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21. 发明授权

US4370255A Stabilization of aqueous silicates using alkali siliconates of silylalkyl phosphonates 失效
标题翻译：使用硅烷基烷基膦酸盐的碱性硅酸盐稳定硅酸水溶液
公开(公告)号：US4370255A
公开(公告)日：1983-01-25
申请号：US245059
申请日：1981-03-18
申请人： Edwin P. Plueddemann
发明人： Edwin P. Plueddemann
IPC分类号： C07F9/02 , C23F11/08 , C09K3/00
CPC分类号： C07F9/02 , C23F11/08
摘要： What is disclosed are novel compositions of matter which are alkali siliconate silylalkylphosphonates which are capable of stabilizing water soluble silicates and which are capable of inhibiting corrosion of metals in aqueous systems.
摘要翻译：所公开的是新型的物质组合物，它们是能够稳定水溶性硅酸盐并且能够抑制含水体系中的金属腐蚀的碱性硅酸盐甲硅烷基烷基膦酸盐。

22. 发明授权

US4299943A Nonaqueous preparation of layered or amorphous organometallic inorganic polymers 失效
标题翻译：层状或无定形有机金属无机聚合物的非水性制备
公开(公告)号：US4299943A
公开(公告)日：1981-11-10
申请号：US133859
申请日：1980-03-25
申请人： Peter M. DiGiacomo , Martin B. Dines
发明人： Peter M. DiGiacomo , Martin B. Dines
IPC分类号： C07F9/02 , C07F9/40 , C07F9/58 , C08G79/00 , C08G79/14 , C08G67/00
CPC分类号： C07F9/02 , C07F9/40 , C07F9/582 , C08G79/00 , C08G79/14
摘要： A process for producing layered organometallic polymers having organo groups covalently bonded to pentavalent metal atoms. The pentavalent metal atoms are, in turn, covalently bonded through an oxygen linkage to tetravalent metal atoms. The layered organometallic compounds are produced by reacting a silyl diester of an organo-substituted pentavalent metal acid with at least one tetravalent metal ion.
摘要翻译：具有共价键合到五价金属原子的有机基团的层状有机金属聚合物的方法。五价金属原子又通过氧键与四价金属原子共价键合。通过使有机取代的五价金属酸的甲硅烷基二酯与至少一种四价金属离子反应来制备层状有机金属化合物。

23. 发明授权

US4261913A Titanate phosphite adducts and their use 失效
标题翻译：钛酸亚磷酸酯加成物及其用途
公开(公告)号：US4261913A
公开(公告)日：1981-04-14
申请号：US968447
申请日：1978-12-11
申请人： Salvatore J. Monte , Gerald Sugerman
发明人： Salvatore J. Monte , Gerald Sugerman
IPC分类号： C07F9/02 , C07F9/141 , C08F299/04 , C08G18/10 , C08G18/22 , C08G59/40 , C08G63/91 , C08K5/524 , C07F7/28
CPC分类号： C07F9/02 , C07F9/141 , C08F299/0464 , C08G18/10 , C08G18/222 , C08G59/4092 , C08G63/914 , C08K5/524
摘要： This invention relates to adducts of tetra-substituted titanates and di-substituted hydrogen phosphites; the use of such adducts for treating particulate fillers, including pigments; the compositions of fillers and the aforesaid adducts with epoxy resins and other casting resins; the reaction product of said adducts with aromatic polyamines; the use of said reaction products for curing epoxide and urethane resins; and compositions of certain of the adducts and casting resins. The titanate-phosphite adducts serve to reduce the viscosity of filled epoxy resins, thereby permitting higher filler loading, to enhance the tinctorial power of pigments, and to render casting resins water-extendible. The titanate-phosphite adducts are the reaction products of one mole of a compound having the formula (RO).sub.4 Ti and two moles of di-substituted hydrogen phosphite, (R'O).sub.2 P(O)H, where R and R' are monovalent alkyl, alkenyl, aryl, aralkyl or alkaryl. Both R and R' may be alkoxy, aroxy, bromo or chloro-substituted derivatives of the aforesaid groups. R may have from 1 to 18 carbon atoms, preferably 3 to 12, except where the titanates are used for water-extension, where R is preferably 6 to 12. R' may be from 3 to 18, preferably from 6 to 14.
摘要翻译：本发明涉及四取代钛酸盐和二取代亚磷酸氢盐的加合物; 使用这种加合物来处理颗粒填料，包括颜料; 填料和上述加成物与环氧树脂和其它浇铸树脂的组合物; 所述加合物与芳族多胺的反应产物; 所述反应产物用于固化环氧化物和聚氨酯树脂; 以及某些加合物和浇注树脂的组合物。钛酸酯 - 亚磷酸酯加合物用于降低填充的环氧树脂的粘度，从而允许更高的填料加载量，以提高颜料的着色力，并使浇铸树脂可水扩展。钛酸酯 - 亚磷酸酯加成物是1摩尔具有式（RO）4 Ti的化合物和2摩尔二取代亚磷酸氢盐（R'O）2 P（O）H的反应产物，其中R和R'是一价烷基，烯基，芳基，芳烷基或烷芳基。 R和R'都可以是上述基团的烷氧基，芳氧基，溴或氯取代的衍生物。 R可以具有1至18个碳原子，优选3至12个，除非钛酸酯用于水延伸，其中R优选为6至12.R'可以为3至18，优选6至14。

24. 发明授权

US4220590A Asymmetric catalysis 失效
标题翻译：不对称催化
公开(公告)号：US4220590A
公开(公告)日：1980-09-02
申请号：US929635
申请日：1978-07-31
申请人： William S. Knowles , Milton J. Sabacky , Billy D. Vineyard
发明人： William S. Knowles , Milton J. Sabacky , Billy D. Vineyard
IPC分类号： C07B31/00 , B01J20060101 , B01J27/18 , B01J31/00 , B01J31/18 , B01J31/24 , B01J31/28 , C07B53/00 , C07B61/00 , C07C20060101 , C07C51/36 , C07C57/00 , C07C67/00 , C07C231/00 , C07C231/12 , C07C231/18 , C07C233/47 , C07D209/10 , C07D233/64 , C07D307/38 , C07D317/48 , C07D333/24 , C07F20060101 , C07F9/02 , C07F9/48 , C07F9/50 , C07F15/00 , C07C101/02 , C07C103/50 , C07D209/20
CPC分类号： B01J31/24 , B01J31/2409 , B01J31/2414 , C07F15/0073 , C07F15/008 , C07F9/02 , C07F9/5027 , B01J2231/645 , B01J2531/821 , B01J2531/822 , B01J2531/827 , B01J31/1875
摘要： New optically active bis phosphine compounds which are usful in optically active catalysts. Such catalysts are particularly useful in catalytic asymmetric hydrogenation.
摘要翻译：可用于光学活性催化剂的新的光学活性双膦化合物。这种催化剂特别适用于催化不对称氢化。

25. 发明授权

US4166796A Composition comprising a cosulfurized blend of lard oil and an olefin 失效
标题翻译：组合物，其包含猪油和烯烃的共硫化共混物
公开(公告)号：US4166796A
公开(公告)日：1979-09-04
申请号：US905909
申请日：1978-05-15
申请人： Alexander D. Recchuite
发明人： Alexander D. Recchuite
IPC分类号： C07F9/02 , C07G99/00 , C10M135/02 , C10M171/00 , C10M1/38 , C07G17/00 , C09B49/00 , C10M5/22
CPC分类号： C07G17/002 , C07F9/02 , C10M135/02 , C10M171/002 , C10M2203/02 , C10M2203/022 , C10M2203/024 , C10M2203/04 , C10M2203/06 , C10M2203/10 , C10M2203/102 , C10M2203/104 , C10M2203/106 , C10M2203/108 , C10M2205/00 , C10M2205/02 , C10M2205/024 , C10M2205/026 , C10M2205/028 , C10M2205/04 , C10M2207/024 , C10M2211/02 , C10M2219/02 , C10M2219/022 , C10M2219/024 , C10M2219/046 , C10M2221/041 , C10M2223/04 , C10M2223/041 , C10M2223/042 , C10M2223/045 , C10M2223/065 , C10M2223/12 , C10N2210/02 , C10N2240/00 , C10N2240/04 , C10N2240/042 , C10N2240/044 , C10N2240/046 , C10N2240/08 , C10N2240/22 , C10N2240/30 , C10N2240/40 , C10N2240/50 , C10N2240/52 , C10N2240/54 , C10N2240/56 , C10N2240/58 , C10N2240/60 , C10N2240/66
摘要： Process of sulfurizing a blend of 90 to 50 and preferably 88 to 70 parts by volume of triglyceride such as lard oil and 10 to 50 and preferably 12 to 30 parts by volume of an ethylenically unsaturated hydrocarbon contaning 2 to 24 carbon atoms. The sulfurization is carried out using elemental sulfur. Simultaneous sulfurization and chlorination may be effected by reacting with sulfur monochloride. Phosphosulfurization may also be carried out by addition of small amounts of a phosphorus sulfide to the sulfurized blend followed by heating at 180.degree. F. to 250.degree. F. for from 30 minutes to 10 hours to effect phosphosulfurization. The sulfurization or phosphosulfurization involves reacting at from 330.degree. F. to 445.degree. F. for 20 minutes to 10 hours followed by blowing with a gas at from 125.degree. F. to 250.degree. F. for 30 minutes to 20 hours to remove hydrogen sulfide. The simultaneous sulfurization and chlorination reaction is carried out at from 90.degree. F. to 280.degree. F. for from 20 minutes to 10 hours followed by blowing with a gas at from 125.degree. F. to 250.degree. F. for 30 minutes to 20 hours. The sulfurized oils contain from 7.5 to 25 weight percent sulfur as based on the blend of olefin and triglyceride.
摘要翻译：将90至50体积％，优选88至70体积份的甘油三酯如猪油和10至50份，优选12至30份体积的含有2至24个碳原子的烯属不饱和烃的共混物硫化的方法。硫化使用元素硫进行。同时硫化和氯化可以通过与一氯化硫反应来实现。磷硫化也可以通过向硫化混合物中加入少量硫化磷，然后在180°F加热至250°F进行30分钟至10小时进行磷硫化。硫化或磷硫化包括在330°F至445°F下反应20分钟至10小时，然后用125°F至250°F的气体吹扫30分钟至20小时以除去硫化氢。同步硫化和氯化反应在90°F至280°F进行20分钟至10小时，随后用125°F至250°F的气体吹扫30分钟至20小时。基于烯烃和甘油三酯的共混物，硫化油含有7.5至25重量％的硫。

26. 发明授权

US4163018A Process for preparing metal salts of alkyl phosphates 失效
标题翻译：制备磷酸烷基酯金属盐的方法
公开(公告)号：US4163018A
公开(公告)日：1979-07-31
申请号：US860408
申请日：1977-12-13
申请人： Fusao Tada , Jajimu Shimizu , Tsutomu Asaoka , Fuminori Matsumoto
发明人： Fusao Tada , Jajimu Shimizu , Tsutomu Asaoka , Fuminori Matsumoto
IPC分类号： C08K5/00 , C07F9/02 , C07F9/11 , C08K5/52 , C08K5/521 , C08L1/00 , C08L7/00 , C08L21/00 , C08L23/00 , C08L27/00 , C08L51/00 , C08L51/02 , C08L101/00 , C07F3/06
CPC分类号： C07F9/02 , C07F9/11 , C08K5/521
摘要： A process for preparing metal salts of alkyl phosphate of either one of the formulae: ##STR1## WHICH COMPRISES REACTING AN ALKYL PHOSPHATE OF EITHER ONE OF THE FORMULAE: ##STR2## in the form of its alkali metal salt with a metal salt of the formula: M.sub.n X.sub.m in an aqueous medium at a temperature of from about 50.degree. to 80.degree. C. (wherein R is an alkyl group of not less than 12 carbon atoms, M is an alkaline earth metal, aluminum or zinc, X is halogen ion, sulfate ion or nitrate ion, l is an integer corresonding to the atomic valency of M, r is an integer of 0, 1 or 2, m is an integer of 1, 2 or 3 and n is an integer of 1 or 2).
摘要翻译：一种制备以下任何一种的金属烷基磷酸盐的方法：＆lt; IMAGE＆gt;和＆lt; IMAGE＆gt;其包含反应式中的一种的碱金属磷酸盐：和以其碱金属的形式在水性介质中在约50〜80℃的温度下与式MnMm的金属盐（其中R是不小于12个碳原子的烷基，M是碱土金属，铝或锌，X是卤素离子，硫酸根离子或硝酸根离子，l是与M的原子价相对应的整数，r是0,1或2的整数，m是1,2或3的整数，n是 1或2的整数）。

27. 发明授权

US4152311A Titanate phosphite adducts and their use 失效
标题翻译：钛酸盐添加剂及其使用
公开(公告)号：US4152311A
公开(公告)日：1979-05-01
申请号：US847151
申请日：1977-10-31
申请人： Salvatore J. Monte , Gerald Sugerman
发明人： Salvatore J. Monte , Gerald Sugerman
IPC分类号： C08K5/00 , C07F7/28 , C07F9/02 , C07F9/141 , C08F299/04 , C08G18/10 , C08G18/22 , C08G59/00 , C08G59/40 , C08G59/68 , C08G63/91 , C08K5/51 , C08K5/524 , C08K5/56 , C08L33/00 , C08L33/02 , C08L63/00 , C08L67/00 , C08L67/06 , C08L87/00 , C08L101/00 , C09D7/00 , C09D7/12 , C09D161/04 , C09D163/00 , C09K3/10 , C08K5/18 , C08K5/42
CPC分类号： C07F9/02 , C07F9/141 , C08F299/0464 , C08G18/10 , C08G18/222 , C08G59/4092 , C08G63/914 , C08K5/524
摘要： This invention relates to adducts of tetra-substituted titanates and di-substituted hydrogen phosphites; the use of such adducts for treating particulate fillers, including pigments; the compositions of fillers and the aforesaid adducts with epoxy resins and other casting resins; the reaction product of said adducts with aromatic polyamines; the use of said reaction products for curing epoxide and urethane resins; and compositions of certain of the adducts and casting resins. The titanate-phosphite adducts serve to reduce the viscosity of filled epoxy resins, thereby permitting higher filler loading, to enhance the tinctorial power of pigments, and to render casting resins water-extendible. The titanate-phosphite adducts are the reaction products of one mole of a compound having the formula (RO).sub.4 Ti and two moles of di-substituted hydrogen phosphite, (R'O).sub.2 P(O)H, where R and R' are monovalent alkyl, alkenyl, aryl, aralkyl or alkaryl. Both R and R' may be alkoxy, aroxy, bromo or chloro-substituted derivatives of the aforesaid groups. R may have from 1 to 18 carbon atoms, preferably 3 to 12, except where the titanates are used for water-extension, where R is preferably 6 to 12. R' may be from 3 to 18, preferably from 6 to 14.

28. 发明授权

US4143057A Coordination complexes as catalysts 失效
标题翻译：协调复合物作为催化剂
公开(公告)号：US4143057A
公开(公告)日：1979-03-06
申请号：US773001
申请日：1977-02-28
申请人： Kurt Weinberg , Gordon C. Johnson
发明人： Kurt Weinberg , Gordon C. Johnson
IPC分类号： C08G63/00 , C07F7/08 , C07F7/18 , C07F7/22 , C07F7/24 , C07F7/28 , C07F7/30 , C07F9/02 , C08G63/181 , C08G63/78 , C08G63/82 , C07F7/00
CPC分类号： C07F9/02 , C07F7/182 , C08G63/181 , C08G63/82
摘要： A process for producing polyesters and copolyesters, useful for making films and fibers, by the polycondensation of dicarboxylic acids and aliphatic glycols using coordinations complexes of metal halides and silicon compounds as catalysts.
摘要翻译：通过使用金属卤化物和硅化合物作为催化剂的配位络合物，通过二羧酸和脂肪族二醇的缩聚制备聚酯和共聚酯的方法，可用于制备膜和纤维。

29. 发明授权

US4139616A Fungicidal compositions based on phosphorous acid esters and salts thereof 失效
标题翻译：基于亚磷酸酯及其盐的杀真菌组合物
公开(公告)号：US4139616A
公开(公告)日：1979-02-13
申请号：US531387
申请日：1974-12-10
申请人： Jacques Ducret , Guy Lacroix , Jean-Michel Gaulliard
发明人： Jacques Ducret , Guy Lacroix , Jean-Michel Gaulliard
IPC分类号： A01N57/12 , A01N57/10 , A01N57/14 , A01N57/16 , A01N59/16 , A01P3/00 , C07F9/02 , C07F9/141 , C07F13/00 , A01N9/36
CPC分类号： C07F9/02 , A01N57/10 , C07F9/141
摘要： Compositions for controlling fungus disease are disclosed which contain as active material a fungicidally effective amount of at least one compound of the formula ##STR1## IN WHICH R is an optionally halogenated or nitrated, linear or branched alkyl radical containing from 1 to 18 carbon atoms and preferably from 1 to 8 carbon atoms, an optionally halogenated alkenyl or alkinyl radical, an alkoxy alkyl radical, an alkenoxy alkyl radical, the hydrocarbon portion of these four types of radicals containing from 1 to 8 and preferably from 1 to 5 carbon atoms, a cyclohexyl radical, an optionally substituted aryl radical, preferably phenyl, or aryl alkyl radical, preferably phenyl alkyl, or even a heterocyclic radical optionally attached to the oxygen through an aliphatic chain, preferably tetrahydrofurfuryl, M represents an ammonium cation, ammonium substituted by 1 to 4 alkyl or hydroxy alkyl radicals containing from 1 to 5 carbon atoms or by 1 to 2 cyclohexyl radicals or a phenyl radical, or a cation of a metal from the group comprising the alkali metals, preferably sodium and potassium, alkaline earth metals, preferably magnesium, barium, calcium, and polyvalent metals such as, preferably, zinc, manganese, copper(I) and (II), iron, nickel, aluminium,N is an integer equal to the valency of M.
摘要翻译：公开了用于控制真菌病的组合物，其含有杀真菌有效量的至少一种下式的化合物，其中R是含有1至18个碳原子的任选卤代或硝化的直链或支链烷基，优选1至8个碳原子，任选卤代的烯基或炔基，烷氧基烷基，链烯氧基烷基，这四种类型的含有1至8个，优选1至5个碳原子的基团的烃部分，环烷基，任选取代的芳基，优选苯基或芳基烷基，优选苯基烷基，或甚至任选地通过脂族链连接到氧上的杂环基，优选四氢糠基，M表示铵阳离子，被1至 4个含有1至5个碳原子的烷基或羟基烷基或1至2个环己基或苯基，或由碱金属，优选钠和钾，碱土金属，优选镁，钡，钙和多价金属（优选锌，锰，铜（I）和（II））组成的金属阳离子，，铁，镍，铝，N是一个整数等于M.

30. 发明授权

US4133823A Reaction products of metal oxides and salts with phosphorus compounds 失效
公开(公告)号：US4133823A
公开(公告)日：1979-01-09
申请号：US724192
申请日：1976-09-17
申请人： Samuel F. Joyce, III , Albert W. Morgan , Norman W. Touchette , William Vanderlinde
发明人： Samuel F. Joyce, III , Albert W. Morgan , Norman W. Touchette , William Vanderlinde
IPC分类号： C07F9/02 , C07F9/40 , C07F15/06
CPC分类号： C07F9/02 , C07F9/4006
摘要： Reaction products are prepared from metal oxides and salts and phosphorus compounds containing trivalent phosphorus. The reaction products are useful as flame retardants and smoke suppressants.

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