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    • 22. 发明申请
    • Method for crystallising a melamine melt
    • 三聚氰胺熔体结晶方法
    • US20060112872A1
    • 2006-06-01
    • US10541796
    • 2004-01-28
    • Tjay Tjioe
    • Tjay Tjioe
    • C30B15/00C30B27/02C30B21/06C30B28/10C30B30/04
    • B01J19/06C07D251/60C07D251/62
    • Method for crystallising a melamine melt to form melamine particles with a D90 of at most 2 mm by cooling a melamine melt to below the crystallisation temperature of the melamine, comprising the formation of a suspension of melamine particles in the cooling medium by spraying the melamine melt with at most 10 wt % of CO2 relative to the sprayed quantity of melamine melt in a space in which a layer of a liquid cooling medium is present that has a temperature below the crystallisation temperature of the melamine and under cooling conditions at which at least 50 wt % of the sprayed melamine melt directly turns into suspended melamine particles. Method for the production of melamine from urea in a preferably continuous, high-pressure process, with application of the present method for the crystallisation.
    • 通过将三聚氰胺熔体冷却至低于三聚氰胺的结晶温度来形成三聚氰胺熔体悬浮液的方法,该方法用于使三聚氰胺熔体结晶以形成至多2mm的三聚氰胺颗粒,其中D 3 < 所述冷却介质通过相对于在存在液体冷却介质层的空间中相对于三聚氰胺熔体的喷射量喷射至多10重量%的CO 3的三聚氰胺熔体,其具有温度 低于三聚氰胺的结晶温度,并且在至少50wt%喷雾的三聚氰胺熔体直接变成悬浮的三聚氰胺颗粒的冷却条件下。 在优选连续的高压过程中由尿素生产三聚氰胺的方法,应用本方法进行结晶。
    • 27. 发明申请
    • Method for producing silicon wafer
    • 硅晶片的制造方法
    • US20060005762A1
    • 2006-01-12
    • US10533147
    • 2003-10-31
    • Susumu MaedaHiroshi InagakiShigeki KawashimaShoei KurosakaKozo Nakamura
    • Susumu MaedaHiroshi InagakiShigeki KawashimaShoei KurosakaKozo Nakamura
    • C30B15/00C30B21/06C30B23/00C30B30/04C30B27/02
    • C30B29/06C30B15/203
    • The present invention is to produce a silicon crystal wherein the boron concentration in the silicon crystal and the growth condition V/G are controlled so that the boron concentration in the silicon crystal is no less than 1×1018 atoms/cm3 and the growth condition V/G falls within the epitaxial defect-free region α2 whose lower limit line LN1 is the line indicating that the growth rate V gradually drops as the boron concentration increases. Further, the present invention is to produce a silicon wafer wherein the boron concentration in the silicon crystal and the growth condition V/G are controlled so as to include at least the epitaxial defect region β1, and the heat treatment condition of the silicon crystal and the oxygen concentration in the silicon crystal are controlled so that no OSF nuclei grow to OSFs. Moreover, the present invention is to produce a silicon crystal wherein the boron concentration in the silicon crystal and the growth condition V/G are controlled so that they fall in the vicinity of the lower limit line LN3 within the epitaxial defect-free region α1.
    • 本发明是为了制造硅晶体,其中硅晶体中的硼浓度和生长条件V / G被控制,使得硅晶体中的硼浓度不低于1×10 18原子/ cm 3,并且生长条件V / G落在外延无缺陷区域α2N中,其下限线LN1是表示生长速率V逐渐下降的线 硼浓度增加。 此外,本发明是为了制造硅晶片,其中硅晶体中的硼浓度和生长条件V / G被控制为至少包括外延缺陷区β1,并且 控制硅晶体的热处理条件和硅晶体中的氧浓度,使得OSF核不生长到OSF。 此外,本发明是为了制造硅晶体,其中硅晶体中的硼浓度和生长条件V / G被控制为使得它们落入外延缺陷区域内的下限线LN3附近, SUB> 1