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31. 发明申请

US20150133687A1 PROCESS FOR PREPARING AN UNSATURATED ALDEHYDE AND/OR AN UNSATURATED CARBOXYLIC ACID 有权
标题翻译：制备不饱和醛和/或不饱和羧酸的方法
公开(公告)号：US20150133687A1
公开(公告)日：2015-05-14
申请号：US14536969
申请日：2014-11-10
申请人： BASF SE
发明人： Josef MACHT , Christian WALSDORFF , Cornelia Katharina DOBNER , Cathrin Alexandra WELKER-NIEUWOUDT , Ulrich HAMMON
IPC分类号： C07C51/25 , B01J23/887 , C07C45/35
CPC分类号： C07C51/252 , B01J23/8876 , C07C45/35 , C07C47/22 , C07C57/04
摘要： An α,β-unsaturated aldehyde and/or an α,β-unsaturated carboxylic acid are prepared by gas phase oxidation of alkene with molecular oxygen over a fixed catalyst bed comprising a bed of hollow cylindrical shaped catalyst bodies having a multimetal oxide active composition. The fixed catalyst bed comprises at least three successive reaction zones; the highest local temperature in the fixed catalyst bed does not occur in the reaction zone closest to the reactor outlet; the highest local temperature in the fixed catalyst bed does not occur in the reaction zone closest to the reactor inlet; and the value WT=(ED−ID)/2 in the reaction zone in which the highest local temperature in the fixed catalyst bed occurs is lower than in the other reaction zones, in which ED is the external diameter and ID is the internal diameter of the shaped catalyst body. The yield of the products of value is enhanced in this way.
摘要翻译：通过在固定的催化剂床上用分子氧气气氧化烯烃制备α，β-不饱和醛和/或α，β-不饱和羧酸，所述催化剂床包含具有多金属氧化物活性的中空圆柱形催化剂体床组成。固定的催化剂床包括至少三个连续的反应区; 在最接近反应器出口的反应区域内不会发生固定催化剂床中最高的局部温度; 固定催化剂床中最高的局部温度不会在最接近反应器入口的反应区中发生; 在固定催化剂床中发生最高局部温度的反应区域中的值WT =（ED-ID）/ 2低于其他反应区域，其中ED为外径，ID为内径的成形催化剂体。以这种方式提高了产品的产量。

32. 发明公开

US20230302432A1 POROUS CATALYST-SUPPORT SHAPED BODY 审中-公开
公开(公告)号：US20230302432A1
公开(公告)日：2023-09-28
申请号：US18011855
申请日：2021-06-25
申请人： BASF SE
发明人： Sung Yeun CHOI , Andrey KARPOV , Christian WALSDORFF , Patrick HUBACH , Hubert WAINDOK , Bernd HINRICHSEN , Gonzalo PRIETO GONZALEZ , Tania RODENAS TORRALBA , Karl C. KHARAS
IPC分类号： B01J21/04 , B01J35/04 , B01J35/10 , B01J35/00 , B01J37/08 , C07D301/10 , B01J37/02
CPC分类号： B01J21/04 , B01J35/002 , B01J35/04 , B01J35/1009 , B01J35/1042 , B01J35/1061 , B01J37/0201 , B01J37/0236 , B01J37/088 , C07D301/10
摘要： A porous shaped catalyst support body comprising at least 85% by weight of alpha-alumina, wherein the support has a total pore volume in the range from 0.5 to 2.0 mL/g as determined by mercury porosimetry, and a pore structure characterized by a geometric tortuosity τ in the range from 1.0 to 2.0; and an effective diffusion parameter η in the range from 0.060 to 1.0; wherein geometric tortuosity τ and effective diffusion parameter η are determined by image analysis algorithms from computer-assisted 3D reconstructions of focused ion beam scanning electron microscope analyses. The structure of the support has a high total pore volume, such that impregnation with a large amount of silver is possible, while the surface area is kept sufficiently high in order to assure optimal dispersion of the catalytically active species, especially metal species. The support has a pore structure that leads to a maximum rate of mass transfer within the support. The invention also relates to a shaped catalyst body for preparation of ethylene oxide by gas phase oxidation of ethylene, comprising at least 15% by weight of silver, based on the total weight of the catalyst, deposited on a porous shaped catalyst support body as described above. The invention further relates to a process for producing the shaped catalyst body, in which a) a porous shaped catalyst support body as described above is impregnated with a silver impregnation solution, preferably under reduced pressure; and the impregnated porous shaped catalyst support body is optionally subjected to drying; and b) the impregnated porous shaped catalyst support body is subjected to a heat treatment; wherein steps a) and b) are optionally repeated. The invention also relates to a process for preparing ethylene oxide by gas phase oxidation of ethylene, comprising the reaction of ethylene and oxygen in the presence of a shaped catalyst body according to claim 11.

33. 发明申请

US20220314209A1 THREE-DIMENSIONAL POROUS CATALYST, CATALYST CARRIER OR ABSORBENT STRUCTURE OF STACKED STRANDS 有权
公开(公告)号：US20220314209A1
公开(公告)日：2022-10-06
申请号：US17626838
申请日：2020-07-16
申请人： BASF SE
发明人： Marco Oskar KENNEMA , Bart MICHIELSEN , Jasper LEFEVERE , Christian WALSDORFF , Fred BORNINKHOF , Florian SCHARF
IPC分类号： B01J35/04 , B01J37/00 , B01J37/16 , B01J20/28 , B33Y80/00 , B33Y10/00 , B33Y40/20 , B22F10/18 , B22F5/10 , B22F10/64 , B33Y40/10
摘要： A three-dimensional porous catalyst, catalyst carrier or absorbent structure of stacked strands of catalyst, catalyst carrier or absorbent material, composed of layers of spaced-apart parallel strands, wherein parallel strands within a layer are arranged in groups of two or more closely spaced-apart, equidistant strands separated by a small distance, wherein the groups of equidistant strands are separated from adjacent strands or adjacent groups of strands by a larger distance.

34. 发明申请

US20220259131A1 A PROCESS FOR THE CONTINUOUS PRODUCTION OF EITHER ACROLEIN OR ACRYLIC ACID AS THE TARGET PRODUCT FROM PROPENE 有权
公开(公告)号：US20220259131A1
公开(公告)日：2022-08-18
申请号：US17628897
申请日：2020-07-14
申请人： BASF SE
发明人： Kazuhiko AMAKAWA , Lukas SCHULZ , Michael BENDER , Klaus Joachim MUELLER-ENGEL , Christian WALSDORFF , Signe UNVERRICHT
IPC分类号： C07C51/145 , C07C45/50 , B01J23/887 , B01J35/02
摘要： A process for the continuous production of either acrolein or acrylic acid as the target product from propene comprising a catalyzed gas phase partial oxidation of propene to yield a product gas containing the target product, transferring the target product in a separating zone from the product gas into the liquid phase and conducting out of the separating zone a stream of residual gas the major portion of which is returned into the partial oxidation and the remaining portion of said stream is purged from the process as off-gas from which synthesis gas can be produced or which can be added to synthesis gas produced otherwise.

35. 发明申请

US20220072524A1 CATALYST, CATALYST CARRIER OR ABSORBENT MONOLITH OF STACKED STRANDS 有权
公开(公告)号：US20220072524A1
公开(公告)日：2022-03-10
申请号：US17291157
申请日：2019-11-04
申请人： BASF SE , VITO NV
发明人： Christian WALSDORFF , Marco Oskar KENNEMA , Miguel Angel ROMERO VALLE , Florian SCHARF , Dirk HENSEL , Juergen ZUEHLKE , Fred BORNINKHOF , Bart MICHIELSEN , Jasper LEFEVERE
IPC分类号： B01J35/04 , B01J35/00 , B01J37/08 , B01J35/06 , B01J37/00 , B01J8/02 , B01J35/10 , B01J35/02
摘要： A three-dimensional porous catalyst, catalyst carrier or absorbent monolith of stacked strands of catalyst, catalyst carrier or absorbent material, composed of alternating layers of linear spaced-apart parallel strands, wherein the strands in alternating layers are oriented at an angle to one another, wherein the distance between inner spaced-apart parallel strands is larger than the distance between outer spaced-apart parallel strands in at least a part of the layers of the monolith.

36. 发明申请

US20210260564A1 METHOD FOR MICROEXTRUSION OF SHAPED BODIES THROUGH A PLURALITY OF MICROEXTRUSION NOZZLES 有权
公开(公告)号：US20210260564A1
公开(公告)日：2021-08-26
申请号：US17270978
申请日：2019-08-07
申请人： BASF SE , VITO NV
发明人： Marco Oskar KENNEMA , Christian WALSDORFF , Bart MICHIELSEN , Jasper LEFEVERE
IPC分类号： B01J20/30 , B01J37/00 , B01J37/08 , B29C64/118 , B29C64/171 , B29C64/209 , B29C64/227 , B33Y10/00
摘要： Process for producing shaped bodies of catalysts, catalyst supports or adsorbents by microextrusion in which a pasty extrusion composition of a shaped body precursor material is extruded through a movable microextrusion nozzle and through movement of the microextrusion nozzle a shaped body precursor is constructed in layerwise fashion and the shaped body precursor is subsequently subjected to a thermal treatment, wherein for construction of each shaped body precursor the pasty extrusion composition is simultaneously extruded through a plurality of microextrusion nozzles.

37. 发明申请

US20190224651A1 MULTIMETAL OXIDE COMPOSITIONS COMPRISING Mo, Bi, Fe AND Cu 审中-公开
公开(公告)号：US20190224651A1
公开(公告)日：2019-07-25
申请号：US16250244
申请日：2019-01-17
申请人： BASF SE
发明人： Kazuhiko AMAKAWA , Christian WALSDORFF , Klaus Joachim MUELLER-ENGEL , Cornelia Katharina DOBNER , Ulrich HAMMON
IPC分类号： B01J23/887 , C01B33/32 , B01J35/00 , B01J35/02 , B01J37/04 , B01J37/08 , C07C45/35
CPC分类号： B01J23/8876 , B01J23/002 , B01J23/8885 , B01J35/008 , B01J35/026 , B01J35/1009 , B01J35/1038 , B01J35/1042 , B01J37/0018 , B01J37/0236 , B01J37/04 , B01J37/08 , B01J37/088 , B01J2523/00 , C01B33/32 , C01G39/006 , C01P2002/50 , C01P2004/30 , C07C45/35 , C07C51/215 , B01J2523/13 , B01J2523/17 , B01J2523/41 , B01J2523/54 , B01J2523/68 , B01J2523/842 , B01J2523/845 , B01J2523/69 , C07C47/22 , C07C57/04
摘要： Multimetal oxide composition comprising Mo, Bi, Fe, Cu and one or more than one of the elements Co and Ni and use thereof.

38. 发明申请

US20170121534A1 USE OF GAMMA IRON(III) OXIDE (GAMMA-FE2O3) CONTAINING PARTICLES FOR THE PREVENTION OF BIOFOULING AND/OR GROWTH OF MICROORGANISMS 审中-公开
公开(公告)号：US20170121534A1
公开(公告)日：2017-05-04
申请号：US15319142
申请日：2015-06-08
申请人： BASF SE
发明人： Rute da Conceicao TAVARES ANDRE , Nico Frederik FISCHER , Patrick HUBACH , Christian WALSDORFF , Christoph SCHWIDETZKY
IPC分类号： C09D5/16 , C09D7/12 , A01N25/02 , A01N59/16 , A01N59/00
CPC分类号： C09D5/1618 , A01N25/02 , A01N59/00 , A01N59/16 , C09D7/67 , C09D7/68 , C11D3/48 , C11D7/20 , A01N25/12
摘要： The present invention relates to the use of gamma iron(III) oxide (γ-Fe2O3) containing particles for the prevention of biofouling and/or growth of microorganisms. Furthermore, it relates to a method for preventing biofouling of a substrate and to a method of imparting biocidal properties to the surface of a substrate.

39. 发明申请

US20160355450A1 PROCESS FOR PREPARING 1,3-BUTADIENE FROM N-BUTENES BY OXIDATIVE DEHYDROGENATION 有权
标题翻译：通过氧化脱氢制备N-丁烯的1,3-丁二烯的方法
公开(公告)号：US20160355450A1
公开(公告)日：2016-12-08
申请号：US15033203
申请日：2014-10-27
申请人： BASF SE
发明人： Philipp GRÜNE , Oliver HAMMEN , Christine SCHMITT , Ragavendra Prasad BALEGEDDE RAMACHANDRAN , Jan Pablo JOSCH , Christian WALSDORFF
IPC分类号： C07C5/48 , B01J23/00 , B01J23/887
CPC分类号： C07C5/48 , B01J23/002 , B01J23/8878 , B01J37/0045 , B01J2523/00 , C07C7/08 , C07C7/11 , C07C2523/04 , C07C2523/18 , C07C2523/26 , C07C2523/28 , C07C2523/745 , C07C2523/75 , C07C2523/887 , C07C11/167 , B01J2523/13 , B01J2523/54 , B01J2523/67 , B01J2523/68 , B01J2523/842 , B01J2523/845
摘要： A process for preparing butadiene from n-butenes, comprising the steps of A) providing an input gas stream a1 comprising n-butenes; B) feeding the input gas stream a1 comprising n-butenes, an oxygenous gas and an oxygenous cycle gas stream a2 into at least one oxidative dehydrogenation zone and oxidatively dehydrogenating n-butenes to butadiene, giving a product gas stream b comprising butadiene, unconverted n-butenes, steam, oxygen, low-boiling hydrocarbons and high-boiling secondary components, with or without carbon oxides and with or without inert gases; Ca) cooling the product gas stream b and optionally at least partly removing high-boiling secondary components and steam, giving a product gas stream b′, Cb) compressing and cooling the product gas stream b′ in at least one compression and cooling stage, giving at least one aqueous condensate stream c1 and one gas stream c2 comprising butadiene, n-butenes, steam, oxygen and low-boiling hydrocarbons, with or without carbon oxides and with or without inert gases, Da) absorbing the C4 hydrocarbons comprising butadiene and n-butenes in an aromatic hydrocarbon solvent as an absorbent and removing uncondensable and low-boiling gas constituents comprising oxygen, low-boiling hydrocarbons, any carbon oxides, aromatic hydrocarbon solvent and any inert gases as gas stream d2 from the gas stream c2, giving an absorbent stream laden with C4 hydrocarbons and the gas stream d2, and then desorbing the C4 hydrocarbons from the laden absorbent stream, giving a C4 product gas stream d1, Db) at least partly recycling the gas stream d2 as cycle gas stream a2 into the oxidative dehydrogenation zone, wherein the content of aromatic hydrocarbon solvent in the cycle gas stream a2 is limited to less than 1% by volume.

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