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21. 发明授权

US06326066B1 1,4-disubstituted 2,6-difluorobenzene compounds, and a liquid-crystalline medium 有权
标题翻译： 1,4-二取代的2,6-二氟苯化合物和液晶介质
公开(公告)号：US06326066B1
公开(公告)日：2001-12-04
申请号：US09514895
申请日：2000-02-28
申请人： Eike Poetsch , Volker Meyer , Volker Reiffenrath , Andreas Wachtler , Ulrich Finkenzeller , Hans Adolf Kurmeier , Reinhard Hittich , Bernhard Rieger , David Coates , Simon Greenfield , Robert William Clemitson
发明人： Eike Poetsch , Volker Meyer , Volker Reiffenrath , Andreas Wachtler , Ulrich Finkenzeller , Hans Adolf Kurmeier , Reinhard Hittich , Bernhard Rieger , David Coates , Simon Greenfield , Robert William Clemitson
IPC分类号： C09K1920
摘要： 1,4-disubstituted 2,6-difluorobenzene compound of formula I wherein R is an alkyl or alkenyl radical, A1 and A2 are independently (a) a trans-1,4-cyclohexylene radical in which a CH2 group may be replaced by -O- and/or -S, (b) a 1,4-phenylene radical in which a CH group may be replaced by N, (c) 1,4-cyclohexenylene, 1,4-bicyclo(2,2,2)octylene, piperidine-1,4-diyl, naphthalene-2,6-diyl, decahydronaphthalene-2,6-diyl or 1,2,3,4-tetrahydronaphthalene-2,6-diyl, Z1 and Z2 are —CO—O—, —O—CO—, —CH2O—,—OCH2—, —CH2CH2—, —CH═CH—,—C≡C—or a single bond m and n are 0, 1, 2 or 3, (m+n) is 1, 2 or 3, X is R or F, Cl, CF3, —OCF3, or —OCHF2, —OCF5, —CN or —NCS with the provisos that at least one of the radicals A1 and A2 present in the molecule is and at least one of Z1 or Z2 is —COO—, are suitable as components of liquid-crystalline media.
摘要翻译：式I的1,4-二取代的2,6-二氟苯化合物，其中R是烷基或烯基，A1和A2独立地是（a）反式-1,4-亚环己基，其中CH 2基可以被-O- 和/或-S，（b）其中CH基团可以被N替代的1,4-亚苯基，（c）1,4-亚环己烯基，1,4-双环（2,2,2）辛烯，哌啶-1,4-二基，萘-2,6-二基，十氢萘-2,6-二基或1,2,3,4-四氢化萘-2,6-二基，Z 1和Z 2为-CO-O-， -O-CO-，-CH 2 O - ， - OCH 2 - ， - CH 2 CH 2 - ， - CH = CH - ， - C = C-或单键，n为0,1,2或3，（m + n） 1,2或3，X是R或F，Cl，CF 3，-OCF 3或-OCHF 2，-OCF 5，-CN或-NCS，条件是分子中存在的基团A1和A2中的至少一个是和在 Z1或Z2中的至少一个是-COO-，适合作为液晶介质的组分。

22. 发明授权

US5204476A Fluorophenylpyridines 失效
标题翻译：氟代苯乙烯
公开(公告)号：US5204476A
公开(公告)日：1993-04-20
申请号：US628887
申请日：1990-12-18
申请人： Andreas Wachtler , Eike Poetsch , Thomas Geelhaar , Reinhard Hittich , Volker Reiffenrath , Hans-Michael Kompter
发明人： Andreas Wachtler , Eike Poetsch , Thomas Geelhaar , Reinhard Hittich , Volker Reiffenrath , Hans-Michael Kompter
IPC分类号： C07D213/30 , C07D213/65 , C09K19/34
CPC分类号： C07D213/30 , C07D213/65 , C09K19/3444
摘要： The invention relates to fluorophenylpyridines of the formula I: ##STR1## where R.sup.1 and R.sup.2 are substituted and unsubstituted monovalent organic radicals.
摘要翻译：本发明涉及式I的氟苯基吡啶：其中R1和R2是取代的和未取代的一价有机基团。

23. 发明授权

US5196141A 5-oxy-2-phenylpyridines, and a liquid-crystalline medium 失效
标题翻译： 5-氧代-2-苯基吡啶，和液晶介质
公开(公告)号：US5196141A
公开(公告)日：1993-03-23
申请号：US598603
申请日：1990-10-22
申请人： Andreas Wachtler , Volker Reiffenrath , Reinhard Hittich , Thomas Geelhaar , Eike Poetsch
发明人： Andreas Wachtler , Volker Reiffenrath , Reinhard Hittich , Thomas Geelhaar , Eike Poetsch
IPC分类号： G02F1/13 , C07D213/65 , C09K19/34 , C09K19/42
CPC分类号： C09K19/3444 , C07D213/65
摘要： The invention relates to 5-oxy-2-phenylpyridines of the formula I ##STR1## in which m and n, independently of one another, are each from 1 to 18,Q.sup.1 is --O--, trans-1,4-cyclohexylene, 1,4-phenylene or a single bond, andQ.sup.2 is --CO--, ##STR2## or a single bond, with the provisos that in the case where Q.sup.1 =Q.sup.2 =a single bond, the sum of m+n.gtoreq.11, and in the case where Q.sup.2 =CO, the radical C.sub.n H.sub.2n+1 is straight-chain, and to ferroelectric liquid-crystalline media containing these compounds.
摘要翻译： PCT No.PCT / EP90 / 01351 Sec。 371 1990年10月22日第 102（e）1990年10月22日PCT PCT 1990年8月17日PCT公布。出版物WO91 / 02722 日本1991年3月7日。本发明涉及式I的5-氧-2-苯基吡啶，其中m和n彼此独立地为1至18，Q 1为-O-，反式-1,4-亚环己基，1,4-亚苯基或单键，Q2为-CO-，或单键，条件是在Q1 = Q2 =单键的情况下， m + n> / = 11的和，并且在Q2 = CO的情况下，基团CnH2n + 1是直链的，并且含有这些化合物的铁电液晶介质。

24. 发明授权

US5308542A 4,4'-disubstituted 2',3-difluorobisphenyls and a liquid-crystalline medium 失效
标题翻译： 4,4'-二取代的2'，3-二氟二苯基和液晶介质
公开(公告)号：US5308542A
公开(公告)日：1994-05-03
申请号：US688490
申请日：1991-05-20
申请人： Eike Poetsch , Volker Reiffenrath , Reinhard Hittich , Bernhard Rieger
发明人： Eike Poetsch , Volker Reiffenrath , Reinhard Hittich , Bernhard Rieger
IPC分类号： C09K19/12 , C07C25/18 , C07C43/225 , C09K19/14 , C09K19/30 , C09K19/44 , G02F1/13 , C07C25/13
CPC分类号： C07C25/18 , C07C43/225 , C09K19/12 , C09K19/14 , C09K19/3003 , C09K19/3028 , C07C2101/14
摘要： The invention relates to 4,4'-disubstituted 2',3-difluorobiphenyls of the formula I ##STR1## in which n is 1 to 7, A is trans-1,4-cyclohexylene or 1,4-phenylene, r is 0 or 1, X is F, Cl, --CF.sub.3, --CHF.sub.2, --OCF.sub.3 or --OCHF.sub.2 and Z is H or F.
摘要翻译： PCT No.PCT / EP91 / 00411 Sec。 371日期1991年5月20日 102（e）日期1991年5月20日PCT 1991年3月5日PCT公布。公开号WO91 / 13850 PCT 日本1991年9月19日。本发明涉及式Ⅰ的4,4'-二取代的2'，3-二氟联苯，其中n为1至7，A为反式-1,4-亚环己基或1 ，4-亚苯基，r为0或1，X为F，Cl，-CF 3，-CHF 2，-OCF 3或-OCHF 2，Z为H或F.

25. 发明授权

US06200654B1 1,4-disubstituted 2,6-difluorobenzene compounds, and a liquid-crystalline medium 失效
标题翻译： 1,4-二取代的2,6-二氟苯化合物和液晶介质
公开(公告)号：US06200654B1
公开(公告)日：2001-03-13
申请号：US08917167
申请日：1997-08-25
申请人： Eike Poetsch , Volker Meyer , Volker Reiffenrath , Andreas Wachtler , Ulrich Finkenzeller , Hans Adolf Kurmeier , Reinhard Hittich , Bernhard Rieger , David Coates , Simon Greenfield , Robert William Clemitson
发明人： Eike Poetsch , Volker Meyer , Volker Reiffenrath , Andreas Wachtler , Ulrich Finkenzeller , Hans Adolf Kurmeier , Reinhard Hittich , Bernhard Rieger , David Coates , Simon Greenfield , Robert William Clemitson
IPC分类号： C09K1920
CPC分类号： C07C17/12 , C07C17/263 , C07C17/269 , C07C25/18 , C07C25/24 , C07C43/225 , C07C69/76 , C07C255/50 , C07C2601/14 , C07D213/26 , C07D239/26 , C09K19/0403 , C09K19/12 , C09K19/14 , C09K19/16 , C09K19/3001 , C09K19/3003 , C09K19/3028 , C09K19/3441 , C09K19/3444 , C09K19/3469 , C09K2019/0407 , C09K2019/0444 , C09K2019/3021 , Y10T428/10
摘要： 1,4-disubstituted 2,6-difluorobenzene compound of formula I wherein R is an alkyl or alkenyl radical, A1 and A2, in each case independently of one another, are (a) a trans-1,4-cyclohexylene radical in which a CH2 group may be replaced by —O— and/or —S, (b) a 1,4-phenylene radical in which a CH group may be replaced by N, (c) 1,4-cyclohexenylene, 1,4-bicyclo(2,2,2)octylene, piperidine-1,4-diyl, naphthalene-2,6-diyl, decahydronaphthalene-2,6-diyl or 1,2,3,4-tetrahydronaphthalene-2,6-diyl, Z1 and Z2 are —CO—O—, —O—CO—, —CH2—O—, —OCH2—, —CH2CH2—, —CH═CH—, —C≡C— or a single bond m and n are 0, 1, 2 or 3, (m+n) is 1, 2 or 3, X is R or F, Cl, CF3, —OCF3, or —OCHF2, —OCF5, —CN or —NCS with the proviso that at least one of the radicals A1 and A2 present in the molecule is are suitable as components of liquid-crystalline media.
摘要翻译：式Ⅰ的1,4-二取代的2,6-二氟苯化合物，其中R是烷基或烯基，A1和A2各自独立地是（a）反式-1,4-亚环己基，其中CH2 基团可以被-O-和/或-S替代，（b）其中CH基团可以被N，（c）1,4-亚环己烯基，1,4-双环（ 2,2,2）辛烯，哌啶-1,4-二基，萘-2,6-二基，十氢萘-2,6-二基或1,2,3,4-四氢化萘-2,6-二基，Z1和 Z2是-CO-O-，-O-CO-，-CH2-O-，-OCH2-，-CH2CH2-，-CH = CH-，-C = C-或单键，n为0,1， 2或3，（m + n）是1,2或3，X是R或F，Cl，CF 3，-OCF 3或-OCHF 2，-OCF 5，-CN或-NCS，条件是至少一个基团分子中存在的A1和A2适合作为液晶介质的组分。

26. 发明授权

US5496499A Biphenylethanes and liquid-crystalline phase 失效
标题翻译：双联乙烷和液晶相
公开(公告)号：US5496499A
公开(公告)日：1996-03-05
申请号：US180413
申请日：1994-01-12
申请人： Eike Poetsch , Volker Meyer , Klaus P. Stahl , Volker Reiffenrath , Ulrich Finkenzeller , Ekkehard Bartmann , Reinhard Hittich , David Coates , Simon Greenfield , Graham Smith , Hans A. Kurmeier , Dieter Dorsch
发明人： Eike Poetsch , Volker Meyer , Klaus P. Stahl , Volker Reiffenrath , Ulrich Finkenzeller , Ekkehard Bartmann , Reinhard Hittich , David Coates , Simon Greenfield , Graham Smith , Hans A. Kurmeier , Dieter Dorsch
IPC分类号： G02F1/13 , C07C22/08 , C07C25/18 , C07C25/24 , C07C43/174 , C07C43/225 , C07C205/12 , C07C255/50 , C07C323/09 , C07C323/18 , C07C323/62 , C07C331/28 , C09K19/14 , C09K19/30 , C09K19/12
CPC分类号： C07C22/08 , C07C25/18 , C07C255/50 , C07C43/225 , C09K19/14 , C09K19/3028 , C07C2101/14
摘要： Biphenylylethanes of the formula I ##STR1## in which one of the radicals R.sup.1 and R.sup.2 is X and the other radical R.sup.1 or R.sup.2 is R--Y-- whereX is H, halogen, --CF.sub.3, --OCHF.sub.2, --OCF.sub.3, --CN, --NCS or --NO.sub.2,R is alkyl, fluoroalkyl, alkenyl or oxaalkyl andY is O, S, --CO--O--, --O--CO--, --O--CO--O--, a single bond or--in the case where m=1--alternatively trans-1,4-cyclohexylene or ##STR2## m is 1 or 2, Ph is in each case identical or different radicals selected from the group comprising 1,4-phenylene, 2-fluoro-1,4-phenylene, 3-fluoro-1,4-phenylene and 3,5-difluoro-1,4-phenylene,L.sup.3 and L.sup.4 are each H, or one of these radicals is alternatively F,L.sup.1, L.sup.2and L.sup.5 are each H or F, with the proviso that in the case where X=CN or R.sup.1 =--NCS, Y is trans-1,4-cyclohexylene or ##STR3## and/or m=2 and/or one of the radicals L.sup.1, L.sup.2 and L.sup.3 is fluorine and/or Ph--CN is 2-fluoro-4-cyanophenyl or 3,5-difluoro-4-cyanophenyl,are suitable as components of liquid-crystalline phases.
摘要翻译：其中基团R 1和R 2中的一个为X并且另一个基团R 1或R 2为RY-，其中X为H，卤素，-CF 3，-OCHF 2，-OCF 3，-CN， - C 1 -C 6烷基的双苯并噻吩， NCS或-NO 2，R是烷基，氟烷基，烯基或氧杂烷基，Y是O，S，-CO-O-，-O-CO-，-O-CO-O-，单键或 - m = 1-替代反-1,4-亚环己基或m为1或2，Ph各自为相同或不同的基团，选自1,4-亚苯基，2-氟-1,4-亚苯基，亚苯基，3-氟-1,4-亚苯基和3,5-二氟-1,4-亚苯基，L3和L4各自为H，或者这些基团中的一个为F，L 1，L 2和L 5各自为H或F 条件是在X = CN或R1 = -NCS的情况下，Y为反式-1,4-亚环己基或/或m = 2，和/或基团L1，L2和L3之一为氟和/或Ph-CN是2-氟-4-氰基苯基或3,5-二氟-4-氰基苯基，适合作为液晶相的组分。

27. 发明授权

US5725796A Liquid-crystal display 失效
标题翻译：液晶显示器
公开(公告)号：US5725796A
公开(公告)日：1998-03-10
申请号：US461737
申请日：1995-06-05
申请人： Ulrich Finkenzeller , Herbert Plach , Eike Poetsch , Volker Reiffenrath
发明人： Ulrich Finkenzeller , Herbert Plach , Eike Poetsch , Volker Reiffenrath
IPC分类号： C09K19/02 , C09K19/04 , C09K19/30 , C09K19/42 , G02F1/13 , G02F1/133 , G09F9/35 , C09K19/52
CPC分类号： C09K19/0403 , C09K19/0208 , C09K19/3003 , C09K2019/0407 , C09K2019/0444
摘要： The invention relates to a liquid-crystal display based on a twisted nematic cell and having two substrates provided with electrode layers and alignment layers thereon and, with a frame, forming a cell, a nematic liquid-crystal mixture having positive dielectric anisotropy present in the cell, and a twist angle of the liquid-crystal layer in the cell with a value of between 0.degree. and 600.degree. from alignment layer to alignment layer,whose liquid-crystal mixture is based on medium-polarity compounds of the SFM type which are selected so that the liquid-crystal mixture has a viscosity at 20.degree. C. of less than 30 mm.sup.2 s.sup.-1 and has a value of K/.DELTA..di-elect cons..ltoreq.1.5 for the quotient of the Frank constant K ##EQU1## and the dielectric anisotropy .DELTA..di-elect cons. .DELTA..di-elect cons.=.di-elect cons..vertline.-.di-elect cons..sub..perp.when used in a TN cell (.nu.=.pi./2, d/p
摘要翻译：本发明涉及一种基于扭转向列单元的液晶显示器，具有在其上设置有电极层和取向层的两个基板，并且具有形成单元的框架，存在于该介质各向异性中的正的介电各向异性的向列型液晶混合物电池中的液晶层和从配向层到取向层的值在0〜600度之间的电池中的液晶层的扭转角，其液晶混合物基于SFM型的中极性化合物选择为使得液晶混合物在20℃下的粘度小于30mm 2 s -1，并且具有值+ E，ovs K + EE / DELTA +531 <= 1.5，对于Frank的商常数+ E，ovs K + EE 和介电常数各向异性DELTA +531 DELTA +531 = + 531 | - + 531当在TN单元中使用ORTHOGONAL（nu = pi / 2，d / p << 1）+ E，ovs K + EE / DELTA +531

28. 发明授权

US5578241A Liquid crystal display 失效
标题翻译：液晶显示器
公开(公告)号：US5578241A
公开(公告)日：1996-11-26
申请号：US63093
申请日：1993-05-18
申请人： Herbert Plach , Bernhard Rieger , Volker Reiffenrath , Eike Poetsch
发明人： Herbert Plach , Bernhard Rieger , Volker Reiffenrath , Eike Poetsch
IPC分类号： C09K19/30 , C09K19/52 , G02F1/13
CPC分类号： C09K19/3001 , Y10T428/1027
摘要： The invention relates to a liquid crystal display element which contains an electrically switchable, dielectrically positive twisted nematic liquid crystal layer between two substrates which together with a frame form a cell, and two layers with alignment layers thereon applied to the substrates. The liquid crystal mixture is based on SFM compounds. One of the electrodes forming an active matrix of non-linear switching elements is integrated within each picture element while the other electrode is the counter electrode. The alignment layer is an organic polymer layer which may be essential uniformly aligned by rubbing. The alignment layer results in an essential homogenous surface alignment of the liquid crystal layer with a surface tilt angle. The liquid crystal material comprises at least 30 wt. % of one or more compounds according to formula I ##STR1## wherein R, Z.sup.1, Z.sup.2, A.sup.1, A.sup.2, X, Y and n are herein defined, and the alignment layer is based on at least partially fluorinated polyimides.
摘要翻译：本发明涉及一种液晶显示元件，该液晶显示元件在两个基板之间包含电可切换的，介于上面的正扭曲向列型液晶层，该液晶显示元件与框架一起形成单元，其上具有对准层的两层施加到基板上。液晶混合物基于SFM化合物。形成非线性开关元件的有源矩阵的电极之一被集成在每个像素内，而另一个电极是对电极。取向层是有机聚合物层，其可以通过摩擦基本均匀排列。取向层导致液晶层与表面倾斜角的基本均匀的表面对准。该液晶材料包含至少30wt。％的一种或多种根据式I的化合物其中R，Z 1，Z 2，A 1，A 2，X，Y和n在此被定义，并且取向层基于至少部分氟化的聚酰亚胺。

29. 发明授权

US5480581A Liquid-crystalline medium 失效
标题翻译：液晶介质
公开(公告)号：US5480581A
公开(公告)日：1996-01-02
申请号：US224377
申请日：1994-04-07
申请人： Herbert Plach , Ulrich Finkenzeller , Volker Reiffenrath , Eike Poetsch , Bernhard Rieger , Hiroshi Numata
发明人： Herbert Plach , Ulrich Finkenzeller , Volker Reiffenrath , Eike Poetsch , Bernhard Rieger , Hiroshi Numata
IPC分类号： C09K19/12 , C09K19/30 , C09K19/34 , C09K19/42 , C09K19/44 , C09K19/46 , G02F1/13
CPC分类号： C09K19/3003 , C09K19/3001 , C09K19/44 , C09K2019/3021
摘要： The invention relates to a liquid-crystalline medium based on a mixture of polar compounds having positive dielectric anisotropy, characterized in that it contains one or more compounds of the general formula I ##STR1## in which X is fluorine, chlorine, CF.sub.3, OCF.sub.3 or OCHF.sub.2, ring A is trans-1,4-cyclohexylene or 1,4-phenylene, and R is alkyl, oxaalkyl, fluoroalkyl or alkenyl, in each case having up to 7 carbon atoms.
摘要翻译：本发明涉及一种基于具有正介电各向异性的极性化合物的混合物的液晶介质，其特征在于其含有一种或多种通式I的化合物，其中X为氟，氯，CF 3，OCF 3 或OCHF 2，环A为反式-1,4-亚环己基或1,4-亚苯基，R为烷基，氧杂烷基，氟代烷基或烯基，每种情况下具有至多7个碳原子。

30. 发明授权

US5271865A Liquid-crystalline mixture of low viscosity 失效
标题翻译：低粘度的液晶混合物
公开(公告)号：US5271865A
公开(公告)日：1993-12-21
申请号：US674367
申请日：1991-04-10
申请人： Reinhard Hittich , Herbert Plach , Volker Reiffenrath
发明人： Reinhard Hittich , Herbert Plach , Volker Reiffenrath
IPC分类号： C09K19/42 , C09K19/44 , C09K19/46 , C09K19/52 , C09K19/20 , C09K19/30 , G02F1/13
CPC分类号： C09K19/42 , C09K19/44 , C09K19/46
摘要： The invention relates to a liquid-crystalline mixture containing one or more compounds of the general formula ##STR1## in which R.sup.1 is straight-chain alkyl having 2 to 12 carbon atoms in which, in addition, one CH.sub.2 group may be replaced by --O-- or --CH.dbd.CH--, the ring A is 1,4-phenylene or trans-1,4-cyclohexylene, and r is 0 or 1, and one or more highly dielectrically positive compounds selected from the group comprising the compounds of the general formulae II, III and IV in a weight ratio between the compounds of the formula I and the compounds of the formulae II, III and IV of from 1:10 to 10:1: ##STR2## in which R.sup.2 has one of the meanings indicated for R.sup.1, and X and Y are each, independently of one another, CH or N, ##STR3## in which R.sup.2 has one of the meanings indicated for R.sup.1, and X' and Y' are CH.sub.2 or O, ##STR4## in which R.sup.2 has one of the meanings indicated for R.sup.1, r is as defined above, the rings A.sup.1 and A.sup.2 have one of the meanings indicated for A, and L is H or F.
摘要翻译： PCT No.PCT / EP91 / 00156 Sec。 371日期：1991年4月10日 102（e）1991年04月10日PCT 1991年1月28日PCT PCT。出版物WO91 / 12294 日本1991年8月22日。本发明涉及含有一种或多种通式“I”的化合物的液晶混合物，其中R 1是具有2至12个碳原子的直链烷基，其中另外一个 CH 2基团可以被-O-或-CH = CH-取代，环A是1,4-亚苯基或反式-1,4-亚环己基，r是0或1，并且选择一个或多个高反应性正性化合物来自包含通式II，III和IV的化合物的组，其中式I化合物与式II，III和IV的化合物的重量比为1:10至10:1：其中R2具有对R1表示的含义之一，X和Y各自独立地为CH或N，其中R 2具有对R 1表示的含义之一，X'和Y 是CH2或O，其中R2具有对R1表示的含义之一，r如上所定义，环A1和A2具有对A表示的含义之一，L是 H或F.

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