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31. 发明授权

US4041186A Flavoring with (2-methyl-3-furyl)(methylthiomethyl) sulfide 失效
标题翻译：（2-甲基-3-呋喃基）（甲硫基甲基）硫醚调味
公开(公告)号：US4041186A
公开(公告)日：1977-08-09
申请号：US740947
申请日：1976-11-11
申请人： William J. Evers , Howard H. Heinsohn, Jr. , Manfred Hugo Vock , Christopher Giacino
发明人： William J. Evers , Howard H. Heinsohn, Jr. , Manfred Hugo Vock , Christopher Giacino
IPC分类号： A23L27/20 , A23L1/226
CPC分类号： A23L27/2054 , A23L27/2052
摘要： Novel 3-furyl sulfides having the formula: ##STR1## wherein R.sub.1 is methylthiomethyl, R.sub.2 is methyl, and R.sub.3 is hydrogen, such 3-furyl sulfide being useful in modifying or enhancing the organoleptic properties of foodstuffs (e.g., taste and/or aroma).
摘要翻译：具有下式的新颖的3-呋喃基硫醚：其中R1是甲硫基甲基，R2是甲基，R3是氢，这种3-呋喃基硫化物可用于改变或增强食品的感官特性（例如味道和/或香味）。

32. 发明授权

US4031256A Foodstuff flavor compositions comprising 3-furyl alkyl sulfides and processes 失效
标题翻译：包含3-呋喃基烷基硫化物的食品风味组合物和方法
公开(公告)号：US4031256A
公开(公告)日：1977-06-21
申请号：US723531
申请日：1976-09-15
申请人： William J. Evers , Howard H. Heinsohn, Jr. , Bernard J. Mayers
发明人： William J. Evers , Howard H. Heinsohn, Jr. , Bernard J. Mayers
IPC分类号： A23L27/20 , C07D307/64 , A23L1/231
CPC分类号： C07D307/64 , A23L27/2052
摘要： 3-Furyl alkyl sulfides having the formula: ##STR1## wherein R.sub.1 is C.sub.1 -C.sub.5 lower alkyl and R.sub.2 is selected from the group consisting of hydrogen and methyl, are described as being useful in altering, modifying or enhancing the organoleptic properties of foodstuffs.
摘要翻译：具有下式的3-呋喃基烷基硫化物：其中R1是C1-C5低级烷基，R2选自氢和甲基，被描述为可用于改变，改进或增强食品的感官特性。

33. 发明授权

US4024289A Flavoring with .alpha.-oxy(oxo)mercaptans 失效
标题翻译：用{60-氧（氧代）硫醇调味
公开(公告)号：US4024289A
公开(公告)日：1977-05-17
申请号：US723535
申请日：1976-09-15
申请人： William J. Evers , Howard H. Heinsohn, Jr. , Manfred Hugo Vock
发明人： William J. Evers , Howard H. Heinsohn, Jr. , Manfred Hugo Vock
IPC分类号： A23L27/20 , A23L27/29 , C07C45/63 , C07C49/16 , A23L1/235
CPC分类号： C07C323/22 , A23L27/2022 , A23L27/203 , A23L27/29 , C07C2101/20
摘要： The fruity flavor of a foodstuff is augmented or enhanced by the use of one or more .alpha.-oxy(oxo)mercaptans selected from the group consisting of:3-mercapto-4-heptanol;4-mercapto-5-nonanol;4-mercapto-5-nonanone;3-mercapto-2,6-dimethyl-4-heptanone;2-mercaptocyclododecanone-1; and2-mercapto-3-pentanoneThese compounds augment or enhance the green, grapefruit, fruity, buchu leaf oil-like, floral, green vegetable and/or minty aromas and grapefruit-like, green, citrus, bitter, lemon, buchu leaf oil-like, blackcurrant-like, green vegetable-like, and/or cooling notes of food flavors.
摘要翻译：通过使用一种或多种选自以下的α-氧代（氧代）硫醇来增强或增强食品的果味：

34. 发明授权

US3985908A 3-Furyl sulfides and foodstuff flavor compositions comprising same 失效
标题翻译： 3-呋喃基硫化物和包含其的食品香料组合物
公开(公告)号：US3985908A
公开(公告)日：1976-10-12
申请号：US666351
申请日：1976-03-12
申请人： William J. Evers , Howard H. Heinsohn, Jr. , Manfred Hugo Vock , Christopher Giacino
发明人： William J. Evers , Howard H. Heinsohn, Jr. , Manfred Hugo Vock , Christopher Giacino
IPC分类号： A23L27/20 , A23L1/226 , A23L1/231
CPC分类号： A23L27/2054 , A23L27/2052
摘要： Novel 3-furyl sulfides having the formula: ##SPC1##Wherein R.sub.2 and R.sub.2 are each selected from the group consisting of hydrogen and methyl; at least one of R.sub.2 and R.sub.3 being methyl, such 3-furyl sulfides being useful in modifying or enhancing the organoleptic properties of foodstuffs (e.g. taste and/or aroma).
摘要翻译：具有下式的新型3-呋喃基硫醚：

35. 发明授权

US4749681A Polyalkyl-substituted oxocycloheptane derivatives, organoleptic uses thereof and processes for preparing same 失效
标题翻译：聚烷基取代的氧代环庚烷衍生物，其感官用途及其制备方法
公开(公告)号：US4749681A
公开(公告)日：1988-06-07
申请号：US53393
申请日：1986-05-22
申请人： William J. Evers , Howard H. Heinsohn, Jr.
发明人： William J. Evers , Howard H. Heinsohn, Jr.
IPC分类号： C07C35/20 , C07C45/51 , C07C45/62 , C07C45/63 , C07C45/65 , C07C45/69 , C07C49/413 , C07C49/607 , C11B9/00 , C11D3/50 , A61K7/46
CPC分类号： C11D3/50 , C07C35/20 , C07C45/511 , C07C45/62 , C07C45/65 , C07C45/69 , C07C49/413 , C07C49/607 , C11B9/0038
摘要： Described are polyalkyl-substituted oxocycloheptane derivatives defined according to the structure: ##STR1## wherein X represents one of the moieties: ##STR2## wherein one of the dashed lines is a carbon-carbon double bond and the other of the dashed lines is a carbon-carbon single bond; or both dashed lines are carbon-carbon single bonds; wherein R.sub.1 and R.sub.2 represents hydrogen or lower alkyl with the proviso that when the dashed line at the 4-5 position is a double bond, R.sub.2 is hydrogen and when the dashed line at the 3-4 position is a double bond, R.sub.1 is hydrogen; wherein R.sub.4 represents C.sub.1 -C.sub.4 lower alkyl; and wherein Y represents chloro or bromo.Also described are the organoleptic uses of said polyalkyl-substituted oxocycloheptane derivatives in augmenting or enhancing the aroma of perfume compositions, colognes and perfumed articles including solid or liquid aninonic, cationic, nonionic or zwitterionic detergents, fabric softener articles, fabric softener compositions and perfumed polymers.Also described are the processes for preparing said polyalkyl-substituted oxocycloheptane derivatives.
摘要翻译：描述的是根据以下结构定义的聚烷基取代的氧代环庚烷衍生物：其中X表示其中一个部分：其中一条虚线是碳 - 碳双键，另一条虚线是碳碳单键; 或两条虚线都是碳 - 碳单键; 其中R 1和R 2表示氢或低级烷基，条件是当4-5位的虚线是双键时，R 2是氢，当3-4位的虚线是双键时，R 1是氢 ; 其中R 4表示C 1 -C 4低级烷基; 并且其中Y表示氯或溴。还描述了所述多烷基取代的氧代环庚烷衍生物在增强或增强香料组合物，古龙水和加香制品的香气中的感官应用，包括固体或液体的无声，阳离子，非离子或两性离子洗涤剂，织物柔软剂制品，织物柔软剂组合物和加香聚合物。还描述了制备所述多烷基取代的氧代环庚烷衍生物的方法。

36. 发明授权

US4451392A Synthesis of triconjugated dienones and novel intermediates used in said process 失效
标题翻译：三氯联二烯酮的合成和所述方法中使用的新型中间体
公开(公告)号：US4451392A
公开(公告)日：1984-05-29
申请号：US431268
申请日：1982-09-30
申请人： William J. Evers , Gilbert Stork , Barja D. Mookherjee , Howard H. Heinsohn, Jr.
发明人： William J. Evers , Gilbert Stork , Barja D. Mookherjee , Howard H. Heinsohn, Jr.
IPC分类号： C07C45/67 , C07C49/203 , C11B9/00 , C11D3/50 , A61K7/46
CPC分类号： C11D3/50 , C07C45/673 , C07C45/676 , C07C49/203 , C07C67/293 , C07C67/297 , C11B9/0015 , C11B9/0061
摘要： Described is a process for preparing triconjugated dienones defined according to the structure: ##STR1## wherein R.sub.1 represents C.sub.1 -C.sub.8 alkyl, phenyl or phenyl methyl and wherein R.sub.2 represents hydrogen or C.sub.1 -C.sub.5 lower alkyl; and wherein the wavy lines are indicative of a "cis" or a "trans" juxtaposition of the R.sub.2, methyl, acyl or vinyl moieties about one or both of the carbon-carbon double bonds which process involves the reaction of an acyl halide having the structure: ##STR2## (wherein X represents chloro) with a substituted or unsubstituted prenyl ester having the structure: ##STR3## wherein R.sub.3 represents C.sub.1 -C.sub.5 alkyl in the presence of an aluminum chloride catalyst and a methylene dichloride solvent in order to form the novel intermediate genus defined according to the structure: ##STR4## then dehydrohalogenating the compound defined according to the structure: ##STR5## using an alkali metal carbonate and a dimethylformamide solvent in order to form the novel compound genus having the structure: ##STR6## wherein one of the dashed lines represents a carbon-carbon double bond and the other of the dashed lines represents a carbon-carbon single bond; and then dehydroacyloxylating the compound having the structure: ##STR7## in order to form the compound having the structure: ##STR8## the dehydroacyloxylation step taking place in the presence of an alkali metal carbonate and dimethylformamide solvent.
摘要翻译：描述了根据以下结构定义的三结合双酮的方法：其中R 1表示C 1 -C 8烷基，苯基或苯基甲基，并且其中R 2表示氢或C 1 -C 5低级烷基; 并且其中波浪线表示R2，甲基，酰基或乙烯基部分在一个或两个碳 - 碳双键上的“顺式”或“反式”并置，该方法涉及具有结构：其中X表示氯，具有以下结构的取代或未取代的异戊二烯基酯：其中R 3表示C 1 -C 5烷基，在氯化铝催化剂和二氯甲烷溶剂的存在下，形成根据以下结构定义的新型中间体：然后使用碱金属碳酸盐和二甲基甲酰胺溶剂将根据结构定义的化合物脱卤化氢，以形成具有以下结构的新颖化合物：其中虚线中的一条代表碳 - 碳双键，另一条虚线表示碳 - 碳单键; 然后将具有以下结构的化合物脱氢酰化氧化：为了形成具有以下结构的化合物：在碱金属碳酸盐和二甲基甲酰胺溶剂的存在下进行脱氢甲酰氧基化步骤。

37. 发明授权

US4107184A 3-Furyl alkyl disulfides 失效
标题翻译： 3-呋喃基烷基二硫化物
公开(公告)号：US4107184A
公开(公告)日：1978-08-15
申请号：US620353
申请日：1975-10-07
申请人： William J. Evers , Howard H. Heinsohn, Jr. , Manfred Hugo Vock
发明人： William J. Evers , Howard H. Heinsohn, Jr. , Manfred Hugo Vock
IPC分类号： A23K1/16 , A23L1/226 , A23L1/231 , C07D307/64
CPC分类号： C07D307/64 , A23K20/00 , A23L27/20 , A23L27/2052 , A23L27/26
摘要： Novel 3-furyl alkyl disulfides having the formula: ##STR1## wherein R.sub.1 is C.sub.1 -C.sub.7 lower alkyl or C.sub.5 -C.sub.6 cycloalkyl; R.sub.2 and R.sub.3 are each selected from the group consisting of hydrogen and methyl, at least one of R.sub.2 and R.sub.3 being methyl provided that when R.sub.1 is methyl, each of R.sub.2 and R.sub.3 is methyl, such 3-furyl alkyl disulfides being useful in altering, modifying or enhancing the organoleptic properties of foodstuffs.

38. 发明授权

US4083862A .alpha.-Oxy(oxo) sulfides and ethers 失效
标题翻译： {60-氧（氧代）硫醚和醚
公开(公告)号：US4083862A
公开(公告)日：1978-04-11
申请号：US783474
申请日：1977-03-31
申请人： William J. Evers , Howard H. Heinsohn, Jr.
发明人： William J. Evers , Howard H. Heinsohn, Jr.
IPC分类号： C07C45/63 , C07C45/70 , C07C49/175 , C07C49/813 , C07C327/22 , C11B9/00 , C07C153/09
CPC分类号： C07C327/00 , C07C323/00 , C07C45/63 , C07C45/70 , C11B9/0011 , C11B9/0015
摘要： Described are .alpha.-oxy(oxo) sulfides and ethers having the generic structure: ##STR1## wherein X is one of: ##STR2## Z is one of sulfur or oxygen; when R.sub.1 and R.sub.2 are taken separately, R.sub.1 is hydrogen or methyl, and R.sub.2 is methyl; and when R.sub.1 and R.sub.2 are taken together, R.sub.1 and R.sub.2 form phenyl moieties; and Y is one of C.sub.1 -C.sub.4 alkyl, C.sub.3 or C.sub.4 alkenyl, acetyl, methoxycarbonylmethyl, or 1,3-diethylacetonyl.Addition of one or more .alpha.-oxy(oxo) sulfides and ethers to foodstuff flavorings or foodstuffs is indicated to produce the following aroma and flavor characteristics, in the alternative or taken together:AromaGreen/spicey, Sweet, Fruity, Fresh/fruity, Gooseberry, Concord grape, Grape, Almond, Nutty, Cereal-like, Lachrymatory onion-like, Oniony, Green onion-like, Leek, Broccoli-like, Grapefruit, Celery stalk-like, Floral, Rosey, Woody, Blackcurrant, Buchu leaf oil-like, Citronellal-like, Neroli-like, Bergamot-like, Violet leaves-like, Jasmin-like, Melony, Cucumber-like, Green, Vegetable, Sweet/floral.FlavorSpicey, Sweet, Fruity, Milk caramel-like (dulce de leche-like), Gooseberry, Broccoli-like, Nutty, Cereal-like, Oniony, Grape, Concord grape, Citrusy, Grapefruit-like, Green fruit-like, Mandarin-like, Petitgrain-like, Blackcurrant, Minty, Astringent, Coriander-like, Green, Piney, Citronellal-like, Violet leaves-like, Melony, Green fruit-like, Cucumber, Green, Floral, Floral/green, Vegetable, Garlic.With lasting mouthfeel and with, in many cases, an oniony aftertaste. The compounds of our invention are useful in augmenting or enhancing the flavor and aroma nuances of berry flavors, cereal-like flavors, nut flavors, broccoli flavors, onion flavors, citrus flavors (including neroli, bergamot, lime), jasmin flavors, grapefruit flavors, concord grape flavors, blackcurrant flavors, milk caramel flavors (e.g., dulce de leche-like flavors), vegetable flavors, cucumber flavors, celery flavors and spice flavors.Addition of a number of these .alpha.-oxy(oxo)sulfides and ethers in perfumes, colognes or perfumed articles imparts thereto sweet, green, floral, herbal, vegetative, basil-like, minty, melony, grapefruit, fruity and alliaceous aromas with yara, neroli and/or verdima-like nuances.
摘要翻译：描述了具有以下通用结构的α-氧代（氧代）硫化物和醚：其中X是以下之一：Z是硫或氧之一; 当R1和R2分开取代时，R1是氢或甲基，R2是甲基; 当R 1和R 2一起时，R 1和R 2形成苯基部分; Y是C 1 -C 4烷基，C 3或C 4链烯基，乙酰基，甲氧羰基甲基或1,3-二乙基丙酰基之一。

39. 发明授权

US4061796A Uses of .alpha.-oxy(oxo) sulfides and ethers in foodstuffs and flavors for foodstuffs 失效
标题翻译：在食品和食品中使用{60-氧（氧代）硫化物和醚类
公开(公告)号：US4061796A
公开(公告)日：1977-12-06
申请号：US765634
申请日：1977-02-04
申请人： William J. Evers , Howard H. Heinsohn, Jr. , Manfred Hugo Vock
发明人： William J. Evers , Howard H. Heinsohn, Jr. , Manfred Hugo Vock
IPC分类号： A23L27/20 , A23L27/29 , C07C45/63 , C07C45/70 , C07C49/16 , C07C49/175 , A23L1/226 , A23L1/235
CPC分类号： C07C327/00 , A23L27/2022 , A23L27/204 , A23L27/29 , C07C323/00 , C07C45/63 , C07C45/70 , C07C49/16 , C07C49/175
摘要： Processes and compositions are described for use in foodstuff flavors and as foodstuff article aroma and taste augmenting and enhancing materials of at least one .alpha.-oxy(oxo) sulfide and ether having the structure: ##STR1## wherein X is one of: ##STR2## Z is one of sulfur or oxygen; when R.sub.1 and R.sub.2 are taken separately, R.sub.1 is hydrogen or methyl, and R.sub.2 is methyl; and when R.sub.1 and R.sub.2 are taken together, R.sub.1 and R.sub.2 form phenyl moieties; and Y is one of C.sub.1 -C.sub.4 alkyl, C.sub.3 or C.sub.4 alkenyl, acetyl, methoxycarbonylmethyl, or 1,3-diethylacetonyl.The compounds of our invention are useful in augmenting or enhancing the flavor and aroma nuances of berry flavors, cereal-like flavors, nut flavors, broccoli flavors, onion flavors, citrus flavors (including neroli, bergamot, lime), jasmin flavors, grapefruit flavors, concord grape flavors, blackcurrant flavors, milk caramel flavors (e.g., dulce de leche-like flavors), vegetable flavors, cucumber flavors, celery flavors and spice flavors.
摘要翻译：描述了用于食品香料的方法和组合物，以及作为食品制品香气和味道增强和增强至少一种具有以下结构的α-氧代（氧代）硫醚和醚的材料：其中X是以下之一： Z是硫或氧之一; 当R1和R2分开取代时，R1是氢或甲基，R2是甲基; 当R 1和R 2一起时，R 1和R 2形成苯基部分; Y是C 1 -C 4烷基，C 3或C 4链烯基，乙酰基，甲氧羰基甲基或1,3-二乙基丙酰基之一。

40. 发明授权

US4055691A Uses of .alpha.-oxy(oxo) sulfides and ethers in foodstuffs and flavors for foodstuffs 失效
公开(公告)号：US4055691A
公开(公告)日：1977-10-25
申请号：US765775
申请日：1977-02-04
申请人： William J. Evers , Howard H. Heinsohn, Jr. , Manfred Hugo Vock
发明人： William J. Evers , Howard H. Heinsohn, Jr. , Manfred Hugo Vock
IPC分类号： A23L27/20 , A23L27/29 , A23L1/226 , A23L1/235
CPC分类号： A23L27/29 , A23L27/2022
摘要： Processes and compositions are described for use in foodstuff flavors and as foodstuff article aroma and taste augmenting and enhancing materials of at least one .alpha.-oxy(oxo) sulfide and ether having the structure: ##STR1##wherein X is one of: ##STR2## Z is one of sulfur or oxygen; when R.sub.1 and R.sub.2 are taken separately, R.sub.1 is hydrogen or methyl, and R.sub.2 is methyl; and when R.sub.1 and R.sub.2 are taken together, R.sub.1 and R.sub.2 form phenyl moieties; and Y is one of C.sub.1 -C.sub.4 alkyl, C.sub.3 or C.sub.4 alkenyl, acetyl, methoxycarbonylmethyl, or 1,3-diethylacetonyl.The compounds of our invention are useful in augmenting or enhancing the flavor and aroma nuances of berry flavors, cereal-like flavors, nut flavors, broccoli flavors, onion flavors, citrus flavors (including neroli, bergamot, lime), jasmin flavors, grapefruit flavors, concord grape flavors, blackcurrant flavors, milk caramel flavors (e.g., dulce de leche-like flavors), vegetable flavors, cucumber flavors, celery flavors and spice flavors.

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