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31. 发明授权

US09540597B2 Process for the preparation of a powder comprising one or more complexing agent salts 有权
标题翻译：制备包含一种或多种络合剂盐的粉末的方法
公开(公告)号：US09540597B2
公开(公告)日：2017-01-10
申请号：US13501390
申请日：2010-10-11
申请人： Frank Mrzena , Ullrich Menge , Michael Schoenherr , Thomas Heidenfelder
发明人： Frank Mrzena , Ullrich Menge , Michael Schoenherr , Thomas Heidenfelder
IPC分类号： C11D11/02 , C11D3/33 , C11D17/06 , C07C227/42 , C07C229/24 , C11D11/00
CPC分类号： C11D3/33 , C07C227/42 , C07C229/24 , C11D11/0088 , C11D11/02 , C11D17/06
摘要： A process for the preparation of a powder comprising one or more complexing agent salts of the general formula comprises atomizing an aqueous solution comprising the one or more complexing agent salts in the presence of a crystalline fine dust of the same complexing agent salts and a drying step, wherein the concentration of the one or more complexing agent salt is from 10 to 80% by weight, based on the total weight of the aqueous solution, with an upper limit for the average particle diameter of the crystalline fine dust which is lower by at least a factor of 2 than the lower limit of the average particle diameter of the powder obtained after the process, and the fraction of the crystalline fine dust is from 0.1 to 20% by weight, based on the weight of the powder obtained after the process.
摘要翻译：提出了一种制备包含一种或多种通式络合剂盐的粉末的方法，其起始于包含浓度为10-80重量％的一种或多种络合剂盐的水溶液，基于总量在喷雾干燥过程中，包括雾化步骤和干燥步骤，其中所述雾化步骤是通过加入与存在于所述雾化步骤中的相同络合剂盐的结晶细粉末来进行的水溶液或一种或多种与其不同的络合剂盐，结晶细粉尘的平均粒径的上限比所得粉末的平均粒径的下限低至少2倍在该方法之后，以0.1至20重量％的比例，基于该方法后获得的粉末的重量。

32. 发明授权

US08748366B2 Process for the preparation of a spray powder comprising one or more glycine-N,N-diacetic acid derivatives and use of the spray powder for producing compression agglomerates 有权
标题翻译：制备包含一种或多种甘氨酸-N，N-二乙酸衍生物的喷雾粉末和使用喷雾粉末生产压缩附聚物的方法
公开(公告)号：US08748366B2
公开(公告)日：2014-06-10
申请号：US13321713
申请日：2010-05-19
申请人： Frank Mrzena , Michael Schoenherr , Robert Heinz , Thomas Heidenfelder
发明人： Frank Mrzena , Michael Schoenherr , Robert Heinz , Thomas Heidenfelder
IPC分类号： C11D11/02 , C11D3/33 , C11D7/32 , B29B9/00
CPC分类号： C11D3/33 , C11D3/3707 , C11D17/0091 , C11D17/06
摘要： A process for the preparation of a spray-dried powder containing at least one glycine-N,N-diacetic acid compound of a formula MOOC—CHR—N(CH2COOM)2, where R is a C1-12-alkyl and M is an alkali metal, the process including: preparing an aqueous solution containing the glycine-N,N-diacetic acid compound; concurrently passing the aqueous solution and air into a spray-drying apparatus; atomizing the aqueous solution by feeding the aqueous solution onto a rotating disk or by compressing the aqueous solution with a pump to a pressure of ≧20 bar absolute, to obtain fine liquid droplets; and drying the droplets, to obtain the spray-dried powder, where a temperature gradient between the aqueous solution and the air is in a range from 70 to 350° C., and a content of the glycine-N,N-diacetic acid compound in the aqueous solution is ≧84% by weight, based on a total weight of the dry mass.
摘要翻译：一种制备含有至少一种式MOOC-CHR-N（CH 2 COOM）2的甘氨酸-N，N-二乙酸化合物的喷雾干燥粉末的方法，其中R是C1-12烷基，M是碱金属，该方法包括：制备含有甘氨酸-N，N-二乙酸化合物的水溶液; 同时将水溶液和空气通入喷雾干燥装置; 通过将水溶液供给到旋转盘上或通过将水溶液压缩至≥20巴绝对压力来雾化水溶液，以获得精细的液滴; 并干燥液滴，得到喷雾干燥的粉末，其中水溶液和空气之间的温度梯度为70-350℃，甘氨酸-N，N-二乙酸化合物的含量在水溶液中，基于干质量的总重量为≥84重量％。

33. 发明授权

US08420174B2 Polymer composition for corrosion protection 有权
标题翻译：聚合物组合物用于防腐蚀
公开(公告)号：US08420174B2
公开(公告)日：2013-04-16
申请号：US12063937
申请日：2006-08-09
申请人： Alexander Goethlich , Frank Klippel , Gunnar Schornick , Guido Vandermeulen , Helmut Witteler , Thomas Heidenfelder , Markus Hickl , Michael Dornbusch , Konrad Roschmann , Monica Fernandez Gonzalez
发明人： Alexander Goethlich , Frank Klippel , Gunnar Schornick , Guido Vandermeulen , Helmut Witteler , Thomas Heidenfelder , Markus Hickl , Michael Dornbusch , Konrad Roschmann , Monica Fernandez Gonzalez
IPC分类号： B05D3/02
CPC分类号： C23C22/48 , B05D1/007 , B05D7/52 , B05D2202/00 , B05D2350/65 , C08F220/06 , C08F220/28 , C08F230/02 , C08G18/6655 , C08G2150/90 , C08L33/02 , C09D5/082 , C09D123/00 , C09D175/12 , C23C22/53 , C23C22/56 , Y10T428/265 , Y10T428/31699
摘要： The present invention relates to a composition for coating metallic surfaces, comprising a binder component; a corrosion inhibitor polymer based on an ethylenically monocarboxylic and dicarboxylic acid and, if appropriate, further ethylenical monomers, a solvent component, and, if appropriate, crosslinkable components, and also pigment/filler components. The invention further relates to processes for its preparation and also to methods of coating a metallic surface using the composition, to coated metallic surfaces thus obtained, and to the use of the composition as a primer, particularly in coil coating or in atmospheric corrosion control. After drying, the applied layer preferably has a thickness of at least 3.1 μm and is therefore thicker than a typical pretreatment layer.
摘要翻译：本发明涉及一种用于涂覆金属表面的组合物，其包含粘合剂组分; 基于烯键式单羧酸和二羧酸的腐蚀抑制剂聚合物，以及如果合适的话，还可以含有乙烯单体，溶剂组分，如果合适的话，可交联组分以及颜料/填料组分。本发明还涉及其制备方法以及使用该组合物涂覆金属表面的方法，如此获得的涂覆的金属表面以及组合物作为底漆的用途，特别是在卷材涂覆中或在大气腐蚀控制中的用途。干燥后，涂布层的厚度优选为3.1μm以上，因此比典型的预处理层厚。

34. 发明申请

US20120071381A1 PROCESS FOR THE PREPARATION OF A SPRAY POWDER COMPRISING ONE OR MORE GLYCINE-N,N-DIACETIC ACID DERIVATIVES AND USE OF THE SPRAY POWDER FOR PRODUCING COMPRESSION AGGLOMERATES 有权
标题翻译：制备包含一种或多种甘氨酸N，N-二酸衍生物的喷雾粉末的制备方法和喷雾粉生产压缩胶乳的用途
公开(公告)号：US20120071381A1
公开(公告)日：2012-03-22
申请号：US13321713
申请日：2010-05-19
申请人： Frank Mrzena , Michael Schönherr , Robert Heinz , Thomas Heidenfelder
发明人： Frank Mrzena , Michael Schönherr , Robert Heinz , Thomas Heidenfelder
IPC分类号： C11D17/00 , C11D17/06 , B29B9/10 , C07C229/24
CPC分类号： C11D3/33 , C11D3/3707 , C11D17/0091 , C11D17/06
摘要： A process for the preparation of a spray-dried powder containing at least one glycine-N,N-diacetic acid compound of a formula MOOC—CHR—N(CH2COOM)2, where R is a C1-12-alkyl and M is an alkali metal, the process including: preparing an aqueous solution containing the glycine-N,N-diacetic acid compound; concurrently passing the aqueous solution and air into a spray-drying apparatus; atomizing the aqueous solution by feeding the aqueous solution onto a rotating disk or by compressing the aqueous solution with a pump to a pressure of ≧20 bar absolute, to obtain fine liquid droplets; and drying the droplets, to obtain the spray-dried powder, where a temperature gradient between the aqueous solution and the air is in a range from 70 to 350° C., and a content of the glycine-N,N-diacetic acid compound in the aqueous solution is ≧84% by weight, based on a total weight of the dry mass.
摘要翻译：一种制备含有至少一种式MOOC-CHR-N（CH 2 COOM）2的甘氨酸-N，N-二乙酸化合物的喷雾干燥粉末的方法，其中R是C1-12烷基，M是碱金属，该方法包括：制备含有甘氨酸-N，N-二乙酸化合物的水溶液; 同时将水溶液和空气通入喷雾干燥装置; 通过将水溶液供给到旋转盘上或通过将水溶液压缩至≥20巴绝对压力来雾化水溶液，以获得精细的液滴; 并干燥液滴，得到喷雾干燥的粉末，其中水溶液和空气之间的温度梯度为70-350℃，甘氨酸-N，N-二乙酸化合物的含量在水溶液中，基于干质量的总重量为≥84重量％。

35. 发明申请

US20110257431A1 PROCESS FOR PRODUCING SIDE PRODUCT-FREE AMINOCARBOXYLATES 审中-公开
标题翻译：生产无机氨基甲酸酯的方法
公开(公告)号：US20110257431A1
公开(公告)日：2011-10-20
申请号：US13050495
申请日：2011-03-17
申请人： Robert Baumann , Markus Christian Biel , Gordon Brasche , Axel Franzke , Thomas Heidenfelder , Paul Klingelhoefer , Alfred Oftring , Marie Katrin Schroter
发明人： Robert Baumann , Markus Christian Biel , Gordon Brasche , Axel Franzke , Thomas Heidenfelder , Paul Klingelhoefer , Alfred Oftring , Marie Katrin Schroter
IPC分类号： C07C227/02
CPC分类号： C07C227/02 , C07C229/16
摘要： The present invention relates to a process for preparing aminocarboxylates, proceeding from amines, by employing a reaction sequence composed of ethoxylation to amino alcohols and subsequent oxidative dehydrogenation to the corresponding aminocarboxylates, especially the alkali metal or alkaline earth metal salts of the complexing agents MGDA (methylglycinediacetic acid), EDTA (ethylenediaminetetra-acetic acid) and GLDA (glutamic acid diacetic acid) or the free acids thereof.
摘要翻译：本发明涉及一种通过使用由乙氧基化氨基醇组成的反应顺序并随后氧化脱氢至相应的氨基羧酸盐，特别是络合剂MGDA的碱金属或碱土金属盐来制备氨基羧酸盐的方法，甲基甘氨酸二乙酸），EDTA（乙二胺四乙酸）和GLDA（谷氨酸二乙酸）或其游离酸。

36. 发明授权

US07749337B2 Method for the passivation of metal surfaces with polymers containing acid groups 有权
标题翻译：用酸性基团聚合物钝化金属表面的方法
公开(公告)号：US07749337B2
公开(公告)日：2010-07-06
申请号：US11659526
申请日：2006-06-13
申请人： Helmut Witteler , Walter Bertkau , Thomas Heidenfelder , Alexander Göthlich , Jens Haas , Frank Klippel , Gunnar Schornick
发明人： Helmut Witteler , Walter Bertkau , Thomas Heidenfelder , Alexander Göthlich , Jens Haas , Frank Klippel , Gunnar Schornick
IPC分类号： C23C22/53
CPC分类号： C09D5/08 , C23C22/12 , C23C22/53 , Y10T428/12014
摘要： Process for the passivation of metallic surfaces by treatment of the surface with an acidic, aqueous preparation which comprises at least one water-soluble acid group-containing polymer and Zn, Ca, Mg or Al ions, said process being in particular a continuous process for the passivation of strip metals.
摘要翻译：通过用包含至少一种含水溶性含酸基团的聚合物和Zn，Ca，Mg或Al离子的酸性含水制剂处理表面来钝化金属表面的方法，所述方法尤其是用于带状金属的钝化。

37. 发明授权

US07638469B2 Methods of increasing permeability in carbonatic rock formations with alkanesulfonic acids 有权
标题翻译：用烷基磺酸提高碳酸盐岩层的渗透性的方法
公开(公告)号：US07638469B2
公开(公告)日：2009-12-29
申请号：US11817698
申请日：2006-03-03
申请人： Thomas Heidenfelder , Marcus Guzmann , Helmut Witteler , Uwe Ossmer
发明人： Thomas Heidenfelder , Marcus Guzmann , Helmut Witteler , Uwe Ossmer
IPC分类号： C09K8/584
CPC分类号： C09K8/528 , C09K8/54 , C09K8/72 , Y10S166/902
摘要： Methods of increasing permeability in a carbonatic rock formation, the methods comprising: providing an alkanesulfonic acid; and introducing the alkanesulfonic acid into the carbonatic rock formation.
摘要翻译：提高碳酸岩层渗透性的方法，其方法包括：提供烷烃磺酸; 并将烷烃磺酸引入碳酸岩层中。

38. 发明申请

US20090233110A1 Use of polypeptides in the form of adhesive agents 有权
标题翻译：使用粘合剂形式的多肽
公开(公告)号：US20090233110A1
公开(公告)日：2009-09-17
申请号：US11886987
申请日：2006-03-28
申请人： Hermann Seyffer , Karl-Heinz Schumacher , Hans-Georg Lemaire , Ulf Baus , Thomas Subkowski , Marvin Karos , Claus Bollschweiler , Thomas Heidenfelder
发明人： Hermann Seyffer , Karl-Heinz Schumacher , Hans-Georg Lemaire , Ulf Baus , Thomas Subkowski , Marvin Karos , Claus Bollschweiler , Thomas Heidenfelder
IPC分类号： B32B9/02 , B05D3/10 , C07K1/00 , C07K14/00
CPC分类号： C08J7/047 , A61L24/043 , A61L27/34 , A61L31/10 , B32B7/12 , B32B9/02 , B32B15/06 , B32B15/08 , B32B15/18 , B32B15/20 , B32B25/042 , B32B25/08 , B32B27/08 , B32B2255/26 , B32B2307/54 , B32B2307/5825 , C08J2489/00 , Y10T428/31678 , Y10T428/31681 , Y10T428/31685 , Y10T428/31768 , C08L89/00
摘要： A multilayered composite or coated substrate, comprising compounds of which at least 40% by weight are composed of alpha-amino acids linked via peptide bonds as adhesion promoters between at least two adjacent layers of the composite or between the coating and the substrate.
摘要翻译：一种多层复合材料或涂覆的基底，其包含其中至少40重量％由通过肽键连接的α-氨基酸组成的化合物，作为复合材料的至少两个相邻层之间或涂层与基底之间的粘合促进剂。

39. 发明申请

US20080199714A1 Method For the Passivation of Metal Surfaces With Compositions Comprising Polymers With Acid Groups and Waxes 有权
标题翻译：金属表面与酸性基团和蜡组成聚合物组合物的钝化方法
公开(公告)号：US20080199714A1
公开(公告)日：2008-08-21
申请号：US11917290
申请日：2006-06-13
申请人： Helmut Witteler , Walter Bertkau , Thomas Heidenfelder , Alexander Gothlich
发明人： Helmut Witteler , Walter Bertkau , Thomas Heidenfelder , Alexander Gothlich
IPC分类号： B32B15/04 , C23C22/48
CPC分类号： C09D5/08 , C09D133/02 , C23C22/12 , C23C22/22 , Y10T428/12007
摘要： Process for the passivation of metallic surfaces, in particular of strip metals, by treatment of the surface with an acidic, aqueous preparation which comprises at least one water-soluble acid group-containing polymer and at least one wax.
摘要翻译：通过用包含至少一种含水溶性含酸基团的聚合物和至少一种蜡的酸性含水制剂处理表面来钝化金属表面，特别是带状金属的方法。

40. 发明授权

US07217820B2 Cosmetic or pharmaceutical preparations which comprise enaminotriazines as light protection agents, and novel enaminotriazines 失效
标题翻译：包含氨基三嗪作为防晒剂的化妆品或药物制剂，以及新的氨基三嗪
公开(公告)号：US07217820B2
公开(公告)日：2007-05-15
申请号：US10984241
申请日：2004-11-10
申请人： Thomas Heidenfelder , Kristin Tiefensee , Thomas Wünsch
发明人： Thomas Heidenfelder , Kristin Tiefensee , Thomas Wünsch
IPC分类号： C07D251/70 , A61K7/42
CPC分类号： A61Q17/04 , A61K8/4966 , C07D251/70
摘要： The invention relates to the use of enaminotriazines of the formula I in which the radicals Y, independently of one another, are hydrogen, an optionally substituted aliphatic, cycloaliphatic, araliphatic or aromatic radical having in each case up to 18 carbon atoms, the radicals X are identical or different, where at least one of the radicals X is the ethenyl radical of the formula II and X may also have the meanings of Y, and where in the formula II the radicals R are identical or different and are cyano, optionally esterified carboxyl, substituted carbonyl, optionally substituted aminocarbonyl, optionally esterified sulfo, substituted sulfonyl or optionally esterified phosphono, and where two adjacent radicals R may optionally form a ring and the radicals R′ are identical or different and are hydrogen, an optionally substituted aliphatic, cycloaliphatic or aromatic radical having in each case up to 18 carbon atoms, as UV filters in cosmetic or pharmaceutical preparations for protecting human skin or human hair against solar rays, alone or together with compounds which absorb in the UV region and which are known per se for cosmetic preparations.
摘要翻译：本发明涉及式I的氨基三嗪的用途，其中基团Y彼此独立地为氢，任选取代的脂族，脂环族，芳脂族或芳族基团，其中每种情况最多可达18个碳原子，基团X 相同或不同，其中基团X中的至少一个是式II的乙烯基，X也可以具有Y的含义，并且其中在式II中，基团R相同或不同并且是氰基，任选地被酯化羧基，取代的羰基，任选取代的氨基羰基，任选酯化的磺基，取代的磺酰基或任选酯化的膦酰基，并且其中两个相邻的基团R可以任选地形成环，并且基团R'相同或不同，并且是氢，任选取代的脂族，脂环族或在每种情况下最多18个碳原子的芳族基团，作为化妆品中的UV过滤剂或用于保护的药物制剂人类皮肤或人类头发抵抗太阳光线，单独或与在UV区域吸收的化合物一起，并且本身已知本身用于化妆品制剂。

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