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21. 发明授权

US4912274A Azaphospholenes and use thereof 失效
标题翻译： Azaphospholenes及其用途
公开(公告)号：US4912274A
公开(公告)日：1990-03-27
申请号：US385614
申请日：1989-07-26
申请人： Gunther Wilke , Jaroslaw Monkiewicz , Herbert Kuhn
发明人： Gunther Wilke , Jaroslaw Monkiewicz , Herbert Kuhn
IPC分类号： B01J31/14 , B01J31/00 , B01J31/22 , B01J31/24 , C07B61/00 , C07C2/04 , C07C2/32 , C07C5/29 , C07C5/31 , C07C13/12 , C07C13/40 , C07C15/44 , C07F9/6564 , C07F9/6584
CPC分类号： C07F9/6584 , C07C2/04 , C07C5/31 , C07C2101/10 , C07C2102/42 , C07C2531/02 , C07C2531/14 , C07C2531/22
摘要： The invention relates to azaphospholenes of the type ##STR1## wherein R.sub.1 and R.sub.2 may be alkyl, aryl and aralkyl groups, processes for preparing same and the use thereof.

22. 发明授权

US4820632A Agent and process for the detection of redox systems 失效
标题翻译：用于检测氧化还原系统的代理和过程
公开(公告)号：US4820632A
公开(公告)日：1989-04-11
申请号：US774353
申请日：1985-09-10
申请人： Gunter Frey , Gerd Zimmermann
发明人： Gunter Frey , Gerd Zimmermann
IPC分类号： A61K49/00 , C07F9/30 , C07F9/32 , C07F9/38 , C07F9/40 , C07F9/572 , C07F9/60 , C07F9/6584 , C09B55/00 , C12Q1/26 , C12Q1/28 , C12Q1/34 , C12Q1/56 , G01N21/78 , G01N31/00 , G01N31/22
CPC分类号： C12Q1/34 , C07F9/301 , C07F9/3211 , C07F9/3808 , C07F9/4006 , C07F9/5728 , C07F9/60 , C07F9/6584 , C12Q1/28 , C12Q2326/00 , Y10T436/173845 , Y10T436/206664
摘要： The present invention is concerned with the use of aniline derivatives of the general formula: ##STR1## wherein R.sub.1 is a hydrogen atom or a lower alkyl or aryl radical, R.sub.2 is a hydrogen atom or a lower alkyl radical which can be substituted by hydroxyl, amino, carboxyl, lower alkoxycarbonyl, lower alkanoylamido, aryl lower alkyl or aryl or by a group of the structure: ##STR2## in which R.sub.5 and R.sub.6 have the meanings given hereinafter, R.sub.3 is a hydrogen or halogen atom or a carboxyl group, R.sub.4 and R'.sub.4, which can be the same or different, are hydrogen or halogen atoms, carboxyl groups or lower alkoxy radicals or lower alkyl radicals which are preferably in the m-position and R.sub.1 and R.sub.4 or R.sub.2 and R.sub.4 or R.sub.4 and R'.sub.4, when the two substituents are ortho to one another, can together form a saturated or unsaturated hydrocarbon chain containing 2 to 6 carbon atoms which can be substituted by hydroxyl or oxo groups, R.sub.5 is a hydrogen atom or a lower alkyl radical and R.sub.6 is a hydroxyl group or a lower alkoxy, lower alkyl or aryl radical; and of the salts thereof with acids and bases(a) as colour former, together with an oxidisable coupling component, in the Trinder reaction for the detection of(a) hydrogen peroxide or hydrogen peroxide-forming systems or(b) peroxidase or peroxidate-acting substances or(b) together with an oxidation agent for the detection of aromatic amines or of systems forming such amines.The present invention also provides agents for the detection of redox systems containing the above aniline derivatives of general formula I.Furthermore, the present invention provides new aniline derivatives coming within the ambit of the above general formula I, as well as processes for the preparation thereof.
摘要翻译：本发明涉及以下通式的苯胺衍生物的用途：其中R 1为氢原子或低级烷基或芳基，R 2为氢原子或可被取代的低级烷基羟基，氨基，羧基，低级烷氧基羰基，低级烷酰氨基，芳基低级烷基或芳基，或以下结构基团：其中R 5和R 6具有下文给出的含义，R 3是氢或卤素原子或羧基基团，可以相同或不同的R 4和R'4是氢或卤素原子，优选位于m位的羧基或低级烷氧基或低级烷基，R 1和R 4或R 2和R 4或R 4 和R'4，当两个取代基彼此邻位时，可以一起形成含有2-6个碳原子的饱和或不饱和烃链，其可以被羟基或氧代基取代，R5是氢原子或低级烷基 R6为羟基或低级a 烷氧基，低级烷基或芳基; （a）作为成色剂和可氧化偶联组分的盐和它们的盐在Trinder反应中用于检测（a）过氧化氢或过氧化氢形成体系，或（b）过氧化物酶或过氧化物 - 作用物质或（b）与氧化剂一起检测芳族胺或形成这种胺的体系。本发明还提供了用于检测含有上述通式I的苯胺衍生物的氧化还原体系的试剂。此外，本发明提供了在上述通式I的范围内的新的苯胺衍生物，以及其制备方法。

23. 发明授权

US4038312A Tricyclic phosphorous triamides 失效
标题翻译：三聚磷酸三聚体
公开(公告)号：US4038312A
公开(公告)日：1977-07-26
申请号：US730519
申请日：1976-10-07
申请人： Thomas Joseph Atkins
发明人： Thomas Joseph Atkins
IPC分类号： C07F9/6584 , D06M15/673 , C07F9/02 , C07F9/22 , C07F9/65
CPC分类号： C07F9/6584 , D06M15/673
摘要： Polycyclic phosphorous triamides of the formula ##STR1## in which R.sup.1 and R.sup.2, alike or different, are alkylene of 2 to about 6 carbons;R.sup.3 and R.sup.4, alike or different, are alkyl of 1 to about 8 carbons, cycloalkyl of 5 to about 8 carbons, or aralkyl where the aryl group is of 6 to about 12 carbons and the alkyl is of 1 to about 8 carbons; or R.sup.3 and R.sup.4 are joined together to form an alkylene group of 2 to about 6 carbons which may be interrupted by1. a ##STR2## group where Q is hydrogen or alkyl of 1 to about 18 carbons, or 2. ONE OR TWO --O-- linkages;There are at least 2 carbons between each two hetero atoms in the outer ring system, and when the triamide is tricyclic, at least one of the chains between the nitrogens linked to phosphorus contains at least three atomsAre useful as flame retardants for cotton.

24. 发明授权

US3987128A Tetracyclic tetraamino phosphoranes and method of preparation 失效
标题翻译：四甲基四胺磷酸盐及其制备方法
公开(公告)号：US3987128A
公开(公告)日：1976-10-19
申请号：US606779
申请日：1975-08-22
申请人： Jack Eugene Richman
发明人： Jack Eugene Richman
IPC分类号： C07F9/6584 , C07F9/09 , C07F9/22 , C07F9/26 , C07F9/58
CPC分类号： C07F9/6584
摘要： Tetracyclic tetraamino phosphoranes of the formula ##EQU1## wherein X is F, C.sub.6 H.sub.5, or C.sub.1 -C.sub.6 alkyl, and tricyclic polyamino phosphine oxides of the formula ##EQU2## wherein x and y are each 2 or 3 Z is --(CH.sub.2)-- where z is 2 to 10 and x + y + z is 7 to 14 orZ is --(CH.sub.2)--NH--(CH.sub.2)-- where v and w are each 2 or 3Are prepared by reacting a silylated cyclic polyamine of the formula ##EQU3## wherein Q is --(CH.sub.2)-- or ##EQU4## with a fluorophosphorane of the formulaXPF.sub.4orPOF.sub.3,provided that when Q is --(CH.sub.2)--, the fluorophosphorane is POF.sub.3. The corresponding alkoxy or amino [X=OR, NR.sub.2 or N(CH.sub.2).sub.2.sub.-6, where R is C.sub.1 -C.sub.6 alkyl] tetracyclic tetraaminophosphoranes are obtained by reaction of an alkali metal alkoxide or amide with the tetracyclic fluorophosphorane. The methyl iodide salts of the tetracyclic tetraamino phosphoranes are also described. All of the polycyclic polyamino phosphoranes and phosphine oxides are useful as flame retardants for cotton.

25. 发明授权

US3965127A Urea-phosphorus compounds 失效
标题翻译：尿素磷化合物
公开(公告)号：US3965127A
公开(公告)日：1976-06-22
申请号：US582962
申请日：1975-06-02
申请人： Gail H. Birum
发明人： Gail H. Birum
IPC分类号： C07F9/30 , C07F9/38 , C07F9/6584 , C09K21/12 , C07F9/02
CPC分类号： C09K21/12 , C07F9/301 , C07F9/3808 , C07F9/6584
摘要： The present invention relates to new cyclic organophosphorus esters having the following structures: ##EQU1## where R is aryl or chloroalkyl of 2 to 10 carbon atoms,R' is aryloxy or chloroalkyloxy of 2 to 10 carbon atoms,R" is hydrogen, alkyl, alkenyl, furanyl or aryl of 1 to 15 carbon atoms and substituted aryl forms where the substituent is fluorine, chlorine, bromine, cyano, hydroxyl, alkyloxy, alkylthio or mixtures of such substituents, andY is O or S.The organophosphorus compounds have biological activity and are also useful as fire retardants, and as lead scavengers in gasoline.
摘要翻译：本发明涉及具有以下结构的新型环状有机磷酯：Y并行-ROH CH3NHCNHCH3 +（RO）2PR'+ R''CHO - > O并列R'-P --- CHR“'| CH3NNCH3角度C并行 Y，其中R是2至10个碳原子的芳基或氯代烷基，R'是2至10个碳原子的芳氧基或氯代烷氧基，R“是氢，烷基，烯基，呋喃基或具有1至15个碳原子的芳基和取代的芳基其中取代基是氟，氯，溴，氰基，羟基，烷氧基，烷硫基或这些取代基的混合物，Y是O或S.

26. 发明授权

US3925456A Cyclic aminophosphonic acids 失效
标题翻译：环状氨基膦酸
公开(公告)号：US3925456A
公开(公告)日：1975-12-09
申请号：US49899674
申请日：1974-08-20
申请人： HENKEL & CIE GMBH
发明人： PLOGER WALTER , SCHMIDT-DUNKER MANFRED , GLOXHUBER CHRISTIAN
IPC分类号： C09K3/00 , A61K8/40 , A61K8/55 , A61K31/675 , A61Q11/00 , C02F5/00 , C02F5/08 , C02F5/10 , C02F5/12 , C02F5/14 , C07F9/24 , C07F9/38 , C07F9/6584
CPC分类号： C02F5/14 , A61K8/55 , A61K31/675 , A61Q11/00 , C07F9/3873 , C07F9/6584
摘要： Cyclic aminophosphonic acids having the formula

wherein R is a member selected from the group consisting of hydrogen and alkyl having from 1 to 6 carbon atoms and n is an integer from 1 to 4; as well as their water-soluble salts. The cyclic aminophosphonic acids are excellent sequestering agents especially for alkaline earth metal ions. They are stabilizers for percompounds and are useful in the delaying of the setting times for gypsum. In addition, the compounds are useful in cosmetic preparations such as toothpastes and mouthwashes where they prevent formation of tartar and plaque and are useful in therapy in the treatment of diseases related to the abnormal deposition or dissolution of difficultly soluble calcium salts in the animal body.
摘要翻译：具有式O的环状氨基膦酸共聚物RN ---- P-OH ||||NHR || O = CC角度平行OH（CH 2）n P ANGLE OH其中R是选自氢和具有1至6个碳原子的烷基，n是1至4的整数; 以及它们的水溶性盐。环状氨基膦酸是优异的螯合剂，特别是对于碱土金属离子。它们是化合物的稳定剂，对于延迟石膏凝固时间是有用的。此外，这些化合物可用于化妆品制剂如牙膏和漱口剂，其中它们防止形成牙垢和斑块，并且可用于治疗与难溶性钙盐在动物体内的异常沉积或溶解有关的疾病的治疗。

27. 发明授权

US3899618A Process for flameproofing cellulosic textiles 失效
标题翻译：隔热纤维素纺织品的工艺
公开(公告)号：US3899618A
公开(公告)日：1975-08-12
申请号：US47151674
申请日：1974-05-20
申请人： US AGRICULTURE
发明人： DAIGLE DONALD J , PEPPERMAN JR ARMAND B , BOUDREAUX GORDON J
IPC分类号： C07F9/6584 , D06M13/285 , C09D5/18 , C07D295/00
CPC分类号： D06M13/285 , C07F9/6584 , Y10S260/24 , Y10S428/921 , Y10T442/268
摘要： 2-Thia-1,3,5-triaza-7-phosphaadamantane 2,2-dioxide was prepared. The phosphine was converted to the phosphine oxide derivative by reaction with hydrogen peroxide and the methyl phosphonium iodide derivative of the phosphene was prepared by reaction with methyl iodide. Dimethyl sulfoxide solutions of said compounds may be used to flameproof cellulosic textiles.
摘要翻译：制备2-硫杂-1,3,5-三氮杂-7-磷杂金刚烷2,2-二氧化物。通过与过氧化氢反应将膦转化为氧化膦衍生物，通过与甲基碘反应来制备磷酸二氢甲基碘化鏻衍生物。所述化合物的二甲亚砜溶液可用于隔离纤维素纺织品。

28. 发明授权

US3897205A Fireproofing cellulose textiles with tetrakis (hydroxymethyl) phosphonium chloride and aniline 失效
标题翻译：用四（羟甲基）氯化鏻和苯胺防火纤维素纺织品
公开(公告)号：US3897205A
公开(公告)日：1975-07-29
申请号：US37697173
申请日：1973-07-06
申请人： US AGRICULTURE
发明人： FRANK ARLEN W , DRAKE JR GEORGE L
IPC分类号： C07F9/50 , C07F9/54 , C07F9/6584 , C08K5/49 , C08K5/50 , D06M13/285 , D06M15/54
CPC分类号： D06M13/285 , C07F9/5004 , C07F9/5407 , C07F9/6584 , C08K5/49 , C08K5/50
摘要： Novel quaternary arylaminoalkyl phosphonium salts having the formula ((ArNHCHR)4P) X , where R is a radical selected from the group consisting of hydrogen, alkyl and aryl, Ar is aryl, and X is halogen, are prepared by the reaction of primary aromatic amines with quaternary hydroxyalkyl phosphonium salts having the formula ((HOCHR)4P) X , where R and X are similarly defined. The compounds of this invention are useful as flame retardant for cotton, plasticizers, lubricant additives, and surface-active agents.
摘要翻译：具有式[（ArNHCHR）4 P] + X'的新型季芳基氨基烷基鏻盐，其中R是选自氢，烷基和芳基的基团，Ar是芳基，X是卤素。通过伯芳族胺与具有式[（HOCHR）4 P] +）的季羟烷基鏻盐的反应，其中R和X的定义类似。本发明的化合物可用作棉花，增塑剂，润滑剂添加剂和表面活性剂的阻燃剂。

29. 发明授权

US3172903A Oxaza- phosphorinane phosphorus ester com- pounds 失效
公开(公告)号：US3172903A
公开(公告)日：1965-03-09
申请号：US3172903D
IPC分类号： C07F9/6584
CPC分类号： C07F9/6584 , C07F9/65842

30. 发明授权

US3151137A Alkylolamine phosphated alkylolamides 失效
标题翻译：烯丙胺磷酸化烷醇酰胺
公开(公告)号：US3151137A
公开(公告)日：1964-09-29
申请号：US84705759
申请日：1959-10-19
申请人： SWIFT & CO
发明人： YOUNG HARLAND H , SPITZMUELLER KURT H
IPC分类号： C07F9/09 , C07F9/6584 , C11D1/38
CPC分类号： C11D1/385 , C07F9/091 , C07F9/6584 , Y10S516/01

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