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    • 26. 发明申请
    • Method and device for analyzing the hardening of hardenable formulations
    • 用于分析可硬化制剂硬化的方法和装置
    • US20050000274A1
    • 2005-01-06
    • US10491423
    • 2002-09-27
    • Wolfgang SchrofThorsten MullerSebastian KoltzenburgMatthias KronerStephan LehmannJoachim Hadeler
    • Wolfgang SchrofThorsten MullerSebastian KoltzenburgMatthias KronerStephan LehmannJoachim Hadeler
    • G01N11/00G01N3/00G01N3/06G01N3/42G01N3/48
    • G01N3/42G01N2203/0092G01N2203/0682
    • The invention relates to a process for the combinatorial investigation of the hardening of hardenable liquid or viscous formulations (a) in which n hardenable formulations are prepared in parallel in n containers, and (b) the degree of hardening is determined at least once on each of the n formulations by inserting a measurement tip into the formulation with a certain force and measuring the maximum penetration depth achieved as a measure of the degree of hardening of this formulation, and (c) for in each case one composition of the formulations, one or more parameters that are characteristic of the kinetics of hardening are determined from the measurement values for the penetration depth at various times after preparation of the formulations. Steps (a) to (c) are preferably carried out a number of times, and a dependence of the characteristic parameter(s) on the composition of the formulations is determined by analysis of the large number of individual values obtained in this way for the parameter(s) that is (are) characteristic of the kinetics of hardening, enabling the composition of the formulations to be optimized with respect to its hardening behavior.
    • 本发明涉及用于组合研究可硬化液体或粘性制剂(a)的硬化的方法,其中在n个容器中并行制备n个可硬化制剂,和(b)硬化程度每个至少确定一次 通过以一定的力将测量尖端插入制剂中并测量作为该制剂的硬化程度的度量而获得的最大穿透深度,以及(c)在每种情况下,制剂的一种组合物,一种 或者从制剂配制后的不同时刻的穿透深度的测定值求出硬化动力学特征的更多的参数。 步骤(a)至(c)优选进行多次,并且通过分析以这种方式获得的大量个体值来确定特征参数对制剂组成的依赖性 硬化动力学特征的参数,使组合物能够根据其硬化行为进行优化。
    • 30. 发明授权
    • Process for preparing cocondensates of aspartic acid amines
    • 制备天冬氨酸胺缩合物的方法
    • US06063961A
    • 2000-05-16
    • US147370
    • 1998-12-10
    • Matthias Kroner
    • Matthias Kroner
    • C08G69/10C08G73/10C07C231/02C08F20/54
    • C08G73/1092
    • A process for preparing cocondensates of aspartic acid and amines by heating aspartic acid and amines in the presence of acidic catalysts comprises supplying the feed region of the extruder with particulate aspartic acid and a downstream metering zone with at least one amine and at least one acidic catalyst, condensing the resulting mixture to such an extent by heating that the downstream end of the extruder discharges a precondensate which contains at least 20-95% by weight of the starting aspartic acid in condensed form, and then completing the condensation of the precondensate. The cocondensates are useful as incrustation inhibitors in detergents.
    • PCT No.PCT / EP97 / 03751 Sec。 371 1998年12月10日第 102(e)日期1998年12月10日PCT 1997年7月14日PCT公布。 第WO98 / 04613号公报 日本1998年2月5日在酸性催化剂存在下,通过加热天冬氨酸和胺来制备天冬氨酸和胺的缩合物的方法包括将挤出机的进料区域供给至少一种胺的颗粒天冬氨酸和下游计量区, 至少一种酸性催化剂,通过加热将所得混合物冷凝至这样的程度,使得挤出机的下游端排出包含至少20-95重量%浓缩形式的起始天冬氨酸的预缩合物,然后完成冷凝 的预缩合物。 共缩合物可用作洗涤剂中的结垢抑制剂。