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    • 27. 发明申请
    • METHOD FOR REDUCING VARIABILITY IN CARBON-CARBON COMPOSITES
    • 减少碳碳复合材料变化的方法
    • US20110254182A1
    • 2011-10-20
    • US13171786
    • 2011-06-29
    • Mark L. La ForestNeil MurdieAllen H. Simpson
    • Mark L. La ForestNeil MurdieAllen H. Simpson
    • C01B31/04
    • F16D69/023C04B35/83C04B2235/608C04B2235/614C04B2235/616C04B2235/77
    • Method for producing carbon-carbon composite brake discs by: (a) providing annular nonwoven carbon fiber brake disc preforms; (b) carbonizing the brake disc preforms; (c) densifying the carbonized preforms by CVD/CVI (chemical vapor deposition/chemical vapor infiltration); (d) densifying the products of step (c) with isotropic or mesophase pitch by VPI (vacuum pitch infiltration) or RTM (resin transfer molding) processing; (e) carbonizing the preforms to remove non-carbon volatiles from the pitch and to open porosity in the pitch-infused preforms; (f) densifying the products of step (e) with isotropic or mesophase pitch by VPI or RTM processing; (g) carbonizing the preforms to remove non-carbon volatiles from pitch and to open porosity in the pitch-infused preforms; and (h) heat-treating the resulting pitch-densified carbon-carbon composite brake disc preforms. This manufacturing approach reduces lot-to-lot variability in friction performance of the resulting carbon-carbon composite brake discs.
    • 通过以下方法生产碳碳复合制动盘的方法:(a)提供环形非织造碳纤维制动盘预制件; (b)将制动盘预制件碳化; (c)通过CVD / CVI(化学气相沉积/化学气相渗透)使碳化预成型体致密化; (d)通过VPI(真空间距浸渗)或RTM(树脂传递模塑)加工使各向同性或中间相沥青致密化步骤(c)的产物; (e)将预成型坯碳化以从间距中除去非碳挥发物并在沥青注入的预制件中开孔; (f)通过VPI或RTM处理使各向同性或中间相沥青致密化步骤(e)的产物; (g)将预成型坯碳化以从间距中除去非碳挥发物并在沥青注入的预制件中开孔; 和(h)对所得沥青密实的碳 - 碳复合制动盘预制件进行热处理。 这种制造方法减少了所得碳 - 碳复合制动盘的摩擦性能的批次变化。
    • 28. 发明授权
    • CVI followed by coal tar pitch densification by VPI
    • CVI随后由VPI煤焦油沥青密实化
    • US07938992B2
    • 2011-05-10
    • US12036881
    • 2008-02-25
    • Mark L. La ForestNeil MurdieAllen H. Simpson
    • Mark L. La ForestNeil MurdieAllen H. Simpson
    • C01B31/00
    • F16D69/023C04B35/6267C04B35/83C04B2235/614C04B2235/616C04B2235/77
    • Method for manufacturing pitch-densified carbon-carbon composite brake discs from carbon fiber preforms, by the following sequential steps: (a) providing a carbon-carbon composite brake disc preform; (b) heat treating the preform; (c) subjecting the heat-treated preform to Chemical Vapor Deposition/Chemical Vapor Infiltration processing; (d) infiltrating the preform with an isotropic low to medium char-yield pitch by Vacuum Pitch Infiltration processing or Resin Transfer Molding processing; (e) carbonizing the pitch-infiltrated preform; (f) machining the surfaces of the resulting carbonized preform; and (g) repeating steps (d) through (f) until the density of the carbon-carbon composite preform is at least 1.70 g/cc. The use of VPI equipment with isotropic, low to medium char-yield pitches for all densification steps following an initial CVD densification reduces capital and pitch materials cost. However, one or more RTM processing steps employing low to medium char-yield pitches may also be used to obtain improved economics.
    • 通过以下顺序步骤从碳纤维预成型件制造俯仰致密的碳 - 碳复合制动盘的方法:(a)提供碳 - 碳复合制动盘预制件; (b)热处理预制件; (c)对经热处理的预制件进行化学气相沉积/化学气相渗透处理; (d)通过真空间距渗透处理或树脂转移成型处理,以各向同性的低至中等焦度的沥青渗透预型体; (e)沥青渗透预制件碳化; (f)加工所得碳化预成型件的表面; 和(g)重复步骤(d)至(f),直到碳 - 碳复合预型体的密度为至少1.70g / cc。 在初始CVD致密化之后,对于所有致密化步骤使用具有各向同性,低至中等焦炭距离的VPI设备,减少了材料和沥青材料的成本。 然而,也可以使用采用低至中等焦炭间距的一个或多个RTM处理步骤来获得改进的经济性。
    • 30. 发明授权
    • Method for reducing variability in carbon-carbon composites
    • 降低碳 - 碳复合材料变异性的方法
    • US08268208B2
    • 2012-09-18
    • US13171786
    • 2011-06-29
    • Mark L. La ForestNeil MurdieAllen H. Simpson
    • Mark L. La ForestNeil MurdieAllen H. Simpson
    • C01B31/00
    • F16D69/023C04B35/83C04B2235/608C04B2235/614C04B2235/616C04B2235/77
    • Method for producing carbon-carbon composite brake discs by: (a) providing annular nonwoven carbon fiber brake disc preforms; (b) carbonizing the brake disc preforms; (c) densifying the carbonized preforms by CVD/CVI (chemical vapor deposition/chemical vapor infiltration); (d) densifying the products of step (c) with isotropic or mesophase pitch by VPI (vacuum pitch infiltration) or RTM (resin transfer molding) processing; (e) carbonizing the preforms to remove non-carbon volatiles from the pitch and to open porosity in the pitch-infused preforms; (f) densifying the products of step (e) with isotropic or mesophase pitch by VPI or RTM processing; (g) carbonizing the preforms to remove non-carbon volatiles from pitch and to open porosity in the pitch-infused preforms; and (h) heat-treating the resulting pitch-densified carbon-carbon composite brake disc preforms. This manufacturing approach reduces lot-to-lot variability in friction performance of the resulting carbon-carbon composite brake discs.
    • 通过以下方法生产碳碳复合制动盘的方法:(a)提供环形非织造碳纤维制动盘预制件; (b)将制动盘预制件碳化; (c)通过CVD / CVI(化学气相沉积/化学气相渗透)使碳化预成型体致密化; (d)通过VPI(真空间距浸渗)或RTM(树脂传递模塑)加工使各向同性或中间相沥青致密化步骤(c)的产物; (e)将预成型坯碳化以从间距中除去非碳挥发物并在沥青注入的预制件中开孔; (f)通过VPI或RTM处理使各向同性或中间相沥青致密化步骤(e)的产物; (g)将预成型坯碳化以从间距中除去非碳挥发物并在沥青注入的预制件中开孔; 和(h)对所得沥青密实的碳 - 碳复合制动盘预制件进行热处理。 这种制造方法减少了所得碳 - 碳复合制动盘的摩擦性能的批次变化。