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21. 发明授权

US09056925B2 Process for production of modified conjugated diene polymers, modified conjugated diene polymers produced by the process, rubber compositions, and tires 有权
标题翻译：改性共轭二烯聚合物的制备方法，通过该方法制备的改性共轭二烯聚合物，橡胶组合物和轮胎
公开(公告)号：US09056925B2
公开(公告)日：2015-06-16
申请号：US12446799
申请日：2007-10-25
申请人： Ken Tanaka , Kouji Masaki , Yoichi Ozawa , Eiji Suzuki , Christine M. Rademacher , Terrence E. Hogan , Takuo Sone , Takaomi Matsumoto
发明人： Ken Tanaka , Kouji Masaki , Yoichi Ozawa , Eiji Suzuki , Christine M. Rademacher , Terrence E. Hogan , Takuo Sone , Takaomi Matsumoto
IPC分类号： C08L83/00 , C08C19/25 , B60C1/00 , C08C19/44 , C08L15/00 , C08L21/00
CPC分类号： C08C19/25 , B60C1/0016 , B60C1/0025 , C08C19/44 , C08K3/04 , C08K3/36 , C08L9/00 , C08L15/00 , C08L21/00 , C08L2666/08
摘要： A process for producing a modified conjugated diene based polymer includes a step (a) of reacting a silicon compound with a conjugated diene based polymer having an active end so that the reaction takes place at the active end, the silicon compound having a protected primary amino group in the molecule thereof and a silicon atom to which a hydrocarbyloxy group and a reactive group are bonded, to thereby modify the active end, and a step (b) of performing condensation reaction, in the presence of a titanium compound serving as a titanium-based condensation-accelerating agent. A rubber composition contains the modified diene polymer, and a tire is produced from the rubber composition.
摘要翻译：改性共轭二烯系聚合物的制造方法包括使硅化合物与具有活性末端的共轭二烯系聚合物反应以使反应在活性末端进行的工序（a），具有被保护的伯氨基在其分子中具有烃氧基和反应性基团键合的硅原子，从而改变活性末端，以及在用作钛的钛化合物的存在下进行缩合反应的步骤（b）的缩合促进剂。橡胶组合物含有改性二烯聚合物，由橡胶组合物制成轮胎。

22. 发明申请

US20110160388A1 PROCESS FOR PRODUCTION OF MODIFIED CONJUGATED DIENE COPOLYMER, MODIFIED CONJUGATED DIENE COPOLYMER PRODUCED BY THE PROCESS, RUBBER COMPOSITION, AND TIRE 审中-公开
标题翻译：生产改性共轭二烯共聚物的方法，由工艺生产的改性共轭二烯共聚物，橡胶组合物和轮胎
公开(公告)号：US20110160388A1
公开(公告)日：2011-06-30
申请号：US12990407
申请日：2009-04-28
申请人： Ken Tanaka , Yoichi Ozawa , Ryuji Nakagawa , Takuo Sone , Takaimi Matsumoto , Yutaka Nagata
发明人： Ken Tanaka , Yoichi Ozawa , Ryuji Nakagawa , Takuo Sone , Takaimi Matsumoto , Yutaka Nagata
IPC分类号： C08F8/42 , C08F236/10 , C08L9/06 , C08K3/36
CPC分类号： C08L15/00 , B60C1/00 , B60C1/0016 , C08C19/22 , C08C19/25 , C08C19/44 , C08F8/42 , C08G77/442 , C08F212/00
摘要： A process for producing a modified conjugated diene-based copolymer comprising bringing a modifier into reaction with the active end of a copolymer of a conjugated diene compound and an aromatic vinyl compound having the active end, wherein a compound having (i) a hydrolyzable functional group having silicon and (ii) a group which can be converted into a protonic amino group or a protonic amino group protected with an eliminable functional group after the reaction is used as the modifier, a step of adding a condensation catalyst is conducted after the modifier is brought into the reaction, and the content of the unit of the aromatic vinyl compound and the structure of the chain of the aromatic vinyl compound are specified. The process provides a modified conjugated diene-based copolymer which is a modified product of a copolymer of a conjugated diene and an aromatic vinyl compound, provides excellent interaction between the rubber component and carbon black and/or silica, can further improve dispersion of the fillers and provides a tire exhibiting excellent low heat buildup property, fracture properties and abrasion resistance.
摘要翻译：一种改性共轭二烯系共聚物的制造方法，其特征在于，将具有（i）水解性官能团的化合物与共轭二烯化合物的共聚物的活性端与具有活性末端的芳香族乙烯基化合物反应，具有硅和（ii）在反应后作为改性剂，可以转化为质子氨基或被可消除官能团保护的质子氨基的基团，在改性剂为引入反应，指定芳族乙烯基化合物的单元含量和芳香族乙烯基化合物的链结构。该方法提供了一种改性共轭二烯基共聚物，它是共轭二烯和芳族乙烯基化合物的共聚物的改性产物，提供橡胶组分与炭黑和/或二氧化硅之间的极好的相互作用，可进一步改善填料的分散性并提供具有优异的低发热性，断裂性和耐磨性的轮胎。

23. 发明申请

US20100016496A1 PROCESS FOR PRODUCTION OF MODIFIED CONJUGATED DIENE POLYMERS, MODIFIED CONJUGATED DIENE POLYMERS PRODUCED BY THE PROCESS, RUBBER COMPOSITIONS, AND TIRES 有权
标题翻译：生产改性共轭二烯聚合物的方法，由工艺生产的改性的共混二烯聚合物，橡胶组合物和轮胎
公开(公告)号：US20100016496A1
公开(公告)日：2010-01-21
申请号：US12446799
申请日：2007-10-25
申请人： Ken Tanaka , Kouji Masaki , Yoichi Ozawa , Eiji Suzuki , Christine M. Rademacher , Terrence E. Hogan , Takuo Sone , Takaomi Matsumoto
发明人： Ken Tanaka , Kouji Masaki , Yoichi Ozawa , Eiji Suzuki , Christine M. Rademacher , Terrence E. Hogan , Takuo Sone , Takaomi Matsumoto
IPC分类号： C08L83/04 , C08G77/08
CPC分类号： C08C19/25 , B60C1/0016 , B60C1/0025 , C08C19/44 , C08K3/04 , C08K3/36 , C08L9/00 , C08L15/00 , C08L21/00 , C08L2666/08
摘要： The invention provides a process for producing a modified conjugated diene based polymer which attains favorable interaction between a rubber component and carbon black and/or silica, thereby improving dispersibility of the fillers, and which exhibits excellent properties such as heat-buildup-suppressing performance, fracture characteristics, and wear resistance; a modified conjugated diene based polymer produced through the process; a rubber composition containing the diene polymer; and a tire produced from the rubber composition and exhibiting the above properties. The process for producing a modified conjugated diene based polymer includes a step (a) of reacting a silicon compound with a conjugated diene based polymer having an active end so that the reaction takes place at the active end, the silicon compound having a protected primary amino group in the molecule thereof and a bi-functional silicon atom to which a hydrocarbyloxy group and a reactive group are bonded, to thereby modify the active end, and a step (b) of performing condensation reaction which involves the compound having a bi-functional silicon atom, in the presence of a titanium compound serving as a titanium-based condensation-accelerating agent.
摘要翻译：本发明提供了一种制备改性共轭二烯系聚合物的方法，其在橡胶组分与炭黑和/或二氧化硅之间具有良好的相互作用，从而提高填料的分散性，并且具有优异的性能如发热抑制性能，断裂特性和耐磨性; 通过该方法制备的改性共轭二烯基聚合物; 含有二烯聚合物的橡胶组合物; 以及由橡胶组合物制成并具有上述特性的轮胎。改性共轭二烯系聚合物的制造方法包括使硅化合物与具有活性末端的共轭二烯系聚合物反应的步骤（a），使得反应在活性末端进行，具有被保护的伯氨基在其分子中具有烃氧基和反应性基团键合的双功能硅原子，从而改变活性末端，以及进行缩合反应的步骤（b），其涉及具有双官能团的化合物硅原子，在用作钛基缩合促进剂的钛化合物的存在下。

24. 发明申请

US20100016500A1 PROCESS FOR PRODUCING MODIFIED POLYMER, MODIFIED POLYMER OBTAINED BY THE PROCESS, AND RUBBER COMPOSITION CONTAINING THE SAME 审中-公开
标题翻译：生产改性聚合物，由该方法获得的改性聚合物的方法和含有该聚合物的橡胶组合物
公开(公告)号：US20100016500A1
公开(公告)日：2010-01-21
申请号：US12446681
申请日：2007-10-25
申请人： Takuo Sone , Takaomi Matsumoto , Kouichirou Tani , Koji Masaki , Ken Tanaka
发明人： Takuo Sone , Takaomi Matsumoto , Kouichirou Tani , Koji Masaki , Ken Tanaka
IPC分类号： C08L9/00 , C08F136/04
CPC分类号： C08C19/44 , C08F8/42 , C08L15/00 , Y02T10/862
摘要： A process for producing a modified polymer that exhibits low rolling resistance, excellent mechanical properties (e.g., tensile strength), high wet-skid resistance, and excellent wear resistance when vulcanized, a modified polymer obtained by the process, and a rubber composition containing the same. The process includes subjecting an alkali metal active end of a conjugated diene polymer to a modification reaction with an alkoxysilane compound, the conjugated diene polymer being produced by subjecting a diene monomer or a diene monomer and a monomer other than the diene monomer to anionic polymerization in a hydrocarbon solvent using an alkali metal initiator, and subjecting the resulting product to a condensation reaction in the presence of a condensation accelerator that includes a compound of at least one element among the elements of the groups 4A (excluding Ti), 2B, 3B, and 5B of the periodic table.
摘要翻译：一种改性聚合物的制造方法，其具有低滚动阻力，优异的机械性能（例如拉伸强度），高耐湿滑性和耐硫化性优异的耐磨性，通过该方法获得的改性聚合物和含有相同。该方法包括使共轭二烯聚合物的碱金属活性末端与烷氧基硅烷化合物进行改性反应，所述共轭二烯聚合物通过使二烯单体或二烯单体和除二烯单体以外的单体进行阴离子聚合而制备使用碱金属引发剂的烃溶剂，并且在冷凝促进剂存在下使所得产物进行缩合反应，所述缩合促进剂包括4A族（不包括Ti），2B，3B等元素中的至少一种元素的化合物，和5B。

25. 发明授权

US09206264B2 Method for producing modified conjugated diene based (co)polymer, modified conjugated diene based (co)polymer, and rubber composition 有权
标题翻译：改性共轭二烯系（共）聚合物，改性共轭二烯系（共）聚合物，橡胶组合物的制造方法
公开(公告)号：US09206264B2
公开(公告)日：2015-12-08
申请号：US13347115
申请日：2012-01-10
申请人： Masahiro Shibata , Takaomi Matsumoto , Tamotsu Nagaoka , Takuo Sone , Toshihiro Tadaki
发明人： Masahiro Shibata , Takaomi Matsumoto , Tamotsu Nagaoka , Takuo Sone , Toshihiro Tadaki
IPC分类号： C08C19/44 , C08C19/12 , C08L15/00 , C08L21/00 , C08K3/00 , C08K3/04 , C08K3/34 , C08K3/36 , C08K5/548 , C08L7/00 , C08L9/00 , C08L9/02 , C08L9/06
CPC分类号： C08C19/12 , C08C19/44 , C08K3/013 , C08K3/04 , C08K3/34 , C08K3/36 , C08K5/548 , C08L7/00 , C08L9/00 , C08L9/02 , C08L9/06 , C08L15/00 , C08L21/00 , C08L2666/08 , C08K3/0033
摘要： The method for producing a modified conjugated diene based (co)polymer, according to the present invention comprises a step of reacting a conjugated diene based (co)polymer with a metal halide compound to obtain a modified conjugated diene based (co)polymer, the conjugated diene based (co)polymer having a weight-average molecular weight of 150,000 to 2,000,000 and being obtained by bonding, to a polymer having at least a conjugated diene unit, an alkoxysilyl group and an optionally protected primary amino group. The method can satisfactorily produce a conjugated diene based (co)polymer which has a high Mooney viscosity, excellent shape stability and good processability.
摘要翻译：根据本发明的改性共轭二烯系（共）聚合物的制造方法包括使共轭二烯系（共）聚合物与金属卤化物反应，得到改性共轭二烯系（共）聚合物的工序，通过与具有至少共轭二烯单元的聚合物，烷氧基甲硅烷基和任意保护的伯氨基键合获得的共轭二烯系（共）聚合物，其重均分子量为15万〜200万。该方法可以令人满意地生产具有高门尼粘度，优异形状稳定性和良好加工性能的共轭二烯基（共）聚合物。

26. 发明授权

US09172092B2 Binder composition for batteries, slurry for battery electrodes, solid electrolyte composition, electrode, and all-solid-state battery 有权
标题翻译：电池用粘结剂组合物，电池电极用浆料，固体电解质组合物，电极，全固态电池
公开(公告)号：US09172092B2
公开(公告)日：2015-10-27
申请号：US13990213
申请日：2011-11-11
申请人： Takuo Sone , Tsukasa Toyoshima
发明人： Takuo Sone , Tsukasa Toyoshima
IPC分类号： H01M4/62 , H01M10/0562
CPC分类号： H01M4/622 , H01M10/0562 , H01M2300/0082
摘要： A binder composition for batteries, including (A) a polymer that has at least one structural unit selected from the group consisting of structural units represented by the following formulae (a1) to (a5), respectively, and (f) a functional group containing a nitrogen atom, an oxygen atom, a silicon atom, a germanium atom, a tin atom or a combination thereof; and (B) a liquid medium, the polymer (A) having a solubility of no less than 5 g in 100 g of cyclohexane at 25° C. and 1 atom.
摘要翻译：一种电池用粘合剂组合物，其包含（A）具有选自由下式（a1）〜（a5）表示的结构单元的至少一种结构单元的聚合物和（f）含有氮原子，氧原子，硅原子，锗原子，锡原子或其组合; 和（B）液体介质，聚合物（A）在25℃和1个原子的100g环己烷中的溶解度不小于5g。

27. 发明授权

US07906035B2 Emulsion composition 有权
标题翻译：乳液组成
公开(公告)号：US07906035B2
公开(公告)日：2011-03-15
申请号：US10583874
申请日：2004-12-14
申请人： Kouji Tamori , Takeshi Mogi , Takuo Sone , Akira Nishikawa
发明人： Kouji Tamori , Takeshi Mogi , Takuo Sone , Akira Nishikawa
IPC分类号： C08F2/32
CPC分类号： H01B1/122 , C09D5/022 , C09D5/24 , C09J101/28 , C09J105/14
摘要： The present invention provides an emulsion composition which has been increased in sulfonic group content, yet has sufficient water resistance and has been enhanced in properties such as small resistance, film-forming property, etc. The emulsion composition contains (A) a water-based solvent, (B) an organic solvent, (C) a sulfonic group-containing polymer soluble in the component (A), and (D) a polymer soluble in the component (B) but insoluble in water. This emulsion composition is enhanced in small resistance and yet has sufficient water resistance and film-forming property.
摘要翻译：本发明提供了一种乳液组合物，其磺酸基含量增加，但具有足够的耐水性，并且在耐电阻性，成膜性等性能方面得到提高。该乳液组合物含有（A）水性溶剂，（B）有机溶剂，（C）可溶于组分（A）的含磺酸基聚合物，和（D）可溶于组分（B）但不溶于水的聚合物。该乳液组合物的电阻小，耐水性和成膜性好。

28. 发明授权

US08258241B2 Method for producing modified conjugated diene polymer, modified conjugated diene polymer, and rubber composition 有权
标题翻译：改性共轭二烯聚合物，改性共轭二烯聚合物和橡胶组合物的制备方法
公开(公告)号：US08258241B2
公开(公告)日：2012-09-04
申请号：US12521331
申请日：2007-12-27
申请人： Ryouji Tanaka , Takahiro Nakamura , Takuo Sone , Toshihiro Tadaki
发明人： Ryouji Tanaka , Takahiro Nakamura , Takuo Sone , Toshihiro Tadaki
IPC分类号： C08F136/04 , C08F4/14
CPC分类号： C08C19/44 , B60C1/00 , B60C1/0016 , B60C1/0025 , B60C1/0041 , B60C2001/0066 , C08K3/013 , C08K3/04 , C08K3/36 , C08L7/00 , C08L15/00 , C08L21/00 , C08L2666/08
摘要： A method for producing a modified conjugated diene polymer includes a modification step (A) that subjects a conjugated diene polymer having a cis-1,4-bond content of 98.5% or more and possessing an active end to a modification reaction to introduce an alkoxysilane compound having two or more reactive groups including an alkoxysilyl group into the active end of the conjugated diene polymer, and a condensation step (B) that subjects the residue of the alkoxysilane compound introduced into the active end to a condensation reaction in the presence of a condensation catalyst that includes at least one element among the elements of the groups 4A, 2B, 3B, 4B, and 5B in the periodic table. The method can produce a modified conjugated diene polymer that exhibits low heat build-up and excellent wear resistance.
摘要翻译：改性共轭二烯系聚合物的制造方法包括使顺式-1,4-键含量为98.5％以上并具有活性末端的共轭二烯聚合物进行改性反应以引入烷氧基硅烷的改性步骤（A）在共轭二烯聚合物的活性端中具有烷氧基甲硅烷基的具有两个以上的反应性基团的化合物和在引入活性末端的烷氧基硅烷化合物的残基在缩合反应存在下进行缩合步骤（B）缩合催化剂，其包括周期表中的基团4A，2B，3B，4B和5B的元素中的至少一个元素。该方法可以生产出显示低发热性和优异耐磨性的改性共轭二烯聚合物。

29. 发明申请

US20110319519A1 RUBBER COMPOSITION AND PNEUMATIC TIRE 审中-公开
标题翻译：橡胶组合物和气动轮胎
公开(公告)号：US20110319519A1
公开(公告)日：2011-12-29
申请号：US13255156
申请日：2010-03-11
申请人： Takuo Sone , Ryouji Tanaka
发明人： Takuo Sone , Ryouji Tanaka
IPC分类号： C08L25/10 , C08K3/04 , C08K3/36
CPC分类号： B60C1/0016 , C08C19/44 , C08K3/013 , C08K3/04 , C08K3/36 , C08K5/548 , C08L9/00 , C08L9/06 , C08L15/00 , Y02T10/862 , C08L2666/08
摘要： A rubber composition from which a vulcanized rubber suitable for producing, for example, a pneumatic tire having excellent abrasion resistance, breaking strength, rolling resistance, wet skid resistance, and the like can be prepared. The rubber composition comprises a rubber component (A) comprising a diene rubber comprising 20 mass % or more of a modified styrene-butadiene copolymer (a1) and 5 mass % or more of a modified conjugated diene polymer (a2), and a filler (B), wherein the modified conjugated diene polymer (a2) is a conjugated diene polymer obtained by modifying the active terminals of a conjugated diene polymer having a cis-1,4 bond content of 80% or higher, with an alkoxysilane compound, and the filler (B) comprises at least either of 2 to 100 mass parts, relative to 100 mass parts of the rubber component (A), of carbon black (b1) and 30 to 100 mass parts, relative to 100 mass parts of the rubber component (A), of silica (b2).
摘要翻译：可以制备适合于制造具有优异的耐磨性，断裂强度，滚动阻力，抗湿滑性等的充气轮胎的硫化橡胶的橡胶组合物。橡胶组合物包含橡胶组分（A），其包含二烯橡胶，其包含改性苯乙烯 - 丁二烯共聚物（a1）和20质量％以上的改性共轭二烯聚合物（a2）的20质量％以上，和填充剂 B），其中所述改性共轭二烯聚合物（a2）是通过用烷氧基硅烷化合物改性具有80％以上的顺式-1,4键含量的共轭二烯聚合物的活性末端而获得的共轭二烯聚合物，相对于100质量份的橡胶成分，填料（B）相对于100质量份橡胶成分（A），炭黑（b1）和30〜100质量份至少包含2〜100质量份（A），二氧化硅（b2）。

30. 发明申请

US20080224088A1 Emulsion Composition 有权
标题翻译：乳液成分
公开(公告)号：US20080224088A1
公开(公告)日：2008-09-18
申请号：US10583874
申请日：2004-12-14
申请人： Kouji Tamori , Takeshi Mogi , Takuo Sone , Akira Nishikawa
发明人： Kouji Tamori , Takeshi Mogi , Takuo Sone , Akira Nishikawa
IPC分类号： H01G9/025 , C08F2/32
CPC分类号： H01B1/122 , C09D5/022 , C09D5/24 , C09J101/28 , C09J105/14
摘要： The present invention provides an emulsion composition which has been increased in sulfonic group content, yet has sufficient water resistance and has been enhanced in properties such as small resistance, film-forming property, etc. The emulsion composition contains (A) a water-based solvent, (B) an organic solvent, (C) a sulfonic group-containing polymer soluble in the component (A), and (D) a polymer soluble in the component (B) but insoluble in water. This emulsion composition is enhanced in small resistance and yet has sufficient water resistance and film-forming property.
摘要翻译：本发明提供了一种乳液组合物，其磺酸基含量增加，但具有足够的耐水性，并且在耐电阻性，成膜性等性能方面得到提高。乳液组合物含有（A）水性溶剂，（B）有机溶剂，（C）可溶于组分（A）的含磺酸基聚合物，和（D）可溶于组分（B）但不溶于水的聚合物。该乳液组合物的电阻小，耐水性和成膜性好。

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