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21. 发明授权

US06548703B1 Toning agent 失效
标题翻译：调色剂
公开(公告)号：US06548703B1
公开(公告)日：2003-04-15
申请号：US09581743
申请日：2000-06-16
申请人： Ryuzo Ueno , Masaya Kitayama , Kenji Minami , Masamitsu Kubotsu
发明人： Ryuzo Ueno , Masaya Kitayama , Kenji Minami , Masamitsu Kubotsu
IPC分类号： C07C23305
CPC分类号： C09B67/0046 , C07C65/11 , C07C69/94 , C07C235/66 , C09B29/106 , C09B29/20
摘要： A toning agent for an azo pigment, an azo pigment with a modified tone, and process for preparing the same are provide. 2-hydroxynaphthalene-3,6-dicarboxylic acid or a derivative thereof is admixed with a primary coupler component for an azo pigment and the mixed coupler composition and an aromatic diazonium are coupled.
摘要翻译：提供了一种偶氮颜料调色剂，具有改性色调的偶氮颜料及其制备方法。将2-羟基萘-3,6-二羧酸或其衍生物与偶氮颜料的一级偶合剂组分混合，并将混合的偶合剂组合物和芳族重氮偶合。

22. 发明授权

US06252104B1 Naphthol derivatives and process for producing the same 失效
标题翻译：萘酚衍生物及其制备方法
公开(公告)号：US06252104B1
公开(公告)日：2001-06-26
申请号：US08764269
申请日：1996-12-12
申请人： Ryuzo Ueno , Shigeru Ito , Kenji Minami , Masaya Kitayama
发明人： Ryuzo Ueno , Shigeru Ito , Kenji Minami , Masaya Kitayama
IPC分类号： C07C22900
CPC分类号： C07C235/64 , C07C65/11 , C07C65/24 , C07C69/94 , C07C235/66 , C07C275/54 , C07C311/46 , C07C2603/24 , C07D209/88 , C07D235/26
摘要： A naphthol derivative represented by the general formula (I), [wherein Y and Y′ indicate —(CONH)n—X or —COR; X is a phenyl group, a naphthyl group, an anthraquinonyl group, a benzimidazolonyl group or a carbazolyl group; R is a hydroxyl group, an alkoxy group having 1 to 6 carbon atoms, a halogen atom, a benzyloxy group, a phenyloxy group or a phenacyloxy group; R2 is a hydrogen atom, an alkaline metal, an alkyl group having 1 to 6 carbon atoms, an acyl group having 1 to 6 carbon atoms or a phenylalkyl group; Z is a group selected from the group consisting of a hydrogen atom, a halogen atom, a nitro group, a nitroso group and an amino group (Z may be substituted on any ring of the naphthalene ring); and n is an integer of 1 or 2; provided that R2 and Z do not simultaneously indicate a hydrogen atom when both R simultaneously indicate a hydroxyl group], and a process for producing the same. This naphthol derivative can be used as raw materials for synthesis, such as dyes, pigments, photosensitive materials and the like.
摘要翻译：由通式（I）表示的萘酚衍生物[其中Y和Y'表示 - （CONH）n -X或-COR; X是苯基，萘基，蒽醌基，苯并咪唑啉基或咔唑基; R为羟基，碳原子数为1〜6的烷氧基，卤原子，苄氧基，苯氧基或苯甲酰氧基。 R2是氢原子，碱金属，碳原子数1〜6的烷基，碳原子数1〜6的酰基或苯基烷基; Z是选自氢原子，卤素原子，硝基，亚硝基和氨基的基团（Z可以在萘环的任意环上被取代）; n为1或2的整数; 条件是当两个R同时表示羟基时，R2和Z不同时表示氢原子]及其制备方法。该萘酚衍生物可以用作合成原料，如染料，颜料，感光材料等。

23. 发明授权

US06239263B1 Water-soluble azo compounds and process for the preparation thereof 失效
标题翻译：水溶性偶氮化合物及其制备方法
公开(公告)号：US06239263B1
公开(公告)日：2001-05-29
申请号：US09380207
申请日：1999-08-26
申请人： Ryuzo Ueno , Masaya Kitayama , Kenji Minami , Masaharu Kittaka
发明人： Ryuzo Ueno , Masaya Kitayama , Kenji Minami , Masaharu Kittaka
IPC分类号： C09B62507
CPC分类号： C09B62/51
摘要： Novel water-soluble azo compounds useful as raw materials for preparing dyes excellent in dyeing properties and fastness and prepared from a coupler consisting of 2-hydroxynaphthalene-3,6-dicarboxylic acid or an ester thereof or an amide derivative of the same and a diazonium compound having a group of the general formula: —B—(CH2)2- Q or —B′—(CH2)2-Q′ (wherein B and B′ are each an electron-attracting group; and Q and Q′ are each a group capable of forming a vinyl group through the elimination with an alkali, provided the groups Q and Q′ are each bonded at the &bgr;-position of the ethyl group).
摘要翻译：新颖的水溶性偶氮化合物可用作制备染料性能和牢度优良的染料的原料，并由由2-羟基萘-3,6-二羧酸或其酯或其酰胺衍生物组成的成色剂和重氮具有以下通式的基团：-B-（CH2）2-Q或-B' - （CH2）2-Q'（其中B和B'各自为吸电子基团; Q和Q'为每个是能够通过用碱去除形成乙烯基的基团，条件是基团Q和Q'各自键合在乙基的β-位）。

24. 发明授权

US6020470A Water-soluble azo compounds and process for producing the same 失效
标题翻译：水溶性偶氮化合物及其制备方法
公开(公告)号：US6020470A
公开(公告)日：2000-02-01
申请号：US254949
申请日：1999-03-22
申请人： Ryuzo Ueno , Masaya Kitayama , Kenji Minami , Masaharu Kittaka
发明人： Ryuzo Ueno , Masaya Kitayama , Kenji Minami , Masaharu Kittaka
IPC分类号： C09B62/008 , C09B62/085 , C09B62/245 , D06P1/382
CPC分类号： C09B62/0083 , C09B62/085 , C09B62/245
摘要： The present invention provides novel water-soluble azo compounds derived from 2-hydroxynaphthalene-3,6-dicarboxylic acid or derivatives thereof and diazonium salts having sulfo group(s). These compounds are useful as raw materials for dyes having excellent dyeing properties and fastness.
摘要翻译： PCT No.PCT / JP98 / 03750 Sec。 371日期1999年3月22日 102（e）1999年3月22日PCT提交1998年8月25日PCT公布。出版物WO99 / 11717 1999年3月11日本发明提供了由2-羟基萘-3,6-二羧酸或其衍生物衍生的新型水溶性偶氮化合物和具有磺基的重氮盐。这些化合物可用作染色性和牢度优异的染料的原料。

25. 发明授权

US5847233A Naphthol derivatives and process for producing the same 失效
标题翻译：萘酚衍生物及其制备方法
公开(公告)号：US5847233A
公开(公告)日：1998-12-08
申请号：US975189
申请日：1997-11-20
申请人： Ryuzo Ueno , Shigeru Ito , Kenji Minami , Masaya Kitayama
发明人： Ryuzo Ueno , Shigeru Ito , Kenji Minami , Masaya Kitayama
IPC分类号： C07C65/11 , C07C65/24 , C07C69/94 , C07C235/64 , C07C235/66 , C07C275/54 , C07C311/46 , C07D209/88 , C07D235/26 , C07C39/14
CPC分类号： C07C235/64 , C07C235/66 , C07C275/54 , C07C311/46 , C07C65/11 , C07C65/24 , C07C69/94 , C07D209/88 , C07D235/26 , C07C2103/24
摘要： A naphthol derivative represented by the general formula (I) �wherein Y and Y' indicate --(CONH).sub.n --X or --COR; X is a phenyl group, a naphthyl group, an anthraquinonyl group, a benzimidazolonyl group or a carbazolyl group; R is a hydroxyl group, an alkoxy group having 1 to 6 carbon atoms, a halogen atom, a benzyloxy group, a phenyloxy group or a phenacyloxy group; R.sub.2 is a hydrogen atom, an alkaline metal, an alkyl group having 1 to 6 carbon atoms, an acyl group having 1 to 6 carbon atoms or a phenylalkyl group; Z is a group selected from the group consisting of a hydrogen atom, a halogen atom, a nitro group, a nitroso group and an amino group (Z may be substituted on any ring of the naphthalene ring); and n is an integer of 1 or 2; provided that R.sub.2 and Z do not simultaneously indicate a hydrogen atom when both R simultaneously indicate a hydroxyl group!, and a process for producing the same. This naphthol derivative can be used as raw materials for synthesis, such as dyes, pigments, photosensitive materials and the like. ##STR1##
摘要翻译：由通式（I）表示的萘酚衍生物[其中Y和Y'表示 - （CONH）n -X或-COR; X是苯基，萘基，蒽醌基，苯并咪唑啉基或咔唑基; R为羟基，碳原子数为1〜6的烷氧基，卤原子，苄氧基，苯氧基或苯甲酰氧基。 R2是氢原子，碱金属，碳原子数1〜6的烷基，碳原子数1〜6的酰基或苯基烷基; Z是选自氢原子，卤素原子，硝基，亚硝基和氨基的基团（Z可以在萘环的任意环上被取代）; n为1或2的整数; 条件是当两个R同时表示羟基时，R2和Z不同时表示氢原子]及其制备方法。该萘酚衍生物可以用作合成原料，如染料，颜料，感光材料等。（一）

26. 发明申请

US20060264670A1 Crystal of p-hydroxybenzoic anhydride and process for producing the same 有权
标题翻译：对羟基苯甲酸酐的结晶及其制备方法
公开(公告)号：US20060264670A1
公开(公告)日：2006-11-23
申请号：US10553451
申请日：2004-04-12
申请人： Ryuzo Ueno , Masaya Kitayama , Nobutaka Izumichi , Masaharu Kittaka
发明人： Ryuzo Ueno , Masaya Kitayama , Nobutaka Izumichi , Masaharu Kittaka
IPC分类号： C07C51/56
CPC分类号： C07C51/43 , C07B2200/13 , C07C65/03
摘要： The present invention provides a process for preparing crystalline parahydroxybenzoic acid anhydride, comprising the step of precipitating and isolating parahydroxybenzoic acid in an aqueous solvent at a temperature equal to or above the transition temperature of parahydroxybenzoic acid.
摘要翻译：本发明提供一种制备结晶对羟基苯甲酸酐的方法，包括在等于或高于对羟基苯甲酸的转变温度的温度下在水性溶剂中沉淀和分离对羟基苯甲酸的步骤。

27. 发明授权

US06451109B1 Columnar crystals of 6-hydroxy-2-naphthoic acid and process for manufacturing the same 有权
标题翻译： 6-羟基-2-萘甲酸的柱状晶体及其制造方法
公开(公告)号：US06451109B1
公开(公告)日：2002-09-17
申请号：US09830119
申请日：2001-04-24
申请人： Ryuzo Ueno , Masaya Kitayama , Hiroyuki Kato , Ryoichi Otsuka
发明人： Ryuzo Ueno , Masaya Kitayama , Hiroyuki Kato , Ryoichi Otsuka
IPC分类号： C30B700
CPC分类号： C07C51/43 , C30B7/00 , C07C65/11
摘要： A process for manufacturing columnar crystals of 6-hydroxy-2-naphthoic acid comprising the steps of, dissolving crude 6-hydroxy-2-naphthoic acid product in an aqueous solvent, adding crystalline 3-hydroxy-2,7-naphthoic acid or columnar crystals as seed crystals, and cooling the mixture to precipitate the desired crystals. The present invention further provides columnar crystals of 6-hydroxy-2-naphthoic acid which have X-ray diffraction peaks 2&thgr; in 16.8-17.8 and/or 21.3-22.3.
摘要翻译：一种制备6-羟基-2-萘甲酸的柱状晶体的方法，包括以下步骤：将6-羟基-2-萘甲酸粗产物溶解在水性溶剂中，加入结晶的3-羟基-2,7-萘甲酸或柱状晶体作为晶种，并冷却混合物以沉淀所需的晶体。本发明还提供在16.8-17.8和/或21.3-22.3中具有X射线衍射峰2θ的6-羟基-2-萘甲酸的柱状晶体。

28. 发明申请

US20090048362A1 Method of Modifying Liquid Crystal Polymers 有权
标题翻译：液晶聚合物改性方法
公开(公告)号：US20090048362A1
公开(公告)日：2009-02-19
申请号：US12223695
申请日：2007-01-31
申请人： Ryuzo Ueno , Kunikazu Asaka , Kazuyuki Hirao , Shingo Kanehira , Masaya Kitayama
发明人： Ryuzo Ueno , Kunikazu Asaka , Kazuyuki Hirao , Shingo Kanehira , Masaya Kitayama
IPC分类号： C08J3/28 , C08G63/00 , C08G65/38 , C08G65/40
CPC分类号： C08J3/28 , B29C71/04 , B29C2035/0838 , B29K2105/24 , C08G63/065 , C08G63/88 , C08J7/123
摘要： A method of modifying liquid crystal polymers, which involves a step of irradiating a liquid crystal polymer with the laser beam having a pulse width of 10−12 seconds or less. Using the invention method, the physical strength of the liquid crystal polymers can be improved as compared with the conventional liquid crystal polymers.
摘要翻译：一种改变液晶聚合物的方法，其包括用脉冲宽度为10-12秒或更短的激光束照射液晶聚合物的步骤。使用本发明的方法，与以往的液晶聚合物相比，能够提高液晶聚合物的物理强度。

29. 发明申请

US20060183939A1 Process for production of hydroxybenzoic acids 审中-公开
标题翻译：羟基苯甲酸的制备方法
公开(公告)号：US20060183939A1
公开(公告)日：2006-08-17
申请号：US10547763
申请日：2004-03-02
申请人： Ryuzo Ueno , Masaya Kitayama , Ryoichi Otsuka , Takeshi Shirai
发明人： Ryuzo Ueno , Masaya Kitayama , Ryoichi Otsuka , Takeshi Shirai
IPC分类号： C07C51/15
CPC分类号： C07C51/15 , C07C65/03
摘要： The present invention provides A method for producing a hydroxybenzoic acid compound comprising, preparing an alkali metal salt of a phenol compound from the phenol compound, and reacting the alkali metal salt of the phenol compound with carbon dioxide, wherein the step of preparing the alkali metal salt of the phenol compound from the phenol compound comprises the steps of: a) reacting an alkali metal alkoxide with an excess amount of the phenol compound, which is in excess of the alkali metal alkoxide, to give the alkali metal salt of the phenol compound, and b) distilling away the generated alcohol from the reaction simultaneously with carrying out step a). The method of the present invention makes it possible to produce hydroxybenzoic acid compound in high yield without using aprotic polar organic solvent.
摘要翻译：本发明提供一种羟基苯甲酸化合物的制造方法，其特征在于，含有由酚化合物制备酚化合物的碱金属盐，使酚化合物的碱金属盐与二氧化碳反应，其中，制备碱金属酚酚化合物的盐包括以下步骤：a）使碱金属醇盐与过量碱金属醇盐的过量的酚化合物反应，得到酚化合物的碱金属盐，和b）在进行步骤a）的同时蒸馏生成的醇与反应物。本发明的方法使得可以在不使用非质子极性有机溶剂的情况下高产率生产羟基苯甲酸化合物。

30. 发明授权

US06403827B1 Crystal of 2-hydroxynaphthalene-3-carboxylic acid and process for the preparation thereof 有权
标题翻译： 2-羟基萘-3-羧酸的晶体及其制备方法
公开(公告)号：US06403827B1
公开(公告)日：2002-06-11
申请号：US09720994
申请日：2001-01-03
申请人： Ryuzo Ueno , Masaya Kitayama , Nobutaka Izumichi , Hiroyuki Kato
发明人： Ryuzo Ueno , Masaya Kitayama , Nobutaka Izumichi , Hiroyuki Kato
IPC分类号： C07C6334
CPC分类号： C07C65/11 , C07C51/412 , C07C51/43
摘要： The present invention provides crystalline 2-hydroxynaphthalene-3-carboxylic acid (BON) characterized in that the average particle size is equal to or more than 157 &mgr;m and the proportion of the particles of which particle size is less than 74 &mgr;m is equal to or less than 14%. The crystalline composition of the present invention can be prepared by a process comprising the step of recrystallizing BON, especially at a high temperature, or by carrying out the acid precipitation step in the method for preparing BON at a high temperature.
摘要翻译：本发明提供结晶的2-羟基萘-3-羧酸（BON），其特征在于平均粒径等于或大于157μm，粒径小于74μm的颗粒的比例等于或等于小于14％。本发明的结晶组合物可以通过包括重结晶BON的步骤，特别是在高温下或通过在高温下进行BON制备方法进行酸沉淀步骤的方法来制备。

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