a catalyst with high chain growth probabilities), and obtaining a waxy heavy fraction including particulate contaminants. The fraction is subjected to hydroprocessing conditions, preferably upflow hydroprocessing conditions, using a catalyst bed which, through judicious selection of hydroprocessing catalysts and/or flow conditions, permits passage of the particulate contaminants. The particulates are then removed from the upgraded liquid product, for example by filtration, distillation and/or centrifugation. Removal of the particulate contaminants from the upgraded liquid hydrocarbon products is significantly easier than removing the particulates from the unprocessed waxy heavy products.
摘要翻译：公开了一种用于从费 - 托烃产物生产液态烃流的综合方法，而不必从热的费托蜡中除去诸如催化剂细粒的微粒污染物。该方法包括进行费 - 托合成，优选在有利于形成蜡和重产物的条件下（即，使用具有高链生长概率的催化剂），并获得包括颗粒污染物的蜡质重馏分。使用催化剂床进行加氢处理条件，优选上流加氢处理条件，催化剂床通过明智选择加氢处理催化剂和/或流动条件允许颗粒污染物通过。然后将微粒从升级的液体产物中除去，例如通过过滤，蒸馏和/或离心。从升级的液体烃产品中除去颗粒污染物比从未加工的蜡质重质产物中除去颗粒更容易。

39. 发明授权

US5955641A Method of making dimethylnaphthalenes 失效
标题翻译：制造二甲基萘的方法
公开(公告)号：US5955641A
公开(公告)日：1999-09-21
申请号：US86295
申请日：1998-05-28
申请人： Cong-Yan Chen , William L. Schinski , Dennis J. O'Rear , Thomas V. Harris
发明人： Cong-Yan Chen , William L. Schinski , Dennis J. O'Rear , Thomas V. Harris
IPC分类号： C07C2/66 , C07C2/68 , C07C5/367 , C07C5/41 , C07C15/24 , C10G57/00 , C07C1/00 , C07C2/70 , C10G35/06
CPC分类号： C07C15/24 , C07C2/66 , C07C2/68 , C07C5/415 , C07C2521/16 , C07C2523/08 , C07C2523/14 , C07C2523/36 , C07C2523/74 , C07C2527/126 , C07C2529/06 , C07C2529/08 , C07C2529/18 , C07C2529/40 , C07C2529/50 , C07C2529/65 , C07C2529/70 , C10G2400/30
摘要： The method of the invention includes making dimethyinaphthalenes by first contacting, in an alkylation zone, at alkylation conditions, a toluene-containing stream with a pentene-containing stream in the presence of an acid alkylation catalyst. At least a portion of the toluene and pentenes react to form pentyltoluenes. At least a portion of the pentyltoluenes is then contacting in a reforming zone with reforming catalyst, at reforming conditions. At least a portion of the pentyltoluenes is converted to dimethylnaphthalenes.
摘要翻译：本发明的方法包括通过在烷基化区，在烷基化条件下，在酸性烷基化催化剂的存在下，将含甲苯的物流与含戊烯的物流接触来制备二甲基萘。至少一部分甲苯和戊烯反应形成戊基甲苯。在重整条件下，至少一部分戊基甲苯然后在重整区与重整催化剂接触。将至少一部分戊基甲苯转化为二甲基萘。

40. 发明授权

US4390413A Hydrocarbon upgrading process 失效
标题翻译：碳氢化合物升级过程
公开(公告)号：US4390413A
公开(公告)日：1983-06-28
申请号：US194729
申请日：1980-10-06
申请人： Dennis J. O'Rear , Jerome F. Mayer
发明人： Dennis J. O'Rear , Jerome F. Mayer
IPC分类号： B01J29/40 , C10G45/64 , C10G65/12 , C10G69/08 , C10G69/10 , C10G11/05 , C10G45/02
CPC分类号： C10G45/64 , B01J29/40 , C10G65/12 , C10G69/08 , C10G69/10 , B01J2229/26 , B01J2229/42
摘要： A petroleum distillate feed is upgraded and an olefinic product is produced by contacting the feed with ZSM-5-type zeolite at (1) a temperature in the 500.degree. F.-800.degree. F. range; (2) a pressure below about 13 atmospheres gauge; and (3) an LHSV in the 0.1-15 V/V/Hr range.
摘要翻译：石油馏分进料升级，通过在（1）500°F-800°F范围的温度下使进料与ZSM-5型沸石接触来生产烯烃产物; （2）压力低于约13大气压表; 和（3）0.1-15 V / V / Hr范围内的LHSV。

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