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21. 发明授权

US07223471B2 Polytrimethylene terephthalate resins with improved properties 有权
标题翻译：具有改进性能的聚对苯二甲酸丙二醇酯树脂
公开(公告)号：US07223471B2
公开(公告)日：2007-05-29
申请号：US10508596
申请日：2003-02-20
申请人： Eckhard Seidel , Bernd Gemmel , Karl-Heinz Heldmann
发明人： Eckhard Seidel , Bernd Gemmel , Karl-Heinz Heldmann
IPC分类号： D02G3/00
CPC分类号： C08K5/0008 , C08G63/183 , C08G63/78 , C08L67/02 , Y10T428/249921 , Y10T428/2913 , Y10T428/2915 , Y10T428/2924 , C08L77/00
摘要： A composition comprising Polytrimethylene terephthalate (PTT) with a reduced emission of acrolein is obtained by contacting Polytrimethylene terephthalate (PTT) resin with an effective amount of a melt stable, organic stabilizing compound. Such PTT resin has an acrolein formation rate at 280° C. of less than 15 ppm/minute. Preferably the residual acrolein content of the PTT resin is less than 10 ppm. The additive organic stabilizing compounds are free from nitrogen atoms. Preferred additive compounds include polyfunctional alkohols, alcoholates, aromatic carboxylic acid anhydrides, carboxylic acids and salts of carboxylic acids. The additive compounds are added to the polymer in molten state and/or to the resin, which is then processed to fibers, filaments, non-wovens, films and/or mouldings.
摘要翻译：通过使聚对苯二甲酸丙二醇酯（PTT）树脂与有效量的熔体稳定的有机稳定化合物接触，获得包含丙烯醛的减少的聚对苯二甲酸丙二醇酯（PTT）的组合物。这种PTT树脂在280℃下的丙烯醛形成速率小于15ppm /分钟。优选地，PTT树脂的残留丙烯醛含量小于10ppm。添加剂有机稳定化合物不含氮原子。优选的添加剂化合物包括多官能醇，醇化物，芳族羧酸酐，羧酸和羧酸盐。将添加剂化合物以熔融状态和/或树脂加入到聚合物中，然后将其加工成纤维，长丝，无纺布，薄膜和/或模制品。

22. 发明授权

US07152742B2 Separation process for carpets 失效
标题翻译：地毯分离工艺
公开(公告)号：US07152742B2
公开(公告)日：2006-12-26
申请号：US10466667
申请日：2002-01-10
申请人： Roland Donaj , Wolfgang Dilly-Louis , Rudolf Kämpf , Norman Schnittker , Reinhard Wolf
发明人： Roland Donaj , Wolfgang Dilly-Louis , Rudolf Kämpf , Norman Schnittker , Reinhard Wolf
IPC分类号： B03B5/60
CPC分类号： B03B9/061 , B03B1/04 , B03B2009/067 , B29B17/02 , B29B2017/0203 , B29B2017/0224 , B29B2017/0231 , B29B2017/0488 , B29K2009/06 , B29K2023/12 , B29K2077/00 , B29K2105/04 , B29K2105/065 , B29K2313/00 , B29L2031/7322 , Y02W30/521 , Y02W30/523 , Y02W30/622 , Y02W30/625 , Y02W30/667
摘要： Comminuted carpet pieces are fed to a first stirred tank together with an aqueous solution containing separating salt, to form a first suspension, which is fed to a first mechanical separating stage. A first high-solids phase, a second high-solids phase containing polymer fiber material, and a liquid phase are obtained therefrom. The second high-solids phase is mixed with a water-containing separation solution in a stirred tank, to give a second suspension, which is fed to a second mechanical separating stage. A third high-solids phase, a polymer fiber material-rich phase and a liquid phase are withdrawn therefrom. An acid which is stronger than H2CO3 is introduced into the stirred tank together with the water-containing separation solution, and the pH of the liquid in the stirred tank is adjusted to 2–6.
摘要翻译：将粉碎的地毯片与含有分离盐的水溶液一起进料至第一搅拌槽，以形成第一悬浮液，将其送入第一机械分离阶段。从其获得第一高固体相，含有聚合物纤维材料的第二高固体相和液相。将第二高固体相与搅拌槽中的含水分离溶液混合，得到第二悬浮液，将其送入第二机械分离阶段。第三高固体相，富聚合物纤维材料相和液相从其中取出。将比H 2 CO 3 3强的酸与含水分离溶液一起引入搅拌槽中，搅拌罐中液体的pH为调整为2-6。

23. 发明申请

US20050269439A1 Method for spinning and reeling polyester multifilament yarns by using spinning additives, and polyester multifilament yarns obtained by said spinning method 审中-公开
标题翻译：通过使用纺丝添加剂纺丝和卷取聚酯复丝纱线的方法以及通过所述纺丝方法得到的聚酯复丝纱线
公开(公告)号：US20050269439A1
公开(公告)日：2005-12-08
申请号：US10508961
申请日：2003-02-21
申请人： Ulrich Mirwaldt , Maria Mirwaldtova , Thomas Mirwaldt , Peter Mirwaldt , Eckhard Seidel , Dietmar Wandel
发明人： Ulrich Mirwaldt , Maria Mirwaldtova , Thomas Mirwaldt , Peter Mirwaldt , Eckhard Seidel , Dietmar Wandel
IPC分类号： D01D10/02 , D01F6/62 , D01F6/92 , B65H18/28
CPC分类号： D01F6/92 , D01D10/02 , D01F6/62
摘要： The present invention relates to a process for producing and winding partially oriented polyester multifilament yarns not less than 85% by weight based on the total weight of the multifilament yarn polybutylene terephthalate (PBT) and/or polytrimethylene terephthalate (PTMT) that contain between 0.05% by weight and 2.5% by weight based on the total weight of the multifilament yarn of at least one additive polymer extensibility enhancer, which comprises providing a wound yarn package which is stable in long-term storage and insensitive to elevated temperatures during storage and transportation by heat-treating the wound polyester multifilament yarn package at a temperature in the range from >45° C. to 65° C. The present invention further relates to the polyester multifilament yarns obtainable by the process and to their use.
摘要翻译：本发明涉及基于复丝纱聚对苯二甲酸丁二醇酯（PBT）和/或聚对苯二甲酸丙二醇酯（PTMT）的总重量为85重量％以上的部分取向的聚酯复丝纱线的制造和卷绕方法，其包含0.05％和2.5重量％，基于至少一种添加剂聚合物可延展性增强剂的复丝纱线的总重量，其包括提供在长期储存中稳定并且在储存和运输期间对高温不敏感的缠绕纱线包装在≥45℃至65℃的温度下对缠绕的聚酯复丝纱线卷进行热处理。本发明还涉及通过该方法获得的聚酯复丝纱线及其用途。

24. 发明授权

US06972102B1 Method and device for continually producing an extrusion solution 失效
标题翻译：用于连续生产挤出溶液的方法和装置
公开(公告)号：US06972102B1
公开(公告)日：2005-12-06
申请号：US10088773
申请日：2000-09-29
申请人： Ralf-Uwe Bauer , Uwe Kind
发明人： Ralf-Uwe Bauer , Uwe Kind
IPC分类号： C08B1/00 , D01D1/02 , D01F2/00 , C08J5/18
CPC分类号： D01D1/02 , C08B1/003 , D01F2/00
摘要： The invention relates to a method for continually producing an extrusion solution for producing cellulosed shaped bodies, such as fibres and films, according to the lyocell method. According to the inventive method, (a) a cellulose suspension is produced from cellulose and an aqueous phase in a mass ratio ranging from 1:3 to 1:40, whereby shearing is maintained for between 5 to 200 minutes. (b) The cellulose suspension is dewatered to form a material having a cellulose content ranging from 20 to 80 mass % and the aqueous phase produced thereby is at least partially returned to step (a). (c) The humid cellulose material being homogenised is transported through a first shearing zone in the absence of N-methylmorpholine-N-oxide. (d) The cellulose material is transported through a second shearing zone after sufficient aqueous N-Methyl-morpholine-N-oxide has been added to the homogenised cellulose material so that, after mixing, a suspension having a N-Methylmorpholine-N-oxide content ranging from 70 to 80 mass % in the liquid phase is obtained. The cellulose material or the suspension completely fills in the available cross-section of transport in the shearing zones and (e) the produced cellulose suspension being sheared is converted into the extrusion solution in aqueous N-Methylmorpholine-N-oxide, whereby water evaporates.
摘要翻译：本发明涉及根据lyocell法连续生产纤维素成形体如纤维和薄膜的挤出溶液的方法。根据本发明的方法，（a）由纤维素和水相以1:3至1:40的质量比产生纤维素悬浮液，由此剪切保持5至200分钟。（b）将纤维素悬浮液脱水，形成纤维素含量为20〜80质量％的材料，由此制造的水相至少部分返回到工序（a）。（c）均匀化的潮湿纤维素材料在没有N-甲基吗啉-N-氧化物的情况下通过第一剪切区输送。（d）在均匀化的纤维素材料中加入足够的N-甲基吗啉-N-氧化物水溶液之后，将纤维素材料输送通过第二剪切区，使混合后得到具有N-甲基吗啉-N-氧化物得到在液相中含量为70〜80质量％的含量。纤维素材料或悬浮液完全填充剪切区域中可用的输送横截面，（e）将所生产的被剪切的纤维素悬浮液转化成N-甲基吗啉-N-氧化物水溶液的挤出溶液，由此水蒸发。

25. 发明授权

US06864345B2 Process and apparatus for producing polyethylene terephthalate 有权
标题翻译：生产聚对苯二甲酸乙二醇酯的方法和设备
公开(公告)号：US06864345B2
公开(公告)日：2005-03-08
申请号：US10477796
申请日：2002-04-30
申请人： Randolf Reimann
发明人： Randolf Reimann
IPC分类号： B01D3/34 , B01D5/00 , B01D53/86 , C08G63/183 , C08G63/78 , C08G63/00
CPC分类号： C08G63/78 , B01D3/343 , B01D5/009 , B01D53/8668 , C08G63/183
摘要： In a process of producing polyethylene terephthalate by esterification of terephthalic acid with ethylene glycol and polycondensation, the vapors formed are rectified, the liquid phase is recirculated to the process, and the lower-boiling components are condensed. To obtain an almost completely stripped condensate, condensate is circulated and stripped the same with air, and the exhaust air is subjected to a catalytic oxidation.
摘要翻译：在通过对苯二甲酸与乙二醇的酯化和缩聚生产聚对苯二甲酸乙二醇酯的方法中，所形成的蒸汽被精馏，液相再循环到该方法中，并且低沸点组分被冷凝。为了获得几乎完全剥离的冷凝物，冷凝物循环并与空气一起汽提，并且排出的空气进行催化氧化。

26. 发明授权

US3624040A Process for the production of polyethylene terephthalate 失效
标题翻译：制备聚乙烯三烯酸的方法
公开(公告)号：US3624040A
公开(公告)日：1971-11-30
申请号：US3624040D
申请日：1970-03-27
申请人： VICKERS ZIMMER AG
发明人： RATH HERMAN , ROTHE HANS-JOCHEN , RIZ OTTO FRIEDRICH DE
IPC分类号： C08G63/86 , C07F9/90
CPC分类号： C08G63/866
摘要： Process for polycondensing di(alkylene glycol) terephthalate by use of metal compounds as catalysts in which the metal compound is an antimony complex of the formula

WHERE X signifies a halogen or thiocyanate, n is a whole number from four to six, preferably, five, and Z is selected from the group consisting of di(pyridyl) ethylene and di(morpholino) ethane bases of basicity (+valence) m 2, and mixtures of said bases.

27. 发明授权

US3496604A Worm melter and extruder 失效
标题翻译： WORM MELTER AND EXTRUDER
公开(公告)号：US3496604A
公开(公告)日：1970-02-24
申请号：US3496604D
申请日：1967-10-17
申请人： VICKERS ZIMMER AG
发明人： SCHWALM WILHELM
IPC分类号： B29C47/64 , B29F3/02
CPC分类号： B29C47/60 , B29C47/0009

28. 发明授权

US3481969A Process for the production of adiponitrile 失效
标题翻译：生产ADIPONITRILE的方法
公开(公告)号：US3481969A
公开(公告)日：1969-12-02
申请号：US3481969D
申请日：1966-06-14
申请人： VICKERS ZIMMER AG
发明人： CORSEPIUS HORST , BENDE FRIEDRICH
IPC分类号： C07C121/10
CPC分类号： C07C255/00

29. 发明授权

US3478102A Hexamethylene diamine manufacture 失效
标题翻译：十六烷基二胺制造
公开(公告)号：US3478102A
公开(公告)日：1969-11-11
申请号：US3478102D
申请日：1966-06-14
申请人： VICKERS ZIMMER AG
发明人： BENDE FRIEDRICH , CORSEPIUS HORST , HANSEL WERNER
IPC分类号： B01J23/89 , C07C209/48 , C07C87/14 , C07C85/12
CPC分类号： B01J23/8986 , C07C209/48

30. 发明授权

US3476804A Method for the production of adipic acid and recovery of nitric acid components 失效
标题翻译：生产酸性和硝酸成份回收方法
公开(公告)号：US3476804A
公开(公告)日：1969-11-04
申请号：US3476804D
申请日：1966-06-14
申请人： VICKERS ZIMMER AG
发明人： BENDE FRIEDRICH , VOLLINGER HEINZ , POHL KURT
IPC分类号： C07C51/31 , C07C55/14 , C07C51/28
CPC分类号： C07C51/316 , C07C55/14

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