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31. 发明授权

US08957269B2 Method for producing olefinic monomers from bio oil 有权
标题翻译：从生物油生产烯烃单体的方法
公开(公告)号：US08957269B2
公开(公告)日：2015-02-17
申请号：US13146857
申请日：2010-01-29
申请人： Ali Harlin , Tapani Penttinen , Jari Räsänen , Olli Aaltonen
发明人： Ali Harlin , Tapani Penttinen , Jari Räsänen , Olli Aaltonen
IPC分类号： C10G11/02 , C10G51/02 , C07C11/02 , C07C11/04 , C07C11/06 , C10G9/00 , C10G3/00 , C10G9/36
CPC分类号： C10G51/02 , C07C11/02 , C07C11/04 , C07C11/06 , C10G3/46 , C10G3/50 , C10G3/54 , C10G9/00 , C10G9/36 , C10G11/02 , C10G2300/1014 , C10G2300/807 , C10G2400/20 , Y02P30/42
摘要： The invention relates to a method of producing olefinic monomers for the production of a polymer. The invention particularly relates to the production of tall oil-based biopolymers, such as polyolefins. In the stages of the method bio oil, with a content of over 50% of fatty acids of tall oil and no more than 25% of resin acids of tall oil, and hydrogen gas are fed into a catalyst bed (7); the oil is catalytically deoxygenated in the bed by hydrogen; the flow exiting the bed is cooled down and divided into a hydrocarbon-bearing liquid phase (10) and a gas phase; and the hydrocarbon-bearing liquid (13) is subjected to steam cracking (4) to provide a product containing polymerizing olefins. The deoxygenation in the bed can be followed by a catalytic cracking or, with a suitable catalyst, the deoxygenation and cracking can be simultaneous. The separated hydrogen-bearing gas phase can be circulated in the process.
摘要翻译：本发明涉及生产用于生产聚合物的烯烃单体的方法。本发明特别涉及妥尔油基生物聚合物如聚烯烃的生产。在方法生物油的阶段，含量超过50％的妥尔油的脂肪酸和不超过25％的妥尔油的树脂酸，并将氢气进料到催化剂床（7）中; 油通过氢气在床中催化脱氧; 离开床的流被冷却并分成含烃液相（10）和气相; 并对含烃液体（13）进行蒸汽裂化（4）以提供含有聚合烯烃的产物。床中的脱氧可能是催化裂化，或者使用合适的催化剂，脱氧和裂解可以同时进行。分离的含氢气相可以在该过程中循环。

32. 发明授权

US08747612B2 Process for the production of microfibrillated cellulose in an extruder and microfibrillated cellulose produced according to the process 有权
标题翻译：在挤出机中生产微纤化纤维素的方法和根据该方法生产的微纤化纤维素
公开(公告)号：US08747612B2
公开(公告)日：2014-06-10
申请号：US13503871
申请日：2010-10-26
申请人： Isto Heiskanen , Ali Harlin , Kaj Backfolk , Risto Laitinen
发明人： Isto Heiskanen , Ali Harlin , Kaj Backfolk , Risto Laitinen
IPC分类号： D21H11/20 , D21H11/18 , D21C1/08 , D21C5/00 , C08B15/08
CPC分类号： D21H11/18 , D21H11/20
摘要： The present invention relates to a process for the production of microfibrillated cellulose wherein the process comprises the steps of, providing a slurry comprising fibers, adding the slurry to an extruder, treating the slurry in the extruder so that the fibers are defibrillated and microfibrillated cellulose is formed. The invention further relates to a microfibrillated cellulose produced.
摘要翻译：本发明涉及一种生产微纤化纤维素的方法，其中该方法包括以下步骤：提供包含纤维的浆料，将浆料加入到挤出机中，处理挤出机中的浆料，使纤维脱纤维和微纤化纤维素形成。本发明还涉及生产的微纤化纤维素。

33. 发明申请

US20130178650A1 HYDROGEN TREATMENT OF IMPURE TALL OIL FOR THE PRODUCTION OF AROMATIC MONOMERS 有权
标题翻译：用于生产芳族单体的不饱和油的氢处理
公开(公告)号：US20130178650A1
公开(公告)日：2013-07-11
申请号：US13701664
申请日：2011-06-03
申请人： Ali Harlin , Jari Räsänen , Tapani Penttinen
发明人： Ali Harlin , Jari Räsänen , Tapani Penttinen
IPC分类号： C10G3/00 , C07C51/16
CPC分类号： C10G3/50 , B01J21/16 , B01J23/883 , B01J23/8892 , B01J29/40 , B01J35/0006 , B01J37/20 , C07C1/2078 , C07C4/06 , C07C51/16 , C07C51/265 , C07C2521/04 , C07C2521/16 , C07C2523/882 , C07C2523/883 , C07C2529/14 , C07C2529/40 , C08G63/183 , C10G3/46 , C10G3/49 , C10G3/54 , C10G45/08 , C10G45/12 , C10G2300/1014 , C10G2400/30 , Y02P20/52 , Y02P30/20 , C07C63/26 , C07C15/04 , C07C15/06 , C07C15/08
摘要： A method of manufacturing aromatic hydrocarbons, which are suitable for the production of terephthalic acid, from tall oil-based raw material. According to the invention, the raw material that contains tall oil or its fraction is catalytically deoxygenated with hydrogen, and one or more aromatic hydrocarbons that can be converted into terephthalic acid are separated from the deoxygenated reaction yield. The deoxygenation catalyst is a NiMo catalyst and, in addition, a cracking catalyst can be used, such as an acidic zeolite catalyst. The separated hydrocarbon can be p-xylene, o-xylene or p-cymene. According to the invention, these can be converted by oxidation and, when needed, by a re-arrangement reaction into terephthalic acid that is suitable for the source material of the manufacture of bio-based polyethylene terephthalate.
摘要翻译：从妥尔油基原料制备适于生产对苯二甲酸的芳烃的方法。根据本发明，含有妥尔油或其馏分的原料用氢催化脱氧，可将一种或多种可转化成对苯二甲酸的芳烃与脱氧反应产率分离。脱氧催化剂是NiMo催化剂，另外还可以使用裂化催化剂，例如酸性沸石催化剂。分离的烃可以是对二甲苯，邻二甲苯或对甲基异丙基苯。根据本发明，这些可以通过氧化，并且在需要时通过重新排列反应转化成适用于制造生物基聚对苯二甲酸乙二醇酯的原料的对苯二甲酸。

34. 发明授权

US08371142B2 System and method for manufacturing fibres 有权
标题翻译：制造纤维的系统和方法
公开(公告)号：US08371142B2
公开(公告)日：2013-02-12
申请号：US12526940
申请日：2008-02-13
申请人： Tiina Nypelö , Ali Harlin , Leena Hupa , Fredrik Ollila , Erik Vedel , Risto Widerholm
发明人： Tiina Nypelö , Ali Harlin , Leena Hupa , Fredrik Ollila , Erik Vedel , Risto Widerholm
IPC分类号： C03B37/01
CPC分类号： C03B37/09 , C03B5/021
摘要： The present invention relates to a system for manufacturing fibres comprising a melting furnace, a crucible within said furnace comprising at least one orifice (6) and at least one induction coil (4) for heating the melting furnace and the crucible. In a typical system according to the invention, the crucible comprises at least a first part (1) made of graphite and comprising said at least one orifice (6). The invention also relates to the use of the system as well as to a method for manufacturing fibres and to said fibres.
摘要翻译：本发明涉及一种用于制造纤维的系统，其包括熔化炉，所述炉内的坩埚包括至少一个孔（6）和用于加热熔炉和坩埚的至少一个感应线圈（4）。在根据本发明的典型系统中，坩埚至少包括由石墨制成并包括所述至少一个孔口（6）的第一部分（1）。本发明还涉及该系统的使用以及用于制造纤维和所述纤维的方法。

35. 发明申请

US20060193994A1 Priming and coating process 有权
标题翻译：启动和涂装工艺
公开(公告)号：US20060193994A1
公开(公告)日：2006-08-31
申请号：US11152656
申请日：2005-06-14
申请人： Tapani Penttinen , Kimmo Nevalainen , Isto Heiskanen , Kaj Backfolk , Minna Peltola , Ali Harlin
发明人： Tapani Penttinen , Kimmo Nevalainen , Isto Heiskanen , Kaj Backfolk , Minna Peltola , Ali Harlin
IPC分类号： B05D1/04
CPC分类号： D21H23/50 , D04H3/16 , D21H19/82
摘要： The invention relates to a method for priming a substrate by contacting the substrate with a primer fed from a primer source and depositing the primer on the substrate. Compared to other priming methods, the claimed priming gives better results because the deposition is carried out electrostatically.
摘要翻译：本发明涉及一种通过使底物与从底物源进料的底物接触并将底物沉积在底物上而引发底物的方法。与其他起动方法相比，所要求的起动给出更好的结果，因为沉积是静电地进行的。

36. 发明申请

US20050159564A1 High melt strength polypropylene 失效
标题翻译：高熔体强度聚丙烯
公开(公告)号：US20050159564A1
公开(公告)日：2005-07-21
申请号：US11075488
申请日：2005-03-08
申请人： Paivi Huovinen , Ali Harlin , Pirjo Jaaskelainen , Amir Karbasi , Nina Manner
发明人： Paivi Huovinen , Ali Harlin , Pirjo Jaaskelainen , Amir Karbasi , Nina Manner
IPC分类号： C08J9/00 , C08F2/01 , C08F2/34 , C08F4/645 , C08F4/654 , C08F4/6592 , C08F10/06 , C08F110/06 , C08L1/00 , C08F2/00
CPC分类号： C08F110/06 , Y10S526/905 , C08F2/001 , C08F2500/12 , C08F2500/04 , C08F2500/17
摘要： The present invention concerns a high melt strength propylene polymer or copolymer suitable for manufacturing foams and thermoformed product exhibiting a melt strength of at least 3 g and comprising a high molar mass portion and a low or medium molar mass portion. The polymers are produced by subjecting propylene and optionally other olefins to polymerization in a plurality of polymerization reactors connected in series, employing different amounts of hydrogen as a molar mass modifier in at least two of the reactors, and carrying out the polymerization reaction in the presence of a catalyst system capable of catalyzing the formation of a high molar mass polymerization product having a MFR2 of less than 0.1 g/10 min and a low or medium molar mass polymerization product having a MFR2 of more than 0.5 g/10 min.
摘要翻译：本发明涉及适用于制造泡沫和热成型产品的高熔体强度丙烯聚合物或共聚物，其具有至少3g的熔体强度并且包含高摩尔质量部分和低或中等摩尔质量部分。聚合物是通过使丙烯和任选的其它烯烃在串联连接的多个聚合反应器中进行聚合而制备的，其中在至少两个反应器中使用不同量的氢作为摩尔质量调节剂，并在存在下进行聚合反应的催化剂体系，其能够催化形成具有小于0.1g / 10min的MFR 2的高摩尔质量聚合产物和具有小于0.1g / 10min的低摩尔质量或中等摩尔质量的聚合产物， 2 <0.5，大于0.5g / 10min。

37. 发明授权

US6090893A Polyethylene composition 失效
标题翻译：聚乙烯组成
公开(公告)号：US6090893A
公开(公告)日：2000-07-18
申请号：US875322
申请日：1997-06-16
申请人： Ali Harlin , Aimo Sahila , Veli Kilpelainen , Anders Nymark
发明人： Ali Harlin , Aimo Sahila , Veli Kilpelainen , Anders Nymark
IPC分类号： C08F10/02 , C08L23/04 , C08L23/06 , C08L23/08 , C08L23/00 , C08F255/02
CPC分类号： C08F10/02 , C08L23/06 , C08L2205/02 , C08L2205/03 , C08L23/0815 , C08L2314/02
摘要： The invention relates to polyethylene compositions containing 85-99.5 weight % of component A, which is a linear (co)polymer of ethylene having a bimodal weight distribution, and 0.5-15 weight % of component B having a unimodal molecular weight distribution. Component A is 40-60% by weight of a low molecular weight component (A1) having a weight average molecular weight between 5,000 and 50,000 g/mol, and a molecular weight distribution Mw/Mn between 2.5 and 9 and 60-40% by weight of a high molecular weight component (A2) having a weight average molecular weight between 300,000 and 900,000 g/mol, and a molecular weight distribution M/w/Mn between 4.5 and 12. Component B is a linear ethylene polymer having a molecular weight between 150,000-600,O00 g/mol and an average molecular weight which is higher than the average molecular weight of component (A1) but lower than the average molecular weight of component (A2) and a density controlled within the range of 910-960 kg/m.sup.3. Component B is produced separately from component A by using Ziegler-Natta or metallocene catalysts.
摘要翻译： PCT No.PCT / FI95 / 00669 Sec。 371日期：1997年6月16日 102（e）日期1997年6月16日PCT提交1995年12月8日PCT公布。公开号WO96 / 18677 日期1996年6月20日本发明涉及含有85-99.5重量％组分A的聚乙烯组合物，组分A是具有双峰重量分布的乙烯的线性（共）聚合物，和0.5-15重量％的具有单峰分子体重分布。组分A为重均分子量为5,000〜50,000g / mol，分子量分布Mw / Mn为2.5〜9，分子量分布为60〜40％的低分子量成分（A1）为40〜60重量％重量平均分子量为300,000〜900,000g / mol，分子量分布M / w / Mn为4.5〜12的高分子量组分（A2）的重量。组分B为具有分子量的直链乙烯聚合物 150,000-600，O00g / mol，平均分子量高于组分（A1）的平均分子量但低于组分（A2）的平均分子量，并且密度控制在910-960的范围内 kg / m3。组分B通过使用齐格勒 - 纳塔或茂金属催化剂与组分A分开制备。

38. 发明授权

US5494965A Process for manufacturing olefin polymers and products prepared by the process 失效
标题翻译：通过该方法制备烯烃聚合物和产品的方法
公开(公告)号：US5494965A
公开(公告)日：1996-02-27
申请号：US217510
申请日：1994-03-24
申请人： Ali Harlin , Ulf Palmqvist
发明人： Ali Harlin , Ulf Palmqvist
IPC分类号： C08F10/00 , C08L23/02 , C08L23/04 , C08L23/10 , C08L23/18
CPC分类号： C08F10/00 , C08L23/02 , C08L23/04 , C08L23/06
摘要： A process for manufacturing bimodal olefin polymers and copolymers having a ratio between low molecular weight fractions within the range of 40:60-70:30, by mixing under shear conditions 5-50 percent by weight of a low molecular weight unimodal polyolefin having a molecular weight (Mw) between 15,000-30,000, and 95-50 percent by weight of a bimodal polyolefin having a ratio between low molecular weight fractions and high molecular weight fractions within the range of 30:70-55:45. According to a preferred embodiment, there is used a multi-phase process including a loop reactor followed by a gas-phase reactor, wherein a part of the product coming out from the loop reactor is separated and combined with the bimodal product coming out from the gas-phase reactor.
摘要翻译：通过在剪切条件下混合5-50重量％的具有分子量的低分子量单峰聚烯烃的制备双峰烯烃聚合物和共聚物的方法，其具有在40:60-70:30的范围内的低分子量分数之间的比例重量（Mw）为15,000-30,000和95-50重量％的在30:70-55:45范围内的低分子量级分与高分子量级分之间的比例的双峰聚烯烃。根据优选实施方案，使用多相方法，其包括循环反应器，随后是气相反应器，其中从环管反应器出来的一部分产物被分离并与从该反应器出来的双峰产物组合气相反应器。

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