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31. 发明授权

US3201400A Propylene oxide adducts of 1-{2[bis(2-hydroxypropyl) amino]ethyl}-4-(2-hydroxypropyl)-piperazine 失效
标题翻译： 1- {2 [双（2-羟丙基）氨基]乙基} -4-（2-羟丙基） - 哌嗪的环氧丙烷加成物
公开(公告)号：US3201400A
公开(公告)日：1965-08-17
申请号：US21022362
申请日：1962-07-16
申请人： JEFFERSON CHEM CO INC
发明人： BEDOIT JR WILLIAM C
IPC分类号： C07D295/13 , C08G18/50
CPC分类号： C07D295/13 , C08G18/506

32. 发明授权

US3138598A Method for preparing piperazines 失效
标题翻译：制备哌嗪的方法
公开(公告)号：US3138598A
公开(公告)日：1964-06-23
申请号：US67503657
申请日：1957-07-30
申请人： JEFFERSON CHEM CO INC
发明人： SPERANZA GEORGE P
IPC分类号： B01J23/00 , B01J23/86 , B01J23/90 , C07D295/023
CPC分类号： C07D295/023 , B01J23/00 , B01J23/868 , B01J23/90 , Y02P20/584

33. 发明授权

US3131132A Purification of dimethylaminoethanol by acid treatment and distillation 失效
标题翻译：通过酸处理和蒸馏纯化二甲基氨基乙醇
公开(公告)号：US3131132A
公开(公告)日：1964-04-28
申请号：US20034962
申请日：1962-06-06
申请人： JEFFERSON CHEM CO INC
发明人： MOSS PHILIP H , YEAKEY ERNEST L
IPC分类号： C07C215/08
CPC分类号： C07C215/08

34. 发明授权

US3128311A Preparation of primary amines 失效
标题翻译：伯胺的制备
公开(公告)号：US3128311A
公开(公告)日：1964-04-07
申请号：US15859661
申请日：1961-12-11
申请人： JEFFERSON CHEM CO INC
发明人： SHIRLEY ROBERT L , SPERANZA GEORGE P
CPC分类号： C07C209/16

35. 发明授权

US3897475A Polyhalobenzonitrile allyl ethers 失效
标题翻译：多卤苄基烯丙基醚
公开(公告)号：US3897475A
公开(公告)日：1975-07-29
申请号：US20616271
申请日：1971-12-08
申请人： JEFFERSON CHEM CO INC
发明人： WATTS JR LEWIS WILLIAM
IPC分类号： C08F16/28 , C08F16/32 , C07C121/74
CPC分类号： C08F16/32 , C08F16/28
摘要： New polyhalobenzonitrile allyl ethers are synthesized in good yield from polyhalobenzonitriles, allyl alcohol and a base. Polymers of these new compounds are useful as metal coatings.
摘要翻译：以多卤代苯腈，烯丙醇和碱为原料合成了新的多卤苄腈烯丙基醚。这些新化合物的聚合物可用作金属涂层。

36. 发明授权

US3860637A Selective manufacture of 4,4{40 -isomer of diaminodiphenyl-methane 失效
标题翻译：选择性制造4,4（4-异构体的二氨基二苯基甲烷）
公开(公告)号：US3860637A
公开(公告)日：1975-01-14
申请号：US10997971
申请日：1971-01-26
申请人： JEFFERSON CHEM CO INC
发明人： BENTLEY FLOYD EDWARD
IPC分类号： C07C85/08
CPC分类号： C07C205/38
摘要： A mixture of poly-(methylenephenylamines) and diaminodiphenylmethane which contains less than 10 percent by weight of the 2,2'' and 2,4'' isomers in the diamine fraction may be made by separating the 2,2'' and 2,4'' isomers of diaminodiphenylmethane and recycling them to the feed of aniline and formaldehyde. This mixture of amines may be phosgenated to the corresponding isocyanates. The isocyanates are useful in the preparation of polyurethane foams.
摘要翻译：在二胺馏分中含有少于10重量％的2,2'和2,4'异构体的聚（亚甲基苯胺）和二氨基二苯基甲烷的混合物可以通过将2,2'和2,4'异构体的二氨基二苯基甲烷，并将其回收到苯胺和甲醛的进料中。胺的这种混合物可以光化到相应的异氰酸酯。异氰酸酯可用于制备聚氨酯泡沫体。

37. 发明授权

US3842081A Preparation of aminocarboxylic acids from aminoalcohols 失效
标题翻译：从氨基醇制备氨基羧酸
公开(公告)号：US3842081A
公开(公告)日：1974-10-15
申请号：US17331671
申请日：1971-08-19
申请人： JEFFERSON CHEM CO INC
发明人： SCHULZE H , MARQUIS E
IPC分类号： C07D295/15 , C07D51/70
CPC分类号： C07D295/15
摘要： 1.AN AQUEOUS PROCESS FOR PREPARING AMINOCARBOXYLIC ACID SALTS COMPRISING THE STEPS OF HEATING AN AMINOALCOHOL IN THE PRESENCE OF AT LEAST A STOICHIOMETRIC QUANTITY, BASED UPON THE AMINOALCOHOL EMPLOYED, OF SODIUM HYDROXIDE, CADMIUM SALTS, AND SUFFICIENT WATER TO MAINTAIN THE COMPONENTS IN THE REACTION MEDIUM IN SOLUTION, SAID AMINOALCOHOL BEING REPRESENTED BY THE FOLLOWING FORMULA:

R"-N(-R'')-CH2-CH2-OH

WHEREIN R'' REPRESENTS HYDROGEN OR A GROUP SELECTED FROM -CH2CH2OH, A C1 TO C15 ALKYL, OR AN AMINOALKYL GROUP HAVING TWO TO THREE CARBON ATOMS; AND R" REPRESENTS HYDROGEN OR A GROUP SELECTED FROM PHENYL, A C1 TO C15 ALKYL SUBSTITUTED PHENYL, OR C1 TO C15 ALKYL; AND WHEREIN EACH R'' AND R" CAN ALSO REPRESENT METHYLENE GROUPS, OR LOWER C1 TO C3 ALKYL SUBSTITUTED METHYLENE GROUPS, SUCH THAT WHEN TAKEN WITH N-CH2CH2OH THEY COMPRISES A PORTION OF AN N-SUBSTITUTED PIPERAZINE COMPOUND WHICH COMPOUND CAN BE FURTHER REPRESENTED BY THE FOLLOWING FORMULA:

R"''-N
WHEREIN R"'' REPRESENTS HYDROGEN, OR A GROUP SELECTED FROM A C1 TO C4 ALKYL OR -CH2CH2OH;AND WHEREIN SAID HEATING 250*C. TO 300*C. FOR A TIME IN THE RANGE OF ABOUT ABOUT 250*C. TO 300*C. FOR A TIME IN THE RANGE OF ABOUT 5 TO 45 MINUTES UNDER A PRESSURE SUFFICIENT TO MAINTAIN THE WATER IN LIQUID PHASE.

38. 发明授权

US3838076A Polyurethane foams from partially aminated polyether polyols 失效
标题翻译：来自部分胺化聚醚多元醇的聚氨酯
公开(公告)号：US3838076A
公开(公告)日：1974-09-24
申请号：US33998873
申请日：1973-03-12
申请人： JEFFERSON CHEM CO INC
发明人： MOSS P , CUSCURIDA M
IPC分类号： C08G18/00 , C08G18/50 , C08G22/44 , C08G22/14
CPC分类号： C08G18/5024
摘要： CELLULAR POLYURETHANE FOAMS ARE PREPARED BY REACTING, IN THE PRESENCE OF A BLOWING ATENT, AN ORGANIC POLYISOCYANATE AND A POLYOXYALKYLENE RESIN HAVING A FUNCTIONALITY OF FROM 2 TO 8 AND AN EQUIVALENT WEIGHT OF FROM ABOUT 900 TO ABOUT 2800. THE TERMINAL GROUPS OF THE POLYOXYALKYLENE RESINS ARE FROM 15 TO ABOUT 55 AMINO GROUPS, WITH THE REMAINING FUNCTIONAL GROUPS BEING HYDROXYL GROUPS.

39. 发明授权

US3833650A Preparation of nitrilotriacetic acid 失效
标题翻译：硝酸酯的制备
公开(公告)号：US3833650A
公开(公告)日：1974-09-03
申请号：US17331571
申请日：1971-08-19
申请人： JEFFERSON CHEM CO INC
发明人： SCHULZE H , MARQUIS E
IPC分类号： C07C99/00 , C07C101/20
CPC分类号： C07C227/02
摘要： AN IMPROVED PROCESS IS PROVIDED FOR PREPARING NITRILOTRIACETIC ACID (NTA) AND ITS SALTS FROM TRIETHANOLAMINE (TEA) IN THE PRESENCE OF ALKALI METAL HYDROXIDES AND CADMIUM SALTS THAT IS CHARACTERIZED BY EMPLOYMENT OF HIGH TEMPERATURES AND VERY SHORT REACTION TIMES.

40. 发明授权

US3816505A Preparation of halogenated dicyanobenzenes 失效
标题翻译：制备二恶烷二恶烷
公开(公告)号：US3816505A
公开(公告)日：1974-06-11
申请号：US29916372
申请日：1972-10-19
申请人： JEFFERSON CHEM CO INC
发明人： WATTS L
IPC分类号： C07C255/51 , C07C121/54 , C07C121/56 , C07C121/58
CPC分类号： C07C255/51
摘要： A PROCESS FOR PREPARING HALOGENATED DERIVATIVES OF DICYANOBENZENES BY A DIRECT VAPOR PHASE REACTION OF A HALOGEN AND A DICYANOBENZENE IN AN OPEN TUBE. HALOGENATED DICYANOBENZENES ARE REPORTED IN HORST SCHEUERMANN''S U.S. PAT. 3,290,353 (1966) AND ROBERT D. BATTERSHELL''S U.S. PAT. 3,331,735 (1967) TO BE USEFUL AS FUNGICIDES, BACTERICIDES AND NEMATOCIDES.

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