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21. 发明授权

US07112702B2 Process for the synthesis of bisphenol 有权
标题翻译：合成双酚的方法
公开(公告)号：US07112702B2
公开(公告)日：2006-09-26
申请号：US10248028
申请日：2002-12-12
申请人： Brian Carvill , Katherine Glasgow , Gurram Kishan , Ramesh Krishnamurti , Nilesh Kumar Parkash Kukalyekar , G. V. Ramanarayanan
发明人： Brian Carvill , Katherine Glasgow , Gurram Kishan , Ramesh Krishnamurti , Nilesh Kumar Parkash Kukalyekar , G. V. Ramanarayanan
IPC分类号： C07C39/16
CPC分类号： B01J31/0218 , B01J31/0237 , B01J31/0244 , B01J31/0271 , B01J31/08 , B01J2231/347 , C07C37/20 , C08G64/20 , Y02P20/582 , C07C39/16
摘要： A commercial scale continuous process for the production of a bisphenol comprising reacting a phenol and a ketone in the presence of a modified ion exchange resin catalyst, wherein said modified ion exchange resin comprises a crosslinked gellular acid functionalized polystyrene resin modified by neutralization of with a mercapto promoter.
摘要翻译：一种用于生产双酚的商业规模的连续方法，包括在改性离子交换树脂催化剂存在下使苯酚和酮反应，其中所述改性离子交换树脂包括通过用巯基中和形成的交联的聚乙烯醇交联聚乙烯树脂启动子。

22. 发明授权

US06599596B2 Methods of post-polymerization injection in continuous polyethylene terephthalate production 有权
公开(公告)号：US06599596B2
公开(公告)日：2003-07-29
申请号：US09738150
申请日：2000-12-15
申请人： Carl Steven Nichols , Tony Clifford Moore
发明人： Carl Steven Nichols , Tony Clifford Moore
IPC分类号： B29D2200
CPC分类号： C08J3/2056 , B29K2105/0002 , C08G63/78 , C08G63/80 , C08G63/91 , C08G64/20 , C08G64/42 , C08G69/04 , C08G69/28 , C08G69/48 , C08J3/226 , C08J2367/02 , C08L67/02 , Y10T428/1352 , Y10T428/1369 , Y10T428/2913 , C08L71/00
摘要： The invention is a novel method for the late introduction of additives into a continuous process for making polyethylene terephthalate. The method employs a reactive carrier that functions as a delivery vehicle for one or more additives. The reactive carrier reacts with the polyethylene terephthalate, thereby binding the reactive carrier in the polyethylene terephthalate resin and preventing the emergence of the reactive carrier and additives from the polyethylene terephthalate during subsequent thermal processing.

23. 发明授权

US06498271B2 Tricarboxylic acids, method, and branched polycarbonates prepared therefrom 失效
公开(公告)号：US06498271B2
公开(公告)日：2002-12-24
申请号：US10041996
申请日：2002-01-10
申请人： David Paul Mobley , Mohan Mark Amaratunga , John Henry Lobos
发明人： David Paul Mobley , Mohan Mark Amaratunga , John Henry Lobos
IPC分类号： C07C5500
CPC分类号： C08G64/20 , C08G64/0216 , C08G64/14 , C08G64/1616
摘要： Aliphatic tricarboxylic acids, as exemplified by 9-carboxy-1,18-octadecanedioic acid, may be prepared by the biotransformation of an olefinic monocarboxylic acid such as oleic acid to the corresponding olefinic dicarboxylic acid, preferably 1,18-octadec-9-enedioic acid, in the presence of a strain of yeast, such as a strain of Candida tropicalis, followed by the carboxylation of the olefinic dicarboxylic acid by reaction with carbon monoxide and water in the presence of a catalyst. The product tricarboxylic acids are useful as branching agents for polycarbonates.

24. 发明授权

US06458899B1 Tricarboxylic acids, method, and branched polycarbonates prepared therefrom 失效
标题翻译：三羧酸，方法和由其制备的支化聚碳酸酯
公开(公告)号：US06458899B1
公开(公告)日：2002-10-01
申请号：US09814484
申请日：2001-03-20
申请人： David Paul Mobley , Mohan Mark Amaratunga , John Henry Lobos , Sukhendu Bikash Hait , Andrew James Caruso
发明人： David Paul Mobley , Mohan Mark Amaratunga , John Henry Lobos , Sukhendu Bikash Hait , Andrew James Caruso
IPC分类号： C08G6416
CPC分类号： C08G64/20 , C08G64/0216 , C08G64/14 , C08G64/1616
摘要： Aliphatic tricarboxylic acids, as exemplified by 9-carboxy-1,18-octadecanedioic acid, may be prepared by the biotransformation of an olefinic monocarboxylic acid such as oleic acid to the corresponding olefinic dicarboxylic acid, preferably 1,18-octadec-9-enedioic acid, in the presence of a strain of yeast, such as a strain of Candida tropicalis, followed by the carboxylation of the olefinic dicarboxylic acid by reaction with carbon monoxide and water in the presence of a catalyst. The product tricarboxylic acids are useful as branching agents for polycarbonates.
摘要翻译：脂肪族三羧酸，例如9-羧基-1,18-十八烷二酸，可以通过将烯属单羧酸如油酸生物转化成相应的烯属二羧酸，优选的是1,18-十八碳-9-烯酸在酵母菌株例如热带假丝酵母菌株的存在下，然后在催化剂存在下与一氧化碳和水反应，使烯属二羧酸羧化。产物三羧酸可用作聚碳酸酯的支化剂。

25. 发明授权

US06433126B1 Preparation of copolycarbonates via solid state polymerization 有权
标题翻译：通过固态聚合制备共聚碳酸酯
公开(公告)号：US06433126B1
公开(公告)日：2002-08-13
申请号：US09681755
申请日：2001-05-31
申请人： Sukhendu Bikash Hait
发明人： Sukhendu Bikash Hait
IPC分类号： C08G6400
CPC分类号： C08G64/30 , C08G64/20
摘要： Polycarbonate copolymers have been prepared by solid state polymerization (SSP). A mixture comprising partially crystalline BPA polycarbonate oligomer having a weight average molecular weight of 10,000 daltons and a source of additional structural units and optionally a catalyst is reacted under SSP conditions to afford a copolycarbonate. Sources of additional structural units include high and low molecular weight polycarbonates incorporating repeat units not derived from BPA and various bisphenols such as BPI, BPM and tetramethyl BPA.
摘要翻译：聚碳酸酯共聚物已经通过固相聚合（SSP）制备。将包含重均分子量为10,000道尔顿的部分结晶BPA聚碳酸酯低聚物和另外的结构单元的源和任选的催化剂的混合物在SSP条件下反应，得到共聚碳酸酯。其他结构单元的来源包括高分子量聚碳酸酯和低分子量聚碳酸酯，其包含不衍生自BPA的重复单元和各种双酚，如BPI，BPM和四甲基BPA。

26. 发明授权

US06248858B1 Method for conducting solid state polymerization of polycarbonates 失效
标题翻译：聚碳酸酯的固态聚合方法
公开(公告)号：US06248858B1
公开(公告)日：2001-06-19
申请号：US09192350
申请日：1998-11-16
申请人： James Day , Godavarthi Satyana Varadarajan
发明人： James Day , Godavarthi Satyana Varadarajan
IPC分类号： C08G6400
CPC分类号： C08G64/20 , C08G63/64 , C08G64/40
摘要： Polymerization of polycarbonates is performed by first enhancing the crystallinity of a precursor polycarbonate, such as an oligomer, by contact in pellet form with an alkanol in the liquid or vapor state as non-solvent, and then conducting solid state polymerization in a stream of inert gas such as nitrogen. The solid state polymerization operation includes a stage of heating at a constant temperature in the range of about 215-225° C., optionally combined with a first heating stage at a constant temperature in the range of about 180-190° C. The method is adaptable to continuous operation and produces a polycarbonate having a number average molecular weight, as determined by gel permeation chromatography relative to polystyrene, of at least 15,000.
摘要翻译：聚碳酸酯的聚合通过首先通过以颗粒形式与液体或蒸气状态的链烷醇作为非溶剂接触来提高前体聚碳酸酯如低聚物的结晶度，然后在惰性气流中进行固态聚合气体如氮气。固态聚合操作包括在约215-225℃的恒定温度下加热的阶段，任选地在约180-190℃的恒定温度下与第一加热阶段组合。方法适用于连续操作，并且通过凝胶渗透色谱法相对于聚苯乙烯产生数均分子量为至少15,000的聚碳酸酯。

27. 发明授权

US06187895B1 Method for preparing polymers by solid state polymerization 有权
标题翻译：通过固态聚合制备聚合物的方法
公开(公告)号：US06187895B1
公开(公告)日：2001-02-13
申请号：US09370435
申请日：1999-08-09
申请人： Godavarthi Satyana Varadarajan , James Day , Bhaskar Bhairavnath Idage
发明人： Godavarthi Satyana Varadarajan , James Day , Bhaskar Bhairavnath Idage
IPC分类号： C08G6400
CPC分类号： C08G64/20 , C08G63/80
摘要： Solid state polymerization of polycarbonates and polyesters is preceded by a step of contacting particles of an amorphous precursor polymer with a particulate material, typically a crystallized polycarbonate, which prevents adherence of the precursor polymer particles to each other. It is then possible to perform the solid state polymerization step without crystallizing the precursor polymer.
摘要翻译：聚碳酸酯和聚酯的固态聚合之前是将无定形前体聚合物的颗粒与颗粒材料（通常为结晶的聚碳酸酯）接触的步骤，其阻止前体聚合物颗粒相互粘附。然后可以进行固态聚合步骤而不使前体聚合物结晶。

28. 发明授权

US5900487A High molecular weight stabilizer compounds for stabilizing polymers 失效
公开(公告)号：US5900487A
公开(公告)日：1999-05-04
申请号：US105640
申请日：1998-06-26
申请人： Niles R. Rosenquist
发明人： Niles R. Rosenquist
IPC分类号： C08G64/06 , C07D249/20 , C08G63/64 , C08G64/00 , C08G64/12 , C08G64/14 , C08G64/20 , C08G64/42 , C08K5/3475 , C08L69/00 , C07D403/10 , C07D403/12
CPC分类号： C08G64/14 , C07D249/20 , C08G64/12 , C08G64/20 , C08G63/64
摘要： A high molecular weight stabilizer compound formed as an ester of 3-(2H-benzotriazol-2-yl)-5-(1,1-dimethylethyl)-4-hydroxy-benzene-propanoic acid, or structural variants thereof, to impart improved resistance to the effects of ultraviolet radiation to polycarbonate comprising polymers, a process for the preparation of said compound, and articles of manufacture comprising said compound.

29. 发明授权

US5362841A Process for the preparation of high molecular weight halogenated polycarbonate 失效
标题翻译：制备高分子量卤代聚碳酸酯的方法
公开(公告)号：US5362841A
公开(公告)日：1994-11-08
申请号：US62884
申请日：1993-05-17
申请人： Sarat Munjal , Clark J. Cummings , Che-I Kao
发明人： Sarat Munjal , Clark J. Cummings , Che-I Kao
IPC分类号： C08G64/00 , C08G64/10 , C08G64/20 , C08G64/26
CPC分类号： C08G64/10 , C08G64/20
摘要： A process for preparing halogenated polycarbonate wherein the total amount of base the end pH of the aqueous phaser and the amount of coupling catalyst employed in the reaction are controlled to selected levels.
摘要翻译：一种制备卤化聚碳酸酯的方法，其中碱的总量将水相移化剂的最终pH和反应中使用的偶联催化剂的量控制在选定的水平。

30. 发明授权

US5266659A Solid state process for the preparation of high molecular weight poly(arylcarbonate)s from amorphous oligomer 失效
标题翻译：用于从无定形低聚物制备高分子量聚（芳基碳酸酯）的固态方法
公开(公告)号：US5266659A
公开(公告)日：1993-11-30
申请号：US878932
申请日：1992-05-05
申请人： Swaminathan Sivaram , Jagdish C. Sehra , Venkat S. Iyer , Koyalagunta Ravindranath
发明人： Swaminathan Sivaram , Jagdish C. Sehra , Venkat S. Iyer , Koyalagunta Ravindranath
IPC分类号： C08G64/06 , C08G64/20 , C08G64/30 , C08G64/40
CPC分类号： C08G64/307 , C08G64/06 , C08G64/20 , C08G64/40
摘要： The invention disclosed is an improved process for the preparation of high molecular weight poly(arylcarbonate), the molecular weight ranging from 45,000-60,000 (corresponding to n.sub.inh 0.8 to 1.0) The process involves heating in a controlled manner, a BPA-polycarbonate oligomer in the presence of a catalyst selected from alkali metal aryl acid, alkali metal borohydrial and a quarternary ammonium salt of bioxiyanion derived from a carboxylic acid poly(arylcarbonate)s of high molecular weight produced by the process of present invention show enhanced crystallinity.
摘要翻译：本发明公开了一种制备高分子量聚（芳基碳酸酯）的改进方法，其分子量范围为45,000-60,000（对应于0.8至1.0）。该方法包括以受控方式加热，将BPA-聚碳酸酯低聚物选自碱金属芳基酸，碱金属硼氢化物的催化剂和由本发明方法生产的高分子量羧酸聚（芳基碳酸酯）衍生的生物氰化物的季铵盐的存在显示出增强的结晶度。

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